Plastic Behavior and Deformation Structure of Silicide Single Crystals with Transition Metals at High Temperatures

1993 ◽  
Vol 322 ◽  
Author(s):  
Y. Umakoshi ◽  
T. Nakashima ◽  
T. Nakano ◽  
E. Yanagisawa
Keyword(s):  
Brittle Fracture ◽  
Slip System ◽  
Single Crystals ◽  
Low Temperatures ◽  
Plastic Behavior ◽  
Deformation Structure ◽  
Secondary Slip ◽  
Ambient Temperatures ◽  
Brittle Transition ◽  
Increasing Temperature

AbstractThe mechanical and plastic behaviors of refractory silicide single crystals with Cllb (MoSi2), C40 (CrSi2, TaSi2 and NbSi2), D88 (Ti5Si3) and Cl (CoSi2 and (Co0.9Ni0.1)Si2) structures were investigated. The C40–type silicides were deformed by (0001)<1120> slip. Their yield stress decreased sharply with increasing temperature but NbSi2 and TaSi2 which were deformable even at low temperatures, exhibited anomalous strengthening around 1350°C. Deformation of Ti5Si3 whose ductile-brittle transition occurred around 1300°C was controlled by twins and the brittle fracture occurred on the basal plane. In CoSi2 the {001}<100> slip was only activated at ambient temperatures but addition of Ni activated {110}<110> slip as secondary slip system and improved the ductility. The creep behavior of MoSi2 and CrSi2 single crystals were also investigated and was found to be controlled by the viscous and glide motion of dislocations.

Kink and Crack Interfaces in Deformed 6H-SiC Single Crystals

1994 ◽  
Vol 357 ◽  
Author(s):  
X. J. Ning ◽  
P. Pirouz
Keyword(s):  
Low Temperature ◽  
Slip System ◽  
Single Crystal ◽  
Single Crystals ◽  
Basal Plane ◽  
Prism Plane ◽  
Secondary Slip ◽  
Micro Cracks ◽  
Indentation Tests ◽  
Temperature Deformations

AbstractWhen a 6H-SiC single crystal is deformed under indentation or uniaxial compression in orientations not favorable for the activation of the 1/3[1120](0001) easy glide system, the secondary slip system is activated. Additionally, for low- temperature deformations, “kinks” and/or micro-cracks form in the crystal. In this paper, experimental results on relatively lowtemperature compression and indentation tests of single crystal 6H-SiC, and the microstructure of the deformed crystals, are presented. Based on the results, the secondary slip system in 6HSiC has been determined to be 1/3[1120](1100), which may actually be a combination of alternate glide of 1/3[1120] dislocations on the (1102) and (1102) planes. Further, dislocation mechanisms for the nucleation of prism-plane and basal-plane cracks, and for the process of kinking, in deformed 6H-SiC are proposed.

Laufzeitmessungen in Fluoren-Einkristallen / Transit Time Measurements in Fluorene Single Crystals

1977 ◽  
Vol 32 (6) ◽  
pp. 580-587
Author(s):  
H. Eckhardt
Keyword(s):  
Single Crystals ◽  
Transit Time ◽  
Low Temperatures ◽  
Pulse Shape ◽  
Room Temperature ◽  
Trap Depth ◽  
Drift Mobility ◽  
Temperature Ranges ◽  
Increasing Temperature ◽  
Shallow Traps

Abstract The hole drift mobility in single crystals of fluorene was determined by transit time measurements. At room temperature the mobility along the c-axis is (0,82 ± 0,14) cm2/Vs and in the abplane (0,72 ± 0,1) cm2/Vs. In the temperature ranges 200K<T<300K and 165K<T<300K μc and μab have been found to be ~T-1,5 and ~T-1,0, respectively. In both cases the mobility reaches a constant value for low temperatures (100 K). In the range 300 K<T<345 K μ decreases very strongly with increasing temperature {μ~T-5). Traps, especially deep and shallow surface traps, influence the pulse heighth and the pulse shape. From the change of the pulse shape with temperature a trap depth EH = 0,4 eV for shallow traps is determined.

