High Resolution Electron Microscopic Study of the Growth of Denser Phases on Zeolite Y and Zeolite L.

1987 ◽  
Vol 111 ◽  
Author(s):  
H. W. Zandbergen
Keyword(s):  
High Resolution ◽  
Local Structure ◽  
Zeolite Y ◽  
High Resolution Electron Microscopy ◽  
Electron Microscopic ◽  
Detailed Characterization ◽  
Zeolite L ◽  
Resolution Electron ◽  
Materials Research

AbstractHigh resolution electron microscopy (HREM) is a powerful tool in materials research. This is especially true in the study of zeolites because most of the questions concerning the properties of zeolites require a detailed characterization of the local structure [1]. The potential of HREM is illustrated with studies on the growth of denser phases on Zeolite Y and Zeolite L.

Defects and Metal Particles in Zeolites Studied with High Resolution Electron Microscopy

1990 ◽  
Vol 183 ◽  
Author(s):  
H. W. Zandbergen ◽  
D. van Dyck
Keyword(s):  
Electron Microscopy ◽  
High Resolution ◽  
Structural Changes ◽  
Zeolite Y ◽  
High Resolution Electron Microscopy ◽  
Metal Particles ◽  
Zeolite L ◽  
Zeolite Β ◽  
Resolution Electron

AbstractA number of examples of high resolution electron microscopy on defects and metal particles in zeolites is given: defects in Zeolite Y and Zeolite β, metal particles in ZSM-5, and structural changes due to reactions in Zeolite L and Zeolite Y.

High-resolution electron microscopy of nanostructured materials

1995 ◽  
Vol 53 ◽  
pp. 172-173
Author(s):  
M. José-Yacamán
Keyword(s):  
Electron Microscopy ◽  
High Resolution ◽  
Grain Boundaries ◽  
Nanostructured Materials ◽  
High Resolution Electron Microscopy ◽  
Hrem Image ◽  
Small Particles ◽  
Resolution Electron ◽  
Nanophase Materials

Electron microscopy is a fundamental tool in materials characterization. In the case of nanostructured materials we are looking for features with a size in the nanometer range. Therefore often the conventional TEM techniques are not enough for characterization of nanophases. High Resolution Electron Microscopy (HREM), is a key technique in order to characterize those materials with a resolution of ~ 1.7A. High resolution studies of metallic nanostructured materials has been also reported in the literature. It is concluded that boundaries in nanophase materials are similar in structure to the regular grain boundaries. That work therefore did not confirm the early hipothesis on the field that grain boundaries in nanostructured materials have a special behavior. We will show in this paper that by a combination of HREM image processing, and image calculations, it is possible to prove that small particles and coalesced grains have a significant surface roughness, as well as large internal strain.

HRTEM simulation of interfacial structure in amorphous multilayers

1989 ◽  
Vol 47 ◽  
pp. 466-467
Author(s):  
Margaret L. Sattler ◽  
Michael A. O'Keefe
Keyword(s):  
Electron Microscopy ◽  
High Resolution ◽  
Cross Section ◽  
High Resolution Electron Microscopy ◽  
Interfacial Structure ◽  
Multilayer Sample ◽  
Resolution Electron ◽  
Multilayered Materials ◽  
Simulated Images

Multilayered materials have been fabricated with such high perfection that individual layers having two atoms deep are possible. Characterization of the interfaces between these multilayers is achieved by high resolution electron microscopy and Figure 1a shows the cross-section of one type of multilayer. The production of such an image with atomically smooth interfaces depends upon certain factors which are not always reliable. For example, diffusion at the interface may produce complex interlayers which are important to the properties of the multilayers but which are difficult to observe. Similarly, anomalous conditions of imaging or of fabrication may occur which produce images having similar traits as the diffusion case above, e.g., imaging on a tilted/bent multilayer sample (Figure 1b) or deposition upon an unaligned substrate (Figure 1c). It is the purpose of this study to simulate the image of the perfect multilayer interface and to compare with simulated images having these anomalies.

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