Stereophotogrammetric Investigation of Overload and Cyclic Fatigue Fracture Surface Morphologies in a Zr–Ti–Ni–Cu–Be Bulk Metallic Glass

2000 ◽  
Vol 15 (4) ◽  
pp. 898-903 ◽  
Author(s):  
A. Tatschl ◽  
C. J. Gilbert ◽  
V. Schroeder ◽  
R. Pippan ◽  
R. O. Ritchie

Fracture surfaces of a recently developed Zr41.2Ti13.8Cu12.5Ni10.0Be22.5 (at.%) bulk metallic glass were investigated using a three-dimensional surface reconstruction technique. Stereoscopic scanning electron microscopy of both fatigue and overload fracture surfaces permitted the creation of digital elevation models that were used to quantify important fracture surface features. Characterization of the surfaces revealed striations of nearly constant spacing on fatigue surfaces and a vein morphology characteristic in amorphous metals on the overload fracture surfaces. Additionally, at the onset of critical failure, crack-tip openings of ˜16 μm were observed that were consistent with measured values of fracture toughness. Interestingly, at the onset of fracture, deformation was confined to one side of the fracture plane, possibly because of the asymmetric emission of shear bands from the crack tip, consistent with the highly inhomogeneous nature of deformation in this alloy.

2005 ◽  
Vol 46 (12) ◽  
pp. 2870-2874 ◽  
Author(s):  
Kyosuke Yoshimi ◽  
Hidemi Kato ◽  
Junji Saida ◽  
Akihisa Inoue

1993 ◽  
Vol 8 (10) ◽  
pp. 2543-2553 ◽  
Author(s):  
D.M. Kulawansa ◽  
J.T. Dickinson ◽  
S.C. Langford ◽  
Yoshihisa Watanabe

We report scanning tunneling microscope observations of fracture surfaces formed during catastrophic crack growth in three metallic glasses: Ni56Cr18Si22B4, Co69Fe4Ni1Mo2B12Si12, and Fe78B13Si9. Macroscopically, the first two glasses fail along a slip band formed during loading and display a characteristic, μm-scale pattern of vein-like ridges; in contrast, Fe78B13Si9 displays little slip prior to fracture, and its fracture surface shows a μm-scale chevron pattern of steps. STM observations of fracture surfaces of all three materials show nm-scale grooves. The grooves in Co69Fe4Ni1Mo2B12Si12 are especially prominent and display stepped edges which we attribute to the intersection of shear bands with the surface. STM observations of the vein-like features on Ni56Cr18Si22B4 also show stepped edges. We attribute the vein features to the interaction of adjacent crack fingers in which the material between adjacent fingers fails in plane stress. The origin of the grooves is uncertain, but may be due to other shear instabilities along crack fingers.


Nanomaterials ◽  
2021 ◽  
Vol 11 (7) ◽  
pp. 1670
Author(s):  
Abhilash Gunti ◽  
Parijat Pallab Jana ◽  
Min-Ha Lee ◽  
Jayanta Das

The effect of cold rolling on the evolution of hardness (H) and Young’s modulus (E) on the rolling-width (RW), normal-rolling (NR), and normal-width (NW) planes in Zr41.2Ti13.8Cu12.5Ni10Be22.5 (Vitreloy 1) bulk metallic glass (BMG) was investigated systematically using nanoindentation at peak loads in the range of 50 mN–500 mN. The hardness at specimen surface varied with cold rolling percentage (%) and the variation is similar on RW and NR planes at all the different peak loads, whereas the same is insignificant for the core region of the specimen on the NW plane. Three-dimensional (3D) optical surface profilometry studies on the NR plane suggest that the shear band spacing decreases and shear band offset height increases with the increase of cold rolling extent. Meanwhile, the number of the pop-in events during loading for all the planes reduces with the increase of cold rolling extent pointing to more homogeneous deformation upon rolling. Calorimetric studies were performed to correlate the net free volume content and hardness in the differently cold rolled specimens.


2008 ◽  
Vol 23 (1) ◽  
pp. 6-12 ◽  
Author(s):  
K.B. Kim ◽  
J. Das ◽  
M.H. Lee ◽  
S. Yi ◽  
E. Fleury ◽  
...  

We report a novel finding of slither propagation of shear bands on the fracture surface of a Cu47.5Zr47.5Al5 bulk metallic glass (BMG). The nanoscale heterogeneities in the as-cast state are aggregated along shear bands with irregular morphology. Such heterogeneities create a fluctuating stress field during shear band propagation leading to a slither propagation mode. The slither propagation of 10 to 15 nm wide shear bands is effective to improve both the plasticity and the “work-hardening-like” behavior of BMGs if the size, the morphology, and the elastic properties of the heterogeneities are intimately intercalated during solidification.


2016 ◽  
Vol 264 (3) ◽  
pp. 304-310 ◽  
Author(s):  
A.H. HUNTER ◽  
V. ARAULLO-PETERS ◽  
M. GIBBONS ◽  
O.D. RESTREPO ◽  
S.R. NIEZGODA ◽  
...  

Author(s):  
Vasily Astanin ◽  
Dmitry Gunderov ◽  
Zhi Qiang Ren ◽  
Ruslan Valiev ◽  
Jing Tao Wang

2003 ◽  
Vol 18 (9) ◽  
pp. 2039-2049 ◽  
Author(s):  
Jun Lu ◽  
Guruswami Ravichandran

An experimental study of the inelastic deformation of bulk metallic glass Zr41.2Ti13.8Cu12.5Ni10Be22.5 under multiaxial compression using a confining sleeve technique is presented. In contrast to the catastrophic shear failure (brittle) in uniaxial compression, the metallic glass exhibited large inelastic deformation of more than 10% under confinement, demonstrating the nature of ductile deformation under constrained conditions in spite of the long-range disordered characteristic of the material. It was found that the metallic glass followed a pressure (p) dependent Tresca criterion τ = τ0 + βp, and the coefficient of the pressure dependence β was 0.17. Multiple parallel shear bands oriented at 45° to the loading direction were observed on the surfaces of the deformed specimens and were responsible for the overall inelastic deformation.


2008 ◽  
Vol 496 (1-2) ◽  
pp. 285-290 ◽  
Author(s):  
L. He ◽  
M.B. Zhong ◽  
Z.H. Han ◽  
Q. Zhao ◽  
F. Jiang ◽  
...  

2019 ◽  
Vol 26 (08) ◽  
pp. 1950037
Author(s):  
BO SHI ◽  
SHIYU LUAN ◽  
PEIPENG JIN

Nanoscale dimples and periodic corrugations are observed on the fracture surface of Zr-based bulk metallic glass composite (BMGC). The nanoscale periodic corrugations display a curved shape, which is different from that observed in previous works. In addition, the crystallization behavior of [Formula: see text][Formula: see text][Formula: see text][Formula: see text] BMG was investigated. The second crystallization event of Zr-Cu-Ni-Al BMG can be controlled by annealing or tuning cooling rate. The in situ Zr-based BMGC was prepared via lowering cooling rate. The Zr-based BMGC displays completely brittleness.


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