Time-Dependent Deformation in Room-Temperature Indentation Experiments using a Nanoindenter

1991 ◽  
Vol 239 ◽  
Author(s):  
Shefford P. Baker ◽  
Troy W. Barbee ◽  
William D. Nix

ABSTRACTTime-dependent deformation in room-temperature indentation is a well known phenomenon which is frequently overlooked in depth-sensing indentation experiments. In this study, the time-dependent displacements which occur during depth-sensing indentation experiments using a Nanoindenter were investigated. Time-dependent displacements were found to result both from plastic deformation of the sample and experimental drift. A simple correction for experimental drift was applied in experiments on sputtered copper thin films and reasonable strain rate sensitivities were obtained. The sources of experimental drift were identified and measured. It appears to be possible to measure the rate-dependence of plastic deformation in a variety of materials using this instrument.

1997 ◽  
Vol 505 ◽  
Author(s):  
S. N. Dub

ABSTRACTA method to obtain curves of elasto-plastic deformation of materials in depth-sensing indentation tests is proposed. Elasto-plastic deformation curves of thin films and brittle materials have been received at room temperature using this method.


2007 ◽  
Vol 22 (2) ◽  
pp. 258-263 ◽  
Author(s):  
B.C. Wei ◽  
L.C. Zhang ◽  
T.H. Zhang ◽  
D.M. Xing ◽  
J. Das ◽  
...  

The strain rate dependence of plastic deformation of Ce60Al15Cu10Ni15 bulk metallic glass was studied by nanoindentation. Even though the ratio of room temperature to the glass transition temperature was very high (0.72) for this alloy, the plastic deformation was dominated by shear banding under nanoindentation. The alloy exhibited a critical loading rate dependent serrated flow feature. That is, with increasing loading rate, the alloy exhibited a transition from less prominent serrated flow to pronounced serrated flow during continuous loading but from serrated to smoother flow during stepped loading.


1997 ◽  
Vol 119 (3) ◽  
pp. 216-222 ◽  
Author(s):  
E. M. Arruda ◽  
S. Ahzi ◽  
Y. Li ◽  
A. Ganesan

We examine the strain rate dependent, large plastic deformation in isotropic semi-crystalline polypropylene at room temperature. Constant strain rate uniaxial compression tests on cylindrical polypropylene specimens show very little true strain softening under quasi-static conditions. At high strain rates very large amounts (38 percent) of apparent strain softening accompanied by temperature rises are recorded. We examine the capability of a recently proposed constitutive model of plastic deformation in semi-crystalline polymers to predict this behavior. We neglect the contribution of the amorphous phase to the plastic deformation response and include the effects of adiabatic heating at high strain rates. Attention is focused on the ability to predict rate dependent yielding, strain softening, strain hardening, and adiabatic temperature rises with this approach. Comparison of simulations and experimental results show good agreement and provide insight into the merits of using a polycrystalline modeling assumption versus incorporating the amorphous contribution. Discrepancies between experiments and model predictions are explained in terms of expectations associated with neglecting the amorphous deformation.


2018 ◽  
Vol 385 ◽  
pp. 59-64 ◽  
Author(s):  
Roberto B. Figueiredo ◽  
Pedro Henrique R. Pereira ◽  
Terence G. Langdon

The mechanical behavior of an AZ31 magnesium alloy processed by high-pressure torsion (HPT) was evaluated by tensile testing from room temperature up to 473 K at strain rates between 10-5 – 10-2 s-1. Samples tested at room temperature and at high strain rates at 373 K failed without any plastic deformation. However, significant ductility, with elongations larger than 200%, was observed at 423 K and 473 K and at low strain rates at 373 K. The high elongations are attributed to a pronounced strain hardening and a high strain rate sensitivity. The results agree with reports for a similar alloy processed by severe plastic deformation. However, the level of flow stress is lower and the strain rate sensitivity and the elongations are larger than observed in this alloy processed by conventional thermo-mechanical processing.


2005 ◽  
Vol 20 (11) ◽  
pp. 3072-3081 ◽  
Author(s):  
H. Li ◽  
A.H.W. Ngan ◽  
M.G. Wang

Using depth-sensing indentation with sub-nanometer displacement resolution, the plastic deformation of a range of materials, including a metallic glass, amorphous selenium, Ni3Al, pure Nb, Al, Cu, and Zn metals, and an Al-Mg alloy, has been investigated at room temperature. In amorphous selenium, even the sub-nanometer displacement resolution of the nanoindentation technique cannot reveal any strain burst during deformation at room temperature. In all other metals studied, what may appear to be smooth load-displacement curves at macroscopic scale during indentation deformation in fact turn out to consist of a continuous series of random bursts of the nanometer scale. The occurrence probability of the bursts is found to decrease at increasing burst size. In all of the crystalline metals and alloys studied, the size distribution of the strain bursts seems to follow an exponential law with a characteristic length scale. The absence of the self-organized critical behavior is likely a result of the small size of the strained volume in the nanoindentation situation, which gives rise to a constraint of a characteristic strain. In the metallic glass sample, due to the limited range of the burst sizes encountered, whether the deformation bursts follow an exponential or a power-law behavior corresponding to self-organized criticality is inconclusive. From a theoretical viewpoint based on the Shannon entropy, the exponential distribution is the most likely distribution at a given mean burst size, and this is thought to be the reason for its occurrence in different materials.


2021 ◽  
Vol 250 ◽  
pp. 05005
Author(s):  
Taisei Sakai ◽  
Hiroyuki Yamada ◽  
Nagahisa Ogasawara ◽  
Muneyuki Kokudai ◽  
Tsutomu Fukui

Steel is widely used as a constituent material for various structures such as automobiles and ships. To perform high precision analysis including high strain rate behavior, an understanding for the strain rate dependence of material strength becomes very important. The purpose of this study is to evaluate the strain rate dependence of material strength with rolled steels for welded structure, JIS SM490B (ASTM E). We investigated the deformation characteristics at room temperature by performing compression tests at a wide range of strain rates and applied the obtained experimental results to the material constitutive model using an optimization method of Nelder-Mead method. The quasi-static tests were conducted using a universal testing machine at the strain rate of 10-3, 10-2 and 10-1 s-1. The impact test was conducted using a split Hopkinson pressure bar apparatus at the strain rate of approximately 103 s-1. As the results of the compression tests, it was confirmed that SM490B has a positive strain rate dependence of material strength. The Cowper-Symonds constitutive model showed good agreement with the experimental results up to the strain of 20%. However, the error became larger between experimental results and CS approximation as the strain increases to 20% or more.


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