Substrate Pretreatments and Strength Limiting Factors in Cu-AlN Direct Bonds

1992 ◽  
Vol 282 ◽  
Author(s):  
Wan-Lan Chiang ◽  
Victor A. Greenhut ◽  
Daniel J. Shanefield ◽  
Lois A. Johnson
Keyword(s):  
Bond Strength ◽  
Failure Modes ◽  
Peel Strength ◽  
Limiting Factors ◽  
Thermal Expansion Mismatch ◽  
High Temperature Annealing ◽  
Optimum Thickness ◽  
Different Temperatures ◽  
Bond Strengths ◽  
Main Factor

ABSTRACTCu-AlN direct bonds were made by the gas-metal eutectic method. Two kinds of AlN substrates from different suppliers were used for the research. The AlN surfaces were preoxidized in O2 at three different temperatures. An optional “anneal” in Ar was applied following the oxidation procedure. Two processes were used for the bonding.The bond strengths and the failure modes were found to depend on the substrate used, the pretreatment of the AlN and bonding conditions. There was an optimum thickness for the Al2O3 layer on the AlN surface. High temperature annealing in Ar was demonstrated to effectively promote bond strength. The highest peel strength measured was 50 N/cm.A thermal expansion mismatch between Al2O3 and AlN was considered to be the main factor which dominated the ultimate bond strength. This mismatch resulted in a residual stress in the Al2O3 layer. A measurement by XRD indicated a 300 MPa tensile stress existed in the surface Al2O3 after AlN oxidation. This made Al2O3/AlN the weakest interface and limited the bond strength rather than the eutectic bond.

scholarly journals Shear Bond Strength of Brackets Rebonded with a Fluoride-Releasing and -Recharging Adhesive System

2009 ◽  
Vol 79 (3) ◽  
pp. 564-570 ◽  
Author(s):  
Toshiya Endo ◽  
Rieko Ozoe ◽  
Koichi Shinkai ◽  
Makiko Aoyagi ◽  
Hiroomi Kurokawa ◽  
...  
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Failure Modes ◽  
Testing Machine ◽  
Adhesive System ◽  
Adhesive Systems ◽  
Bond Failure ◽  
Minimum Requirement ◽  
Adhesive Remnant Index ◽  
Bond Strengths

Abstract Objective: To ascertain the effects of repeated bonding on the shear bond strength of orthodontic brackets bonded with a fluoride-releasing and -recharging adhesive system with a self-etching primer in comparison with two other types of adhesive system. Materials and Methods: A total of 48 premolars were collected and divided equally into three groups of 16. Each group was assigned one of three adhesive systems: Transbond XT, Transbond Plus, or a fluoride-releasing and -recharging adhesive system, Beauty Ortho Bond. Shear bond strength was measured 24 hours after bracket bonding, with the bonding/debonding procedures repeated twice after the first debonding. A universal testing machine was used to determine shear bond strengths, and bracket/adhesive failure modes were evaluated with the adhesive remnant index after each debonding. Results: At every debonding sequence, all of these three adhesive systems had a shear bond strength of 6 MPa, which is a minimum requirement for clinical use. Transbond XT and Transbond Plus had significantly higher mean shear bond strengths than did Beauty Ortho Bond at each debonding. No significant differences in mean bond strength were observed between the three debondings in each adhesive system. Bond failure at the enamel/adhesive interface occurred more frequently in Beauty Ortho Bond than in Transbond XT or Transbond Plus. Conclusions: The fluoride-releasing and -recharging adhesive system with the self-etching primer (Beauty Ortho Bond) had clinically sufficient shear bond strength in repeated bracket bonding; this finding can help orthodontists to decrease the risk of damage to enamel at debonding.

scholarly journals Adhesion of real seal to human root dentin treated with different solutions

2012 ◽  
Vol 23 (5) ◽  
pp. 521-526 ◽  
Author(s):  
Renata Baldissera ◽  
Ricardo Abreu da Rosa ◽  
Márcia Helena Wagner ◽  
Milton Carlos Kuga ◽  
Fabiana Soares Grecca ◽  
...  
Keyword(s):  
Bond Strength ◽  
Root Canal ◽  
Failure Modes ◽  
Chlorhexidine Gluconate ◽  
The Other ◽  
Significant Difference ◽  
Root Dentin ◽  
Bond Strengths ◽  
Group 2 ◽  
Push Out

