Analysis of Delamination Propagation in the Composite Layer of Metal-to-Composite Stepped-Lap Joints

Author(s):  
MM Ratwani ◽  
H-P Kan
2019 ◽  
Author(s):  
Xiaohan Wu ◽  
Juliette Billaud ◽  
Iwan Jerjen ◽  
Federica Marone ◽  
Yuya Ishihara ◽  
...  

<div> <div> <div> <p>All-solid-state batteries are considered as attractive options for next-generation energy storage owing to the favourable properties (unit transference number and thermal stabilities) of solid electrolytes. However, there are also serious concerns about mechanical deformation of solid electrolytes leading to the degradation of the battery performance. Therefore, understanding the mechanism underlying the electro-mechanical properties in SSBs are essentially important. Here, we show three-dimensional and time-resolved measurements of an all-solid-state cell using synchrotron radiation x-ray tomographic microscopy. We could clearly observe the gradient of the electrochemical reaction and the morphological evolution in the composite layer. Volume expansion/compression of the active material (Sn) was strongly oriented along the thickness of the electrode. While this results in significant deformation (cracking) in the solid electrolyte region, we also find organized cracking patterns depending on the particle size and their arrangements. This study based on operando visualization therefore opens the door towards rational design of particles and electrode morphology for all-solid-state batteries. </p> </div> </div> </div>


2017 ◽  
Vol 68 (5) ◽  
pp. 928-932
Author(s):  
Agripina Zaharia ◽  
Viorica Ghisman Plescan ◽  
Elena Maria Anghel ◽  
Viorica Musat

The purpose of this work is to induce biomimetic remineralization of acid etched coronal human dentine in artificial saliva (AS) under agarose (A) hydrogel or chitosan (CS)-A hydrogel action. The investigations focused on the morphology, chemical composition and crystalline structure of the new remineralized layers grown onto the etched dentinal surface (R) using scanning electron microscopy coupled with energy dispersive X-ray spectrometry and micro-Raman spectroscopy. Experimental results showed that remineralized layers grown in the presence of A or CS-A hydrogels consist in B-type Ca-deficient hydroxyapatite (HAP). After 7 days treatment into artificial saliva under agarose hydrogel, nanorod-like extrafibrilar HAP crystals randomly self-assembled in a discontinuous layer were formed, while in presence of chitosan-agarose hydrogel a continuous compact CS-HAP composite layer was obtained. The new biomimetic layer (A-CS4) formed after 4 days on dentine surface under A-CS hydrogel has higher crystallinity. Longer exposed (7 days) dentine in the presence of agarose hydrogel shows a higher mineral-to-collagen ratio (A7). Since dentine mineralization increases, the collagen quality factor decreases in succession A-CS4]R]A7. Results show a benefic effect of chitosan on remineralization of etched dentine.


1999 ◽  
Vol 17 (2) ◽  
pp. 319-325 ◽  
Author(s):  
Koichi OSAWA ◽  
Tsuyoshi SHIOZAKI ◽  
Toshiaki URABE ◽  
Akihide YOSHITAKE ◽  
Takanobu SAITO ◽  
...  

Open Physics ◽  
2019 ◽  
Vol 17 (1) ◽  
pp. 320-328
Author(s):  
Delin Sun ◽  
Minggao Zhu

Abstract In this paper, the energy dissipation in a bolted lap joint is studied using a continuum microslip model. Five contact pressure distributions compliant with the power law are considered, and all of them have equal pretension forces. The effects of different pressure distributions on the interface stick-slip transitions and hysteretic characteristics are presented. The calculation formulation of the energy dissipation is introduced. The energy dissipation results are plotted on linear and log-log coordinates to investigate the effect of the pressure distribution on the energy distribution. It is shown that the energy dissipations of the lap joints are related to the minimum pressure in the overlapped area, the size of the contact area and the value of the power exponent. The work provides a theoretical basis for further effective use of the joint energy dissipation.


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