Superconducting yba2cu3o7‐x Thin Film on Metal Substrate by Chemical Vapor Deposition Process.

1989 ◽  
Vol 169 ◽  
Author(s):  
T. Yamaguchi ◽  
S. Aoki ◽  
N. Sadakata ◽  
O. Kohno

AbstractSuperconducting YBa2Cu307_x thin films were prepared by chemical vapor deposition using beta‐diketonate chelates on various oxide substrates and metal substrates. According to X‐ray diffraction patterns, the existence of a well‐oriented orthorhombic YBagCUgO^x structure has been confirmed in all specimens. The temperature of complete superconducting transition were observed at 89K on single‐crystalline oxide substrate, and 84K on metal substrate. Reduced critical current density of the film on single‐crystalline substrate in magnetic fields up to 600mT at 77K remained one or two order of magnitude higher than that of the film on metal substrate.

1995 ◽  
Vol 388 ◽  
Author(s):  
John Kouvetakis ◽  
Renu SharmA ◽  
B. L. Ramakrisna ◽  
Jeff Drucker ◽  
Paul Seidler

AbstractWe demonstrate a novel technique for in situ observation of the chemical vapor deposition of high purity gold using ethyl(trimethylphosphine)gold(I). an environmental transmission electron microscope with 3.8 eV resolution was used to observe and compare the growth of the material with or without electron beam irradiation (120 keV) with Si (100) substrate temperatures ranging from 125-200 °C. Typical precursor pressures of 10-4 Torr and E-beam irradiation resulted in rapid growth of virtually continuous gold films. thermal deposition without the beam resulted in low nucleation densities, low deposition rates, and island-like growth. Images and diffraction patterns acquired during the deposition process indicated polycrystalline gold and elemental analysis at the nanometer scale showed that the films had excellent chemical purity. atomic force microscopy was also used to investigate the three dimensional morphology of the materials. the most notable result of the deposition process is the dramatic enhancement of the growth rate due to the beam irradiation.


Nanoscale ◽  
2017 ◽  
Vol 9 (40) ◽  
pp. 15416-15422 ◽  
Author(s):  
Kai Zhang ◽  
Jia Ding ◽  
Zheng Lou ◽  
Ruiqing Chai ◽  
Mianzeng Zhong ◽  
...  

Heterostructured ZnS/InP nanowires, composed of single-crystalline ZnS nanowires coated with a layer of InP shell, were synthesized via a one-step chemical vapor deposition process.


2000 ◽  
Vol 15 (8) ◽  
pp. 1702-1708
Author(s):  
Ruichao Zhang ◽  
Ren Xu

A novel two-step metalorganic chemical vapor deposition process was used in this study to prepare Sr1−xBaxNb2O6 (SBN) thin films. Two thin layers of single-phase SrNb2O6 and BaNb2O6 were deposited alternately on a silicon substrate, and the solid solution of SBN was obtained by high-temperature annealing. The stoichiometry control of the SrNb2O6 and the BaNb2O6 thin films was achieved through deposition process control, according to the evaporation characteristics of double metal alkoxide. The evaporation behavior of double metal alkoxide precursors SrNb2(1-OC4H9)12 and BaNb2(1-OC4H9)12 was studied, and the results were compared with the evaporation of single alkoxide Nb(1-OC4H9)5.


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