The aim of this study was to evaluate the effects of different irrigants on sealer-dentin bond strength when using Real Seal. Thirty single-rooted teeth were divided into 3 groups. In one group, the teeth were irrigated with 3 mL of 2.5% NaOCl after each file change, flushed with 17% EDTA for 3 min and finally rinsed with 3 mL of 2.5% NaOCl. In the other two groups, rinse with NaOCl was replaced with 2% chlorhexidine gluconate (CHX) and 0.9% saline, respectively. Each root was sectioned transversally into apical, middle and coronal thirds to obtain 2-mm-thick slices. Each slice was filled with Real Seal and Resilon. Push-out test was used to analyze bond strength and failure modes were classified as adhesive, cohesive or mixed, according to SEM observations. The push-out test did not reveal any statistically significant difference (p>0.05) between the irrigants. However, the groups exhibited significantly different (p<0.05) bond strengths in terms of the root canal third. Higher bond strength was observed at the apical third when compared with coronal third, while middle third presented intermediary values. Fifteen specimens were analyzed by SEM (5 per group). Eleven specimens exhibited adhesive failures (5 in saline, 4 in NaOCl and 2 in CHX group); 2 cohesive failures were observed in the CHX group, and 1 mixed failure each was observed in the CHX and NaOCl groups. The tested irrigants did not influence the bond strength of Resilon and Real Seal to dentin. The apical third exhibited higher mean bond strengths and adhesive failures were predominant.

scholarly journals Bond strength of modern self-adhesive resin cements to human dentin and different CAD/CAM ceramics

2020 ◽  
Vol 22 (2) ◽  
Author(s):  
Andrzej Małysa ◽  
Joanna Weżgowiec ◽  
Dariusz Danel ◽  
Klauss Boening ◽  
Katarzyna Walczak ◽  
...  
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Failure Modes ◽  
Resin Cements ◽  
Adhesive Resin ◽  
Shear Strength Test ◽  
Software Failure ◽  
Human Dentin ◽  
Cad Cam ◽  
Bond Strengths

Purpose: The aim of the study was to evaluate the shear bond strength of CAD/CAM ceramics to dentin after cementation with conventional or self-adhesive resin cements. Methods: Three self-adhesive, self-etching cements (Panavia SA, RelyX U200, Maxcem Elite), and one conventional cement (Panavia V5), were selected to lute three CAD/CAM ceramics (IPS Empress CAD, IPS e.max CAD, IPS e.max ZirCAD) onto the dentin. The bond strength was evaluated using a shear strength test according to the PN-EN ISO 29022:2013-10. Evaluation of the differences was performed using the Statistica software. Failure modes were analyzed using a light microscope. Results: All the studied cements differed (regardless of the ceramic type) in the bond strength. The highest bond strength was observed in Panavia V5, lower – in RelyX U200 and Panavia SA, and the lowest – in Maxcem. For IPS e.max ZirCAD, it was observed that compared to Panavia V5, the other cements were characterized by a significantly higher bond strength. For the IPS Empress CAD and the IPS e.max CAD, Panavia V5 displayed the highest bond strength. For all the studied self-adhesive cements, the failure of adhesion between the cement and dentin was predominant mode. Conclusions: Significant differences were found in the shear bond strengths of the CAD/CAM ceramics luted to dentin using tested self-adhesive and conventional cements. The bond strength depended on the combination of ceramic and cement. The IPS e.max ZirCAD had the highest bond strength to dentin after cementation with RelyX U200, while the IPS Empress CAD and IPS e.max CAD – with Panavia V5.

scholarly journals Effects of CPP-ACP Paste on the Shear Bond Strength of Orthodontic Brackets

2009 ◽  
Vol 79 (5) ◽  
pp. 945-950 ◽  
Author(s):  
Ding Xiaojun ◽  
Lu Jing ◽  
Guo Xuehua ◽  
Ruan Hong ◽  
Yu Youcheng ◽  
...  
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Failure Modes ◽  
Artificial Saliva ◽  
Orthodontic Brackets ◽  
Acid Etching ◽  
Bonding System ◽  
Significant Difference ◽  
Bond Strengths ◽  
Scanning Electron

