A Novel Processing Route for the Fabrication of Monolithic and Composite Silicon Nitride

1992 ◽  
Vol 287 ◽  
Author(s):  
R. V. Raman ◽  
S. V. Rele
Keyword(s):  
Volume Fraction ◽  
Hot Isostatic Pressing ◽  
Thermal Exposure ◽  
Processing Route ◽  
Promising Alternative ◽  
Α Phase ◽  
Key Issues ◽  
Novel Processing ◽  
Composite Silicon

ABSTRACTCurrent hot isostatic consolidation methodology used for the fabrication of complex-shaped Si3N4-based components requires the use of an expensive glass encapsulation technique and extended thermal exposure (in hours) of the specimen. An alternative consolidation approach involving the use of solid pressure transmitting media under high pressure, has enabled the consolidation of Si3N4 alloys without the need for glass encapsulation.Characterization of microstructures and mechanical properties of this (MOR, fracture toughness) material has been carried out and will be presented. It has been noted that in Si 3N4/8%Y2O3-4%Al2O3 composition, consolidated using this approach, a significantly larger volume fraction of α phase has been retained compared with typically observed conversion in α⇒ β in hot isostatically pressed material or sintered material.Key issues for addressing densification and microstructure control using this process are presented. This rapid consolidation approach appears to be a promising alternative to hot isostatic pressing for the fabrication of complex-shaped Si3N4 components.

Evaluation of a Ni-20Cr Alloy Processed by Multi-Axis Forging

2006 ◽  
Vol 503-504 ◽  
pp. 793-798 ◽  
Author(s):  
R. DiDomizio ◽  
M.F.X. Gigliotti ◽  
J.S. Marte ◽  
P.R. Subramanian ◽  
Vener Valitov
Keyword(s):  
Grain Size ◽  
Room Temperature ◽  
High Cycle Fatigue ◽  
Thermal Exposure ◽  
Fatigue Properties ◽  
Processing Route ◽  
Bulk Alloy ◽  
Processed Material ◽  
Fatigue Data ◽  
Novel Processing

This paper discusses the development of a novel processing route to produce ultra finegrain bulk alloy forgings; the microstructural response of these forgings to thermal exposure; and the comparison of mechanical properties to those from conventionally processed material. A Ni- 20Cr [wt%] alloy was processed by near-isothermal multi-axis forging to a grain size of approximately 1 μm. A heat-treatment study over the range 900 to 1200°C was conducted to determine the resultant grain size as a function of time and temperature. Tensile properties were measured at room temperature, 500°C, and 930°C. High-cycle fatigue properties were measured at room temperature. The room-temperature tensile strength was approximately 2.5 times greater than that of conventionally processed Ni-20Cr. Fatigue data showed that the room-temperature highcycle fatigue run-out stress was greater than 100% of the yield stress.

Characterization of Global and Local Textures in Hot Rolled CGO Fe3%Si

2006 ◽  
Vol 509 ◽  
pp. 25-30 ◽  
Author(s):  
Francisco Cruz-Gandarilla ◽  
Thierry Baudin ◽  
Marie Helene Mathon ◽  
Richard Penelle ◽  
Hector Mendoza León ◽  
...  
Keyword(s):  
Volume Fraction ◽  
Distribution Functions ◽  
Processing Route ◽  
Rolled Sheet ◽  
Electron Backscattered Diffraction ◽  
Goss Texture ◽  
Hot Rolled ◽  
Global And Local ◽  
Half Thickness

