Precision of the air void characteristics measurement by ASTM C 457: results of an interlaboratory test program

Since 1993, the Quebec Department of Transportation requires all its concrete suppliers to demonstrate that their concrete satisfies the requirements of the CSA A23.1 standard as regards the maximum spacing factor of the air void system. This new requirement raises questions about the reproducibility of the ASTM C 457 test method. An interlaboratory study was carried out to verify if the variability of the test method is sufficiently low to allow reliable decisions on the acceptance or rejection of in-place hardened concrete. A total of 18 operators from 13 different laboratories microscopically examined the six concrete slabs used for the study. It is concluded that the average reproducibility coefficient of variation is 14.4% for the total air content measurement and 14.2% for the spacing factor measurement. Considering these results, the probability that the measured value of the spacing factor exceeds the mandatory limit of 230 μm on a concrete production containing an air void system with a spacing factor of 170 μm (the target value proposed in the CSA A23.1 M-94 standard) is less than 0.7% (a probability of error of about 1%, 5%, or 10% is typical of most quality control test methods). Key words: concrete, air content, air void measurement, spacing factor, ASTM C 457 standard, interlaboratory study, freeze–thaw durability.