Abstract Objective: To evaluate the effect of casein phosphopeptide–amorphous calcium phosphate (CPP-ACP) paste on shear bond strength and debonding failure modes of orthodontic brackets. Materials and Methods: Freshly extracted premolars were randomly divided into four groups (n =18) as follows: in groups 1 and 3, the enamel was treated with a solution of CPP-ACP dissolved in artificial saliva; groups 2 and 4 served as controls, and the enamel was treated with artificial saliva. After conventional acid etching, in groups 1 and 2, brackets were bonded using a light-cured bonding system (Blugloo); while in groups 3 and 4, brackets were bonded using a conventional bonding system (Unite Bonding Adhesive). Bonded specimens were subjected to thermal cycling for 1000 cycles before debonding procedures. After debonding, teeth and brackets were examined under a stereomicroscope at 10× magnification to determine whether any adhesive remained, in accordance with the adhesive remnant index. The acid-etched enamel surfaces were also observed using scanning electron microscopy after treatment with and without CPP-ACP paste. Results: The shear bond strengths of group 1 were significantly higher than those seen in group 2 (P &lt; .01). There was no significant difference in the shear bond strengths of groups 3 and 4 (P &gt; .05). Scanning electron microscopic observation showed that the pretreated enamel surface was rougher than that of the control surface after acid etching. Conclusion: The use of CPP-ACP can be considered as an alternative prophylactic application in orthodontic practice since it did not compromise bracket bond strength.

Incremental Layer Shear Bond Strength of Low-shrinkage Resin Composites Under Different Bonding Conditions

2014 ◽  
Vol 39 (6) ◽  
pp. 603-611 ◽  
Author(s):  
AH Al Musa ◽  
HNA Al Nahedh
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Failure Modes ◽  
Resin Composites ◽  
Adhesive Resin ◽  
Aging Conditions ◽  
Bond Strengths

SUMMARY The purpose of this study was to determine the incremental shear bond strength of a silorane-based composite (Filtek Silorane) repaired with silorane or a methacrylate-based composite (Filtek Z250) under various aging conditions. Also, the incremental bond strength of the silorane-based composite was compared with that of another low-shrinkage methacrylate-based composite (Aelite LS Posterior) under fresh and aged conditions, with and without the use of an adhesive resin between successive layers. The two brands of low-shrinkage composites were compared with a microhybrid, Filtek Z250, which served as the control. Substrate discs were fabricated and second layers were adhered to them immediately, after two weeks of aging, or after four weeks of aging and with and without an adhesive resin. Shear bond strengths were measured and failure modes were evaluated. The incremental bond strength of silorane to the silorane-based composite was not significantly different from that of the methacrylate-based composite. However, repairing a silorane-based composite with a methacrylate-based composite significantly reduced the bond strength. Aelite showed a lower incremental bond strength than Z250 and silorane, but the use of an adhesive significantly improved the bond strength. The absence of an oxygen-inhibited layer did not affect the bond strength of the consecutive layers of the silorane-based composite.

scholarly journals Comparison of Shear Bond Strength of Calcium-enriched Mixture Cement and Mineral Trioxide Aggregate to Composite Resin

2011 ◽  
Vol 12 (6) ◽  
pp. 457-462 ◽  
Author(s):  
Siavash Savadi Oskoee ◽  
Soodabeh Kimyai ◽  
Mahmoud Bahari ◽  
Paria Motahari ◽  
Mohammad Jafar Eghbal ◽  
...  
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Failure Modes ◽  
Composite Resin ◽  
Mineral Trioxide Aggregate ◽  
Acid Etching ◽  
Surface Etching ◽  
Machine Failure ◽  
Significant Difference ◽  
Bond Strengths

