Practice for Conducting an Interlaboratory Study to Determine Precision Estimates for a Fire Test Method with Fewer Than Six Participating Laboratories

2015 ◽  
Author(s):  
Keyword(s):  
Fire Test ◽  
Test Method ◽  
Interlaboratory Study

Research on Fire Test Method of High Pressure Hydrogen Storage Cylinders for Transportation

2021 ◽  
Author(s):  
Jun Li ◽  
Xiang Li ◽  
Jiepu Li ◽  
Baodi Zhao ◽  
Chunlin Gu ◽  
...  
Keyword(s):  
Hydrogen Storage ◽  
Fire Test ◽  
Test Methods ◽  
Test Method ◽  
Working Pressure ◽  
Industry Chain ◽  
Gas Cylinder ◽  
Fire Condition ◽  
Chinese Standard ◽  
Gas Cylinders

Abstract As important equipment in the entire hydrogen industry chain, composite hydrogen storage cylinders for transportation have developed rapidly in recent years. The fire test is used to verify the explosion resistance of gas cylinders under specified fire conditions. Compared to steel gas cylinder, composite gas cylinder is more dangerous in the fire condition. The wound layer, as the main pressure-bearing structure of the composite hydrogen storage cylinder, is inflammable. In the case of fire, the mechanical properties of the cylinder will degrade quickly due to the high temperature. If the gas inside the cylinder cannot be discharged in time, the cylinder explosion will occur. Currently, some relevant standards or standard drafts have been drawn up by the international organizations, which are useful for formulating Chinese standard for hydrogen storage cylinders for transportation. The applicable scope of the standards was discussed in this paper, such as composite cylinder type, working pressure, nominal volume and design life, etc. The fire test methods of composite gas cylinders in various standards were compared and analyzed, such as experiment method, cylinder placement method, cylinder filling requirements, fuel selection, fire source setting, temperature measurement requirements, and qualified indicators, etc. Finally, the challenges for development of composite hydrogen storage cylinders and compressed hydrogen storage systems in China were proposed.

Precision of the air void characteristics measurement by ASTM C 457: results of an interlaboratory test program

1996 ◽  
Vol 23 (5) ◽  
pp. 1118-1128 ◽  
Author(s):  
François Saucier ◽  
Richard Pleau ◽  
Daniel Vézina
Keyword(s):  
Test Method ◽  
Interlaboratory Study ◽  
Hardened Concrete ◽  
Probability Of Error ◽  
Air Content ◽  
Spacing Factor ◽  
Interlaboratory Test ◽  
Void System ◽  
Concrete Production ◽  
Air Void

Since 1993, the Quebec Department of Transportation requires all its concrete suppliers to demonstrate that their concrete satisfies the requirements of the CSA A23.1 standard as regards the maximum spacing factor of the air void system. This new requirement raises questions about the reproducibility of the ASTM C 457 test method. An interlaboratory study was carried out to verify if the variability of the test method is sufficiently low to allow reliable decisions on the acceptance or rejection of in-place hardened concrete. A total of 18 operators from 13 different laboratories microscopically examined the six concrete slabs used for the study. It is concluded that the average reproducibility coefficient of variation is 14.4% for the total air content measurement and 14.2% for the spacing factor measurement. Considering these results, the probability that the measured value of the spacing factor exceeds the mandatory limit of 230 μm on a concrete production containing an air void system with a spacing factor of 170 μm (the target value proposed in the CSA A23.1 M-94 standard) is less than 0.7% (a probability of error of about 1%, 5%, or 10% is typical of most quality control test methods). Key words: concrete, air content, air void measurement, spacing factor, ASTM C 457 standard, interlaboratory study, freeze–thaw durability.

Sign in / Sign up

Export Citation Format

Share Document