The present work is an attempt to understand the recrystallisation mechanisms in Fe-3% Si alloys used in transformer cores. After secondary recrystallisation silicon steels exhibit a Goss texture with a more or less important spread depending on the details of the processing route, namely, Conventional Grain Orientation CGO or High Permeability Hi-B. The mechanisms of Goss grain formation during hot rolling and primary recrystallisation, as well as those controlling the first steps of abnormal growth, are not yet well understood. The present work mainly deals with texture characterization of the hot rolled state. Surface, quarter and half thickness samples are prepared from hot-rolled sheet. Global and local textures are characterized by neutron diffraction and electron backscattered diffraction, respectively. The Orientation Distribution Functions and the volume fraction of the different texture components are calculated. The components from global texture measurements are (001)[1-10], (112)[1-10] (α fiber ), (011)[100] (Goss) and (111)[1-21] (111) [1-10](γ fiber). EBSD measurements have shown large variations of texture from the surface to the half thickness of the sheet. These local measurements are related to the global results by rotation about the transverse direction. Moreover, the grain size appears to be inhomogeneous.

scholarly journals HOT-DEFORMATION BEHAVIOR OF HOT ISOSTATIC PRESSED Ti-6Al-4V ALLOY DURING HOT COMPRESSION

2021 ◽  
Vol 55 (4) ◽  
Author(s):  
Haijun Liu ◽  
Zhimin Zhang ◽  
Kaihua Xu ◽  
Jishi Zhang ◽  
Yong Xue ◽  
...  
Keyword(s):  
Strain Rate ◽  
Volume Fraction ◽  
Hot Isostatic Pressing ◽  
Strain Curve ◽  
Strain Rates ◽  
Stress Strain Curve ◽  
Single Pass ◽  
Α Phase ◽  
Deformation Pass ◽  
The One

A single-pass and multi-pass compression experiments with a Ti-6Al-4V alloy fabricated with hot isostatic pressing (HIP) were carried out on a Gleeble-1500D simulator. The true stress-strain curve, microstructure and microhardness of the alloy deformed at a total strain of about 70 % were studied. The results show that the stress value increased as the strain rate increased during each deformation pass and the same was true for the single pass. At the initial deformation stage, the flow stress increased rapidly with the increase in the strain until it reached the peak; then it showed a different softening extent, which was more obvious for the three-pass deformation than for one-pass and two-pass deformation. During the multi-pass deformation, the lamellar α phase was mainly distorted, but during the one-pass and two-pass deformation, it was bent; the spheroidisation of the lamellar α phase mainly occurred during the three-pass deformation, significantly increasing the extent of softening. Meanwhile, the degree of the spheroidized α phase and the volume fraction of β-transformed phase (βt) increased as the strain rates increased. Finally, a tri-modal microstructure, including the β-transformed phase (βt), lamellar α phase and equiaxed α phase was obtained during three-pass deformation. In the process of multi-pass deformation, the microhardness increased with the increase in deformation passes. When the strain rate was 1 s–1, the microhardness increased from 299.5 HV and 309.1 HV to 342.6 HV with the increase in deformation passes. It was also found that the microhardness increased with an increase in the strain rate under a certain amount of deformation.

Direct imaging of order-disorder and antiphase domain structures in Ti3Al intermetallic compound

1990 ◽  
Vol 48 (4) ◽  
pp. 480-481
Author(s):  
H. Q. Ye ◽  
T.S. Xie ◽  
D. Li
Keyword(s):  
Intermetallic Compound ◽  
Volume Fraction ◽  
Fundamental Problem ◽  
Antiphase Domain ◽  
Atomic Scale ◽  
Orientation Relationships ◽  
Domain Structures ◽  
Α Phase ◽  
Diffraction Patterns ◽  
Two Phases

The Ti3Al intermetallic compound has long been recognized as potentially useful structural materials. It offers attractive strength to weight and elastic modulus to weight ratios. Recent work has established that the addition of Nb to Ti3Al ductilized this compound. In this work the fundamental problem of this alloy, i.e. order-disorder and antiphase domain structures was investigated at the atomic scale.The Ti3Al+10at%Nb alloys used in this study were treated at 1060°C and then aged at 700°C for 2 hours. The specimens suitable for TEM were prepared by standard jet electrolytic-polishing technique. A JEM-200CX electron microscope with an interpretable resolution of about 0.25 nm was used for HREM.The [100] and [001] projections of the α2 phase were shown in Fig.l.The alloy obtained consist of at least two phases-α2(Ti3Al) and β0 structures. Moreover, a disorder α phase with small volume fraction was also observed. Fig.2 gives [100] and [001] diffraction patterns of the α2 phase. Since lattice parameters of the ordered α2 (a=0.579, c=0.466 nm) and disorder α phase (a0=0.294≈a/2, c0=0.468 nm) are almost the same, their diffraction patterns are difficult to be distinguished when they are overlapped with epitaxial orientation relationships.

