INVESTIGATING THE EFFECT OF NANO SILICA ON THE MECHANICAL PROPERTIES OF HARDENED CEMENT PASTE

Author(s):  
Sameer Hamoush ◽  
Miguel Picornell ◽  
Taher Abu-Lebdeh

This study investigated the compressive strength of hardened cement paste and the formation of calcium silicate hydrate (C-S-H) with the addition of nano silica (SiO2). Through this search, the development of the concretes strength was determined to better understand the process of cement hydration. Compressive strength testing was performed using MTS and Forney testing machines to determine stress-strain curves and elastic modulus of materials. The hydration process and formation of C-S-H and calcium hydroxide (CH) was examined using Scanning Electron Microscopy (SEM) and Fourier Transform Infrared Spectroscopy (FTIR). This study also incorporates the use of vacuum curing, in comparison to that of the traditional water curing method. Results indicate an increase in compressive strength using 1%, 3% and 5% of nano silica to cement replacement by volume in comparison to the control mix (without nano silica). The optimum cement replacement to yield maximum strength was of the 1% nano silica content. The formation of C-S-H increases significantly during the early testing days which correspond with the drastic increase in compressive strength. The hydration process continues to increase throughout the 56 day trails at a moderate rate. The traditional water curing method proves to be more efficient and beneficial than of the vacuum curing method. However, vacuum cured results showed only about a 5% reduction in strength after 56 day tests in comparison to the water curing method.

2019 ◽  
Vol 39 (3) ◽  
pp. 248-260 ◽  
Author(s):  
Taher Abu-Lebdeh ◽  
Relly Victoria Virgil Petrescu ◽  
Moayyad Al-Nasra ◽  
Florian Ion Tiberiu Petrescu

This study investigated the influence of adding nano silica (SiO2) on the cement hydration process, particularly on the formation of calcium silicate hydrate (C-S-H) at different stages of hydration. The study investigated the effect of adding nano-silica on the mechanical properties of the hardened cement corresponding to the formation of C-S-H during the hydration process of a cement paste. Specimens made up of four different percentage of nano silica (0%, 1%, 3% and 5%) were tested at different stages of hydration ranging from 3 to 56 days. The effect of nano-silica on the compressive strength, stressstrain, and elastic modulus of nano-cement was examined using MTS and Forney testing machines. The signature phase and formation of C-S-H and calcium hydroxide (CH) were monitored using Fourier Transform Infrared Spectroscopy (FTIR) and Scanning Electron Microscopy (SEM). The study also investigated the effect of curing method (vacuum and water curing) on the strength development. The experimental results show that the formation of calcium silicate hydrate (C-S-H) increases significantly during the early stages of hydration which correspond to the drastic increase in compressive strength. The formation of C-S-H continues to increase throughout the 56 days but at a moderate rate. The results reveal that 1% of nano silica by volume of cement is the optimum ratio that yields the maximum strength. The results also indicated that the strength of the traditional water cured specimens were higher than that of vacuum cured specimens.


2021 ◽  
Vol 2109 (1) ◽  
pp. 012019
Author(s):  
Xuelian Yuan ◽  
Jie Hu

Abstract Through using cube resisting compression test, fracture properties and micro-structure, the mechanical properties of high volume ground slag concrete under low temperature are studied in this paper. The results show that low temperature can improve the compressive strength of high volume ground slag concrete. And strength increased with the decreased of temperature. Low temperature can also improve the fracture energy and fracture toughness. Not only can ground slag reduce the content of calcium hydroxide in hardened cement paste, but ground slag can improve the compactness of hardened cement paste, reduce porosity and improve the strength of the interface.


1984 ◽  
Vol 42 ◽  
Author(s):  
Huang Yiun-Yuan ◽  
Ding Wei ◽  
Lu Ping

AbstractThe pore-structure strongly influences the carpressive strength of hardened cement paste (hcp) and other porous materials, as well as other mechanical properties. The simplest but most currently used expression representing the relationship between the pore-structure and compressive strength is fram Balshin: σ = σ0 (l-P)A, in which only the total porosity P is involved as a single parameter and σ0 and A are empirical constants. The influence of pore size distribution and pore shapes etc. are not considered.The authors introduce second parameter w - the factor of relative specific surface area of the pores other than the total porosity P into consideration and a new expression is proposed:σc=K11-p/1+2p(K2(1-p))K3w+K4 all the constants K1 - K4 can be determined experimentally. By using of this expression the new information relating the influence of pore-structure on the caopressive strength of hcp can be predicted.


2011 ◽  
Vol 250-253 ◽  
pp. 182-187 ◽  
Author(s):  
Wei Juan Guo ◽  
Gao Xiang Du ◽  
Qiang Xue ◽  
Jing Hui Liao

The compressive strength of ultrafine white cement samples at three ages: 3, 7 and 28 days and micro appearance of hydrates were tested. The influence of the usage of superplasticizers on the compressive strength of ultrafine white cement paste and hydrates were investigated. The results indicated that the 28d compressive strength of ultrafine white cement with 3% naphthalene based superplasticizers added was 92.9 MPa, 22.9% of that of pure ultrafine white cements (75.6 MPa). The addition of superplasticizers was beneficial to the density of white cement paste. A large number of hydrates (AFt, C-H-S, and so on) were generated in the capillary pores, which would improve the structure of capillary pores of hardened cement paste, increase the density and strength.


1994 ◽  
Vol 370 ◽  
Author(s):  
Asif Ahmed ◽  
Leslie Struble

AbstractMechanical properties of any material, including hardened cement paste, are assumed to be controlled by its microstructure. An attempt has been made here to establish a link between bulk fracture parameters of hardened cement paste and its microstructure. Paste microstructure has been varied by changing the initial w/c ratio, curing time and curing temperature, and by addition of chemicals to change the calcium hydroxide morphology. It has been found that, like compressive strength, fracture parameters depend directly on porosity. Contrary to our initial hypothesis, CH morphology was found to have no effect on the fracture parameters.


2021 ◽  
Vol 267 ◽  
pp. 121724
Author(s):  
Min Liu ◽  
Shuxian Hong ◽  
Yanshuai Wang ◽  
Jinrui Zhang ◽  
Dongshuai Hou ◽  
...  

2016 ◽  
Vol 683 ◽  
pp. 113-117 ◽  
Author(s):  
Alexander I. Kudyakov ◽  
Alexey B. Steshenko

The results of studies of modified hardened cement paste with glyoxal-containing additive are given in this article. The goal was to study the patterns of influence of crystalline glyoxal on compressive strength of hardened cement paste. Introduction of crystalline glyoxal in the amount of 0.01-0.05% by weight of cement in the cement paste enables the increase in the compressive strength of hardened cement paste in 28 days by 7-8%. The studies have established that the introduction of crystalline glyoxal in the amount of 0.1-1% by weight of cement is inefficient; there is a decrease of the strength values in comparison with control samples. The results of microstructure investigation (of control samples and samples of the modified hardened cement paste) have shown that the introduction of crystalline glyoxal in the amount of 0.01-0.05% by weight of cement provides the structure of hardened cement paste that does not contain sedimentative pores and increases the quantity of hydroaluminate.


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