ABSTRACT Aim Adhesion of composite resin and pulp capping biomaterials remarkably influences treatment outcomes. This in vitro study aimed to compare the shear bond strength of composite resin to calcium enriched mixture (CEM) cement, mineral trioxide aggregate (MTA) and resin modified glass ionomer (RMGI) with or without acid etching. Materials and methods A total of 90 cylindrical acrylic blocks containing a central hole, measuring 4 mm diameter and 2 mm height were prepared. The blocks were randomly divided into three experimental groups based on being filled with CEM, MTA or RMGI. Samples in each group were then randomly divided into two subgroups, i.e. with or without phosphoric acid etching. Placing composite resin cylinders on the samples, shear bond strengths were measured using a universal testing machine. Failure modes of the samples were evaluated under a stereomicroscope. Data were analyzed using two-way ANOVA and Tukey tests. Results Shear bond strengths in the etched and nonetched samples were not significantly different (p = 0.60). There was a significant difference in shear bond strength values of the three experimental materials (p < 0.001) and RMGI showed the highest strength values (p < 0.001); no significant difference was observed between MTA and CEM (p = 0.51). The interaction of the type of material and surface etching was statistically significant (p < 0.001). All of the samples showed cohesive failure mode. Conclusion Acid etching of MTA, CEM and RMGI do not improve the shear bond strength of these materials to composite resin. Besides, shear bond strength values of MTA and CEM to composite resin, are favorable due to their cohesive mode of failure. Clinical significance When MTA and CEM biomaterials are used in vital pulp therapy, it is advisable to cover these materials with RMGI. In addition, if it is not possible to use RMGI, the surface etching of MTA and CEM biomaterials is not necessary prior to composite restoration using total-etch adhesive resin. How to cite this article Oskoee SS, Kimyai S, Bahari M, Motahari P, Eghbal MJ, Asgary S. Comparison of Shear Bond Strength of Calcium-enriched Mixture Cement and Mineral Trioxide Aggregate to Composite Resin. J Contemp Dent Pract 2011;12(6):457-462.

Experimental Research on Bond Strength between Rebar and Concrete after High Temperature

2011 ◽  
Vol 71-78 ◽  
pp. 1057-1061 ◽  
Author(s):  
Ke Fang Yin ◽  
Yang Han ◽  
Yi Liu
Keyword(s):  
Reinforced Concrete ◽  
High Temperature ◽  
Bond Strength ◽  
Experimental Research ◽  
Bonding Strength ◽  
Different Temperatures ◽  
Ultimate Bond Strength

With the centrally pulling-out test, the bond strength of reinforced concrete is measured with different temperatures and different cooling ways after high temperature; and the ultimate bond strength and slip of reinforced and concrete under different conditions are analyzed. The results show that the bonding strength declines gradually with the increase of temperature, and the ultimate slippage also decreases gradually.

scholarly journals Shear bond strength of orthodontic brackets to enamel after application of a caries infiltrant

2014 ◽  
Vol 85 (4) ◽  
pp. 645-650 ◽  
Author(s):  
Laura Mews ◽  
Matthias Kern ◽  
Robert Ciesielski ◽  
Helge Fischer-Brandies ◽  
Bernd Koos
Keyword(s):  
Statistical Analysis ◽  
Bond Strength ◽  
Shear Force ◽  
Shear Bond Strength ◽  
Orthodontic Brackets ◽  
Enamel Defects ◽  
Adhesive Remnant Index ◽  
Demineralized Enamel ◽  
Kolmogorov Smirnov ◽  
Bond Strengths

ABSTRACT Objective:  To examine differences in the shear bond strength of orthodontic brackets on differently mineralized enamel surfaces after applying a caries infiltrant or conventional adhesive. Materials and Methods:  A total of 320 bovine incisors were assigned to eight pretreated groups, and the shear force required for debonding was recorded. Residual adhesive was evaluated by light microscopy using the adhesive remnant index. Statistical analysis included Kolmogorov-Smirnov, analysis of variance (ANOVA), and Scheffé tests. Results:  The highest bond strength (18.8 ± 4.4 MPa) was obtained after use of the caries infiltrant. More residual adhesive and fewer enamel defects were observed on infiltrated enamel surfaces. Brackets on demineralized enamel produced multiple enamel defects. Conclusions:  Acceptable bond strengths were obtained with all material combinations. A caries-infiltrant applied before bracket fixation has a protective effect, especially on demineralized enamel.

scholarly journals Effect of Using Nano and Micro Airborne Abrasive Particles on Bond Strength of Implant Abutment to Prosthesis

