Mechanical properties of Bombyx mori silkworm silk subjected to microwave radiation

2014 ◽  
Vol 29 (7) ◽  
pp. 833-842 ◽  
Author(s):  
Emily J. Reed ◽  
Christopher Viney

Abstract

2011 ◽  
Vol 1301 ◽  
Author(s):  
Emily J. Reed ◽  
Christopher Viney

ABSTRACTWe have developed a reproducible protocol for studying the effect of microwave radiation on the mechanical behavior of Bombyx mori cocoon silk. In the course of this work, we identified multiple improvements that can be made to ASTM F 1317-98, the standard according to which microwave oven power output is calibrated.Exposure to microwaves does not significantly affect mechanical properties of silkworm silk, if samples are kept in a desiccator after degumming (or after degumming and microwaving) and prior to testing in a dry environment. This finding contrasts with previous work in which samples were not kept in a desiccator, and were tested in a relatively humid environment.Because the effect of microwave radiation on the mechanical behavior of silk is sensitive to ambient moisture, meaningful comparison or pooling of test results acquired in different laboratories is contingent on standardization of both the sample storage environment and the environment in which samples are tested. Interpretation of the extensive existing literature on silk mechanical properties must take account of the reality that the sample storage and testing environments are not standardized and are usually not reported.


2012 ◽  
Vol 1465 ◽  
Author(s):  
Emily J. Reed ◽  
Christopher Viney

ABSTRACTIt has been reported [1] that microwave radiation can enhance many of the mechanical properties of Bombyx mori silkworm cocoon silk, as measured in constant strain rate tensile tests to failure and in stress relaxation tests. The consequences of microwave radiation will affect decisions about the use of silk in settings subjected to significant microwave exposure – for example, as a reinforcing fiber in an epoxy matrix composite that may be microwave cured, or as a component in aircraft radomes.There are two possible mechanisms by which microwave radiation may affect a material [2]: (i) the radiation may enable chemical and/or microstructural changes – and therefore property changes – in the same way that conventional heating would, or (ii) the high heating rates that are achievable by microwaving may selectively favor changes that would be masked under conventional conditions, where heating rates are low enough to give preference to changes that have a lower activation energy. Here we explore the former possibility for silk.We characterized several mechanical properties of degummed and subsequently annealed B. mori silk, and compared them to the corresponding properties of degummed B. mori silk that was not annealed. The annealing treatment was carried out at 140 °C for 7 hours (conditions that optimally increased crystal size in an unrelated study of B. mori silk [3]), and then the fibers were allowed to cool gradually to room temperature over the course of an hour. Comparison of mechanical properties revealed no differences between the materials that we tested. Thus, for annealed silk, we do not observe the enhancements that can be achieved by microwaving. We conclude that in cases where microwaving affects the properties of silk, those changes are not a simple consequence of annealing by the microwaves.


2019 ◽  
Vol 181 ◽  
pp. 108077 ◽  
Author(s):  
Shaoyong Chen ◽  
Mingyue Liu ◽  
Huiming Huang ◽  
Lan Cheng ◽  
Hong-Ping Zhao

2019 ◽  
Vol 11 (1) ◽  
Author(s):  
Suna Fan ◽  
Xiaoting Zheng ◽  
Qi Zhan ◽  
Huihui Zhang ◽  
Huili Shao ◽  
...  

Abstract Fluorescent silk is fundamentally important for the development of future tissue engineering scaffolds. Despite great progress in the preparation of a variety of colored silks, fluorescent silk with enhanced mechanical properties has yet to be explored. In this study, we report on the fabrication of intrinsically super-strong fluorescent silk by feeding Bombyx mori silkworm carbon nanodots (CNDs). The CNDs were incorporated into silk fibroin, hindering the conformation transformation, confining crystallization, and inducing orientation of mesophase. The resultant silk exhibited super-strong mechanical properties with breaking strength of 521.9 ± 82.7 MPa and breaking elongation of 19.2 ± 4.3%, improvements of 55.1% and 53.6%, respectively, in comparison with regular silk. The CNDs-reinforced silk displayed intrinsic blue fluorescence when exposed to 405 nm laser and exhibited no cytotoxic effect on cells, suggesting that multi-functional silks would be potentially useful in bioimaging and other applications.


2013 ◽  
Vol 28 (17) ◽  
pp. 2509-2519 ◽  
Author(s):  
Nazim Mahmutyazicioglu ◽  
Onder Albayrak ◽  
Mehmet Ipekoglu ◽  
Sabri Altintas

Abstract


2017 ◽  
Vol 7 (3) ◽  
pp. 595-600 ◽  
Author(s):  
Baoming Wang ◽  
M. A. Haque ◽  
Vikas Tomar ◽  
Khalid Hattar

Abstract


2012 ◽  
Vol 27 (19) ◽  
pp. 2551-2560 ◽  
Author(s):  
Gaylord Guillonneau ◽  
Guillaume Kermouche ◽  
Sandrine Bec ◽  
Jean-Luc Loubet

Abstract


2017 ◽  
Vol 32 (19) ◽  
pp. 3712-3722 ◽  
Author(s):  
Yushi Chen ◽  
Guohua Wu ◽  
Wencai Liu ◽  
Liang Zhang ◽  
Haohao Zhang ◽  
...  

Abstract


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