scholarly journals Spot size characterization of focused non-Gaussian X-ray laser beams

2010 ◽  
Vol 18 (26) ◽  
pp. 27836 ◽  
Author(s):  
J. Chalupský ◽  
J. Krzywinski ◽  
L. Juha ◽  
V. Hájková ◽  
J. Cihelka ◽  
...  
2010 ◽  
Vol 1 (MEDSI-6) ◽  
Author(s):  
M. Nicola ◽  
H. P. van der Kleij

For some beamlines, where the X-ray beam is focussed to less than 100 nm spot size, it is necessary to rotate the sample using very accurate rotary axes. The accuracy of these devices is defined in terms of radial, axial and tilt errors. At the Precision Engineering Laboratory of the ESRF, we are able to calibrate rotary stages and spindles in agreement with the ISO 230-7 and ASME B89.3.4 standards, in static mode (step by step, at given position increments) or in continuous motion. This type of measurement is possible through the use of non-contact capacitive sensors (with measuring resolution in the field of the nanometre) and reference spherical artefacts, working under controlled environmental conditions to minimize the influence of thermal instabilities. The setup includes a special granite stage with a gantry, supported by an active anti-vibration system. The presentation will illustrate the measurement principle and some examples of calibrations, including results obtained on a motorized air-bearing rotary stage for which the measured errors are about 20 nm.


2019 ◽  
Vol 966 ◽  
pp. 308-313
Author(s):  
M.P. Izaak ◽  
H. Sitompul ◽  
Wisnu Ari Adi ◽  
Yohanes Edi Gunanto

Synthesis and characterization of α-Fe2O3 nanoparticles were obtained from extraction of ilmenite iron sand with coprecipitation method and to obtain α-Fe2O3 nanoparticles, high energy milling (HEM) was used. Surface morphology and identification of the elements contained in the sample were analyzed using scanning electron microscope (SEM) and energy dispersive spectroscopy (EDS). For phase analysis and crystal structure, X-ray diffractometer (XRD) was used. Moreover a vibrating magnetometer sample (VSM) was used to characterize its magnetic properties, while tunneling electron microscopy (TEM) was used for particle size characterization. Ilmenite-type iron sand has a diverse particle shape with a size of more than 100 μm with ilmenite (FeTiO3) mineral content of about 64.7%. The results of extraction using coprecipitation method with sintering 750 °C, obtained hematite α-Fe2O3 material which has not been saturated to an external magnetic field of 1 tesla, the magnetic remanent value (Mr) is about 0.8 emu/g and the coercivity field value is Hc around 773 Oe. The average size of hematite α-Fe2O3 particles after being milled 50 hours is between 15-30 nm with a cube-like shape.


Clay Minerals ◽  
1998 ◽  
Vol 33 (3) ◽  
pp. 435-442 ◽  
Author(s):  
M. Dondi ◽  
B. Fabbri ◽  
G. Guarini

AbstractThe grain size of raw materials influences their behaviour during the technological process and affects many properties of building clay products. Over the last few years, brickworks have been technologically updated and grain size requirements have been modified to ensure good behaviour during shaping and drying. Therefore, the reference schemes used to assess the suitability of clays, such as the classic Winkler diagram, should be updated.For this purpose, the grain-size distribution of 350 clays currently used in ~240 Italian plants was determined by X-ray monitoring of gravity sedimentation. Raw materials are basically represented by silty clays and clayey silts, while bodies present a narrower grain-size range. With reference to the Winkler diagram, most of the Italian bodies fall within the field of ‘thin-walled hollow bricks’, with no significant differentiation among the various product types.In order to improve the grain-size characterization of bodies, a new classification scheme for Italian raw materials is proposed, based on three ranges: >10 µm, 2-10 µm and <2 µm, respectively. It allows distinction of specific grain-size features of bodies for (a) facing bricks; (b) roofing tiles; and (c) lightweight blocks, paving bricks and hollow slabs.


Author(s):  
J. Chalupsky ◽  
P. Bohacek ◽  
V. Hajkova ◽  
S.P. Hau-Riege ◽  
P.A. Heimann ◽  
...  
Keyword(s):  

2012 ◽  
Author(s):  
Tatiana A. Pikuz ◽  
Anatoly Y. Faenov ◽  
Yuji Fukuda ◽  
Yoshiaki Kato ◽  
Tetsuya Kawachi ◽  
...  

2020 ◽  
Vol 28 (18) ◽  
pp. 25664
Author(s):  
Vojtěch Vozda ◽  
Tomáš Burian ◽  
Věra Hájková ◽  
Libor Juha ◽  
Hartmut Enkisch ◽  
...  
Keyword(s):  

2014 ◽  
Vol 66 ◽  
pp. 146-151 ◽  
Author(s):  
Yu Qin ◽  
Takashi Nakajima ◽  
Heishun Zen ◽  
Xiaolong Wang ◽  
Toshiteru Kii ◽  
...  

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