2015 ◽  
Vol 26 (1) ◽  
pp. 50-55 ◽  
Author(s):  
Mansour Rismanchian ◽  
Amin Davoudi ◽  
Elham Shadmehr
Keyword(s):  
Bond Strength ◽  
Testing Machine ◽  
Control Group ◽  
Abrasive Particles ◽  
Significant Difference ◽  
Implant Abutments ◽  
Implant Abutment ◽  
Roughened Surface ◽  
Bond Strengths ◽  
Spss Software

Connecting prostheses to the implant abutments has become a concern and achieving a satisfactory retention has been focused in cement-retention prostheses recently. Sandblasting is a method to make a roughened surface for providing more retention. The aim of this study was to compare effects of nano and micro airborne abrasive particles (ABAP) in roughening surface of implant abutments and further retention of cemented copings. Thirty Xive abutments and analogues (4.5 D GH1) were mounted vertically in self-cured acrylic blocks. Full metal Ni-Cr copings with a loop on the top were fabricated with appropriate marginal adaptation for each abutment. All samples were divided into 3 groups: first group (MPS) was sandblasted with 50 µm Al2O3 micro ABAP, second group (NSP) was sandblasted with 80 nm Al2O3 nano ABAP, and the third group (C) was assumed as control. The samples were cemented with provisional cement (Temp Bond) and tensile bond strength of cemented copings was evaluated by a universal testing machine after thermic cycling. The t test for independent samples was used for statistical analysis by SPSS software (version 15) at the significant level of 0.05. Final result showed significant difference among all groups (p<0.001) and MPS manifested the highest mean retention (207.88±45.61 N) with significant difference among other groups (p<0.001). The control group showed the lowest bond strength as predicted (48.95±10.44 N). Using nano or micro ABAP is an efficient way for increasing bond strengths significantly, but it seems that micro ABAP was more effective.

scholarly journals Effects of Fluorosis and Self Etching Primers on Shear Bond Strengths of Orthodontic Brackets

2009 ◽  
Vol 03 (03) ◽  
pp. 173-177 ◽  
Author(s):  
Ahmet Yalcin Gungor ◽  
Hakan Turkkahraman ◽  
Necdet Adanir ◽  
Huseyin Alkis
Keyword(s):  
Bond Strength ◽  
Testing Machine ◽  
Orthodontic Brackets ◽  
Universal Testing ◽  
Adhesive Remnant Index ◽  
Halogen Light ◽  
Significant Difference ◽  
Bond Strengths ◽  
Group Ii ◽  
Clinical Changes

ABSTRACTObjectives: To evaluate the effects fluorosis and self etching primers (SEP) on shear bond strengths (SBS) of orthodontic brackets.Methods: A total of 48 (24 fluorosed and 24 non-fluorosed) non-carious freshly extracted human permanent premolar teeth were used in this study. Fluorosed teeth were selected according to the modified Thylstrup and Fejerskov index (TFI), which is based on the clinical changes in fluorosed teeth. Fluorosed and non-fluorosed teeth were randomly assigned to 4 groups of 12 each. In groups I (non-fluorosed teeth) and II (fluorosed teeth), standard etching protocol was used and brackets were bonded with Light Bond. In groups III (non-fluorosed teeth) and IV (fluorosed teeth), Transbond Plus SEP was used and brackets were bonded with Transbond XT Light Cure Adhesive. All specimens were cured with a halogen light. After bonding, SBS of the brackets were tested with Universal testing machine. After debonding, all teeth and brackets in the test groups were examined under 10x magnifications. Any adhesive remained after debonding was assessed and scored according to the modified Adhesive Remnant Index (ARI).Results: ANOVA indicated a significant difference between groups (P<.001). SBS in group II (Light Bond+Fluorosis) were significantly lower than other groups. ARI scores of the groups were also significantly different (P<.001). There was a greater frequency of ARI scores of 1,2 and 3 in group II (Light Bond+Fluorosis).Conclusions: When standard etching protocol was used enamel fluorosis significantly decreased the bond strength of orthodontic brackets. Satisfactory bond strengths were obtained when SEP was used for bonding brackets to the fluorosed teeth. (Eur J Dent 2009;3:173-177)

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