scholarly journals Isolation and Characterization of Salmonella Jumbo-Phage pSal-SNUABM-04

Viruses ◽  
2020 ◽  
Vol 13 (1) ◽  
pp. 27
Author(s):  
Jun Kwon ◽  
Sang Guen Kim ◽  
Hyoun Joong Kim ◽  
Sib Sankar Giri ◽  
Sang Wha Kim ◽  
...  
Keyword(s):  
Morphological Traits ◽  
Open Reading Frames ◽  
Genome Comparison ◽  
The Novel ◽  
Promising Alternative ◽  
Isolation And Characterization ◽  
Global Issue ◽  
Reading Frames ◽  
Predicted Function

The increasing emergence of antimicrobial resistance has become a global issue. Therefore, many researchers have attempted to develop alternative antibiotics. One promising alternative is bacteriophage. In this study, we focused on a jumbo-phage infecting Salmonella isolated from exotic pet markets. Using a Salmonella strain isolated from reptiles as a host, we isolated and characterized the novel jumbo-bacteriophage pSal-SNUABM-04. This phage was investigated in terms of its morphology, host infectivity, growth and lysis kinetics, and genome. The phage was classified as Myoviridae based on its morphological traits and showed a comparatively wide host range. The lysis efficacy test showed that the phage can inhibit bacterial growth in the planktonic state. Genetic analysis revealed that the phage possesses a 239,626-base pair genome with 280 putative open reading frames, 76 of which have a predicted function and 195 of which have none. By genome comparison with other jumbo phages, the phage was designated as a novel member of Machinavirus composed of Erwnina phages.

scholarly journals Design of Low-Cost and High-Strength Titanium Alloys Using Pseudo-Spinodal Mechanism through Diffusion Couple Technology and CALPHAD

Materials ◽  
2021 ◽  
Vol 14 (11) ◽  
pp. 2910
Author(s):  
Chaoyi Ding ◽  
Chun Liu ◽  
Ligang Zhang ◽  
Di Wu ◽  
Libin Liu
Keyword(s):  
Diffusion Couple ◽  
Titanium Alloys ◽  
High Throughput ◽  
Volume Fraction ◽  
Raw Materials ◽  
Low Cost ◽  
High Strength ◽  
High Yield ◽  
Α Phase ◽  
Cr System

The high cost of development and raw materials have been obstacles to the widespread use of titanium alloys. In the present study, the high-throughput experimental method of diffusion couple combined with CALPHAD calculation was used to design and prepare the low-cost and high-strength Ti-Al-Cr system titanium alloy. The results showed that ultra-fine α phase was obtained in Ti-6Al-10.9Cr alloy designed through the pseudo-spinodal mechanism, and it has a high yield strength of 1437 ± 7 MPa. Furthermore, application of the 3D strength model of Ti-6Al-xCr alloy showed that the strength of the alloy depended on the volume fraction and thickness of the α phase. The large number of α/β interfaces produced by ultra-fine α phase greatly improved the strength of the alloy but limited its ductility. Thus, we have demonstrated that the pseudo-spinodal mechanism combined with high-throughput diffusion couple technology and CALPHAD was an efficient method to design low-cost and high-strength titanium alloys.

