Degradation profiles of silk textiles in diverse environments: Synchrotron based infrared micro-spectroscopy analysis

MRS Advances ◽  
2017 ◽  
Vol 2 (63) ◽  
pp. 3939-3949 ◽  
Author(s):  
Zhanyun Zhu ◽  
Nicole Tse ◽  
Petronella Nel ◽  
Mark Tobin

Abstract:In this paper, synchrotron based infrared micro-spectroscopy was utilized to describe the degradation profile of fibroin contained in silk textiles (Bombyx mori). The spatial distributions of deterioration effects in silk samples artificially aged at an assortment of conditions (thermal, hydrolytic and ultraviolet) were distinctly visualised and in accordance with the findings from conventional infrared spectroscopy in references. Further this method was applied on a historic sample from a private collection in Melbourne, and presented consistent results. This established synchrotron IR chemical mapping method could enable museum professionals to better understand the preservation state of historic silk and make informed decisions for conservation.

2020 ◽  
Vol 2020 ◽  
pp. 1-9
Author(s):  
Tiannv Shi ◽  
Yongmei Guan ◽  
Lihua Chen ◽  
Shiyu Huang ◽  
Weifeng Zhu ◽  
...  

Product quality control is a prerequisite for ensuring safety, effectiveness, and stability. However, because of the different strain species and fermentation processes, there was a significant difference in quality. As a result, they should be clearly distinguished in clinical use. Among them, the fermentation process is critical to achieving consistent product quality. This study aims to introduce near-infrared spectroscopy analysis technology into the production process of fermented Cordyceps powder, including strain culture, strain passage, strain fermentation, strain filtration, strain drying, strain pulverizing, and strain mixing. First, high performance liquid chromatography (HPLC) was used to measure the total nucleosides content in the production process of 30 batches of fermented Cordyceps powder, including uracil, uridine, adenine, guanosine, adenosine, and the process stability and interbatch consistency were analyzed with traditional Chinese medicine (TCM) fingerprinting, followed by the near-infrared spectroscopy (NIRS) combined with partial least squares regression (PLSR) to establish a quantitative analysis model of total nucleosides for online process monitoring of fermented Cordyceps powder preparation products. The model parameters indicate that the established model with good robustness and high measurement precision. It further clarifies that the model can be used for online process monitoring of fermented Cordyceps powder preparation products.


2021 ◽  
Vol 35 (8) ◽  
Author(s):  
Stefan Graaf ◽  
Hubert B. Vonhof ◽  
Elan J. Levy ◽  
Monika Markowska ◽  
Gerald H. Haug

2016 ◽  
Vol 19 (2) ◽  
pp. 145-154 ◽  
Author(s):  
Mun Fei Yam ◽  
Yung Sing Ch’ng ◽  
Chu Shan Tan ◽  
Yean Chun Loh ◽  
Mariam Ahmad ◽  
...  

1993 ◽  
Vol 63 (1-4) ◽  
pp. 236-239 ◽  
Author(s):  
B. Garrido ◽  
J.A. Moreno ◽  
J. Samitier ◽  
J.R. Morante

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