Computational Aspects of Elasto-Plastic Deformation in Polycrystalline Solids

2012 ◽  
Vol 79 (3) ◽  
Author(s):  
Ronaldo I. Borja ◽  
Helia Rahmani
Keyword(s):  
Constitutive Equation ◽  
Slip System ◽  
Single Crystals ◽  
Plastic Behavior ◽  
Slip Systems ◽  
Exact Integration ◽  
Computational Aspects ◽  
System Activation ◽  
Crystallographic Planes ◽  
Return Algorithm

The overall elasto-plastic behavior of single crystals is governed by individual slips on crystallographic planes, which occur when the resolved shear stress on a critical slip system reaches a certain maximum value. The challenge lies in identifying the activated slip systems for a given load increment since the process involves selection from a pool of linearly dependent slip systems. In this paper, we use an “ultimate algorithm” for the numerical integration of the elasto-plastic constitutive equation for single crystals. The term ultimate indicates exact integration of the elasto-plastic constitutive equation and explicit tracking of the sequence of slip system activation. We implement the algorithm into a finite element code and report the performance for polycrystals subjected to complicated loading paths including non-proportional and reverse/cyclic loading at different crystal orientations. It is shown that the ultimate algorithm is comparable to the widely used radial return algorithm for J2 plasticity in terms of global numerical stability.

In situ Tensile Experiments at Low Temperatures on Niobium Single Crystals by H.V.E.M.

1975 ◽  
Vol 33 ◽  
pp. 58-59
Author(s):  
F. H. Louchet ◽  
L. P. Kubin
Keyword(s):  
Electron Microscope ◽  
Transition Temperature ◽  
Low Temperature ◽  
Slip System ◽  
Low Temperatures ◽  
Tensile Axis ◽  
Image Intensifier ◽  
Screw Dislocations ◽  
Source Operation

Experiments have been carried out on the 3 MeV electron microscope in Toulouse. The low temperature straining holder has been previously described Images given by an image intensifier are recorded on magnetic tape.The microtensile niobium samples are cut in a plane with the two operative slip directions [111] and lying in the foil plane. The tensile axis is near [011].Our results concern:- The transition temperature of niobium near 220 K: at this temperature and below an increasing difference appears between the mobilities of the screw and edge portions of dislocations loops. Source operation and interactions between screw dislocations of different slip system have been recorded.

Investigation of shock-wave deformation history from recovered structure

1986 ◽  
Vol 44 ◽  
pp. 434-435
Author(s):  
M.A. Mogilevsky ◽  
L.S. Bushnev
Keyword(s):  
Shock Wave ◽  
Plastic Deformation ◽  
Dislocation Density ◽  
Shock Waves ◽  
Shock Front ◽  
Single Crystals ◽  
Residual Deformation ◽  
Deformation Structure ◽  
Deformation History ◽  
Deformation Velocity

Single crystals of Al were loaded by 15 to 40 GPa shock waves at 77 K with a pulse duration of 1.0 to 0.5 μs and a residual deformation of ∼1%. The analysis of deformation structure peculiarities allows the deformation history to be re-established.After a 20 to 40 GPa loading the dislocation density in the recovered samples was about 1010 cm-2. By measuring the thickness of the 40 GPa shock front in Al, a plastic deformation velocity of 1.07 x 108 s-1 is obtained, from where the moving dislocation density at the front is 7 x 1010 cm-2. A very small part of dislocations moves during the whole time of compression, i.e. a total dislocation density at the front must be in excess of this value by one or two orders. Consequently, due to extremely high stresses, at the front there exists a very unstable structure which is rearranged later with a noticeable decrease in dislocation density.

scholarly journals A Comparative Electrochemical and Morphological Investigation on the Behavior of NiCr and CoCr Dental Alloys at Various Temperatures

Metals ◽  
2021 ◽  
Vol 11 (2) ◽  
pp. 256
Author(s):  
Florentina Golgovici ◽  
Mariana Prodana ◽  
Florentina Gina Ionascu ◽  
Ioana Demetrescu
Keyword(s):  
Low Temperatures ◽  
Artificial Saliva ◽  
Electrochemical Stability ◽  
Morphological Investigation ◽  
Dental Alloys ◽  
Ion Release ◽  
Icp Ms ◽  
Different Temperatures ◽  
Good Concordance ◽  
Increasing Temperature

The purpose of our study is to compare the behavior of two reprocessed dental alloys (NiCr and CoCr) at different temperatures considering the idea that food and drinks in the oral cavity create various compositions at different pH levels; the novelty is the investigation of temperature effect on corrosion parameters and ion release of dental alloys. Electrochemical stability was studied together with morphology, elemental composition and ions release determination. The results obtained are in good concordance: electrochemistry studies reveal that the corrosion rate is increasing by increasing the temperature. From SEM coupled with EDS, the oxide film formed on the surface of the alloys is stable at low temperatures and a trend to break after 310K. ICP-MS results evidence that in accordance with increasing temperature, the quantities of ions released from the alloys immersed in artificial saliva also increase, though they still remain small, less than 20 ppm.

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