Magnetic Characterization of SUS316L Deformed by High Pressure Torsion

2011 ◽  
Vol 239-242 ◽  
pp. 1300-1303
Author(s):  
Hong Cai Wang ◽  
Minoru Umemoto ◽  
Innocent Shuro ◽  
Yoshikazu Todaka ◽  
Ho Hung Kuo
Keyword(s):  
Plastic Deformation ◽  
High Pressure ◽  
Stainless Steel ◽  
Phase Transformation ◽  
Austenitic Stainless Steel ◽  
Volume Fraction ◽  
High Pressure Torsion ◽  
Austenitic Matrix ◽  
Magnetic Characterization

SUS316L austenitic stainless steel was subjected to severe plastic deformation (SPD) by the method of high pressure torsion (HPT). From a fully austenitic matrix (γ), HPT resulted in phase transformation from g®a¢. The largest volume fraction of 70% a¢ was obtained at 0.2 revolutions per minute (rpm) while was limited to 3% at 5rpm. Pre-straining of g by HPT at 5rpm decreases the volume fraction of a¢ obtained by HPT at 0.2rpm. By HPT at 5rpm, a¢®g reverse transformation was observed for a¢ produced by HPT at 0.2rpm.

Estimation of Interlayer Thickness in Inorganic Particulate-Filled Polymer Composites

2011 ◽  
Vol 24 (6) ◽  
pp. 777-788 ◽  
Author(s):  
J.Z. Liang
Keyword(s):  
Polymer Composites ◽  
Volume Fraction ◽  
Particle Diameter ◽  
Interfacial Structure ◽  
Interlayer Thickness ◽  
Filled Polymer ◽  
Mechanical And Physical Properties ◽  
The Relationship ◽  
Good Agreement

The structure of the interlayer between matrix and inclusions affect directly the mechanical and physical properties of inorganic particulate-filled polymer composites. The interlayer thickness is an important parameter for characterization of the interfacial structure. The effects of the interlayer between the filler particles and matrix on the mechanical properties of polymer composites were analyzed in this article. On the basis of a simplified model of interlayer, an expression for estimating the interlayer thickness ([Formula: see text]) was proposed. In addition, the relationship between the [Formula: see text] and the particle size and its concentration was discussed. The results showed that the calculations of the [Formula: see text] and thickness/particle diameter ratio ([Formula: see text]) increased nonlinearly with an increase of the volume fraction of the inclusions. Moreover, the predictions of [Formula: see text] and the relevant data reported in literature were compared, and good agreement was found between them.

Characterization of Micro-Pore Structure in Novel Cement Matrices

2014 ◽  
Vol 1712 ◽  
Author(s):  
Seyoon Yoon ◽  
Isabel Galan ◽  
Kemal Celik ◽  
Fredrik P. Glasser ◽  
Mohammed S. Imbabi
Keyword(s):  
Portland Cement ◽  
Pore Structure ◽  
Engineering Properties ◽  
Calcium Sulfoaluminate ◽  
Pore Structures ◽  
Porosity And Permeability ◽  
Experimental Protocols ◽  
Novel Processing ◽  
Main Component

ABSTRACTCalcium sulfoaluminate (CSA) cements are being developed using a novel processing method having as its objective lowering specific CO2 emissions by ∼50% relative to a Portland cement benchmark. We need to be able to measure the properties of the products. Porosity and permeability measurements help define the engineering properties but their quantification is influenced by the choice of experimental protocols. In the present study we used ordinary Portland cement (PC) paste as a benchmark and hydrated ye’elimite, which is a main component of CSA cements, to understand its pore structure. We report on the use of synchrotron-sourced radiation for µCT (Computerized Tomography) and 3D image re-construction of the internal micro-pore structure of PC and ye’elimite-gypsum pastes. As a comparison, porosity and permeability measurements were traditionally obtained using Mercury Intrusion Porosimetry (MIP). The Mori-Tanaka method and the polynomial statistical model were used to analyze the effects of different 3-D micro-pore structures on mechanical properties. The results show that e micro-pore structures differ considerably between PC and ye’elimite pastes and their bulk modulus is significantly affected by the shapes of their micro-pore structures.

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