scholarly journals A New Experimental Method for Determining Simultaneously True Radial Temperature Profiles of Polymer Melts under Isothermal Capillary Flow

2001 ◽  
Vol 33 (6) ◽  
pp. 491-494 ◽  
Author(s):  
Narongrit Sombatsompop ◽  
Somjate Patcharaphun
2001 ◽  
Author(s):  
Matt O’ Donnell ◽  
Sumanta Acharya

Abstract This work summarizes efforts to determine the accuracy and performance characteristics of a new and novel laser diagnostic to measure instantaneous, in flight, droplet temperatures. The instrument uses the location of the rainbow peak to deduce the refractive index of the droplet, which in turn is related to the droplet temperature. Preliminary experiments were undertaken in order to understand the fundamental operating principles and limitations of the instrument. These experiments measured the temperature of an isothermal, single stream of monodisperse droplets. These measurements indicate that the mean refractive index can be measured with a standard deviation as low as 0.0001m. Once the operation of the refractometer was proved under isothermal conditions, the measurement of droplet temperatures in a swirl-stabilized combustor was performed. These measurements indicate that the strength of the rainbow signal is significantly hampered by the noise induced by the flame. Preliminary temperature measurements with the combustor equipped with 45° vanes showed relatively constant radial temperature profiles (∼55–60°C) at locations less than 2 inches from the nozzle exit. A detailed examination of the temperature correlation with velocity and diameter revealed that larger and faster moving droplets dominate the distributions. Thus, the smaller droplets that are suspected of having the highest temperatures are inadequately represented in the mean droplet temperature.


1992 ◽  
Vol 200 ◽  
pp. 401-411
Author(s):  
Rafael Bilbao ◽  
María Benita Murillo ◽  
Angela Millera

Author(s):  
Felix Fischer ◽  
Julian Bartz ◽  
Katharina Schmitz ◽  
Ludwig Brouwer ◽  
Hubert Schwarze

The dynamic viscosity of a fluid is an important input parameter for the investigation of elastohydrodynamic contacts within tribological simulation tools. In this paper, a capillary viscometer is used to analyse the viscosity of a calibration fluid for diesel injection pumps. Capillary viscometers are often used for the determination of viscosities that show a significant dependence on shear rate, pressure and temperature such as polymer melts or blood. Therefore most of the research on corrections of measured viscosities have been made using polymer melts. A new method is presented to shorten the effort in evaluating the capillary experiment. The viscosity itself can be calculated from experimental data. Essential parameters are the radius of the capillary, its length, the capillary flow and the pressure difference over the capillary. These quantities are used in the Hagen-Poiseuille equation to calculate the viscosity, assuming laminar and monodirectional flow. According to said equation, the viscosity depends on the geometry and the pressure gradient. A typical capillary viscometer contains three main flow irregularities. First the contraction of the flow at the capillary inlet, second the expansion of the flow at the capillary outlet and third the inlet section length of the flow after which the velocity profile is fully developed. These flow phenomena cause pressure losses, which have to be taken into account, as well as the altered length of the laminar flow in the capillary. Furthermore, the temperature difference over the capillary also affects the outlet flow. Therefore, in this paper, a newly developed method is proposed, which shortens the effort in pressure and length correction. The method is valid for viscometers, which provide a single phase flow of the sampling fluid. Furthermore, the proposed correction is suited for arbitrary geometries. A numerical approach is chosen for the analysis of the experiment. In order to facilitate the experimental procedure of a capillary viscometer, a special algorithm was developed. The numerical approach uses a static CFD simulation, which is recursively passed through. If a termination condition, regarding the pressure difference between two cycles, is fulfilled, the real viscosity can be calculated in the usual way from the Hagen-Poiseuille equation. A special advantage of the proposed experimental evaluation is the general applicability for arbitrary geometries. In this paper, the procedure is validated with a well-known reference fluid and compared to data, which was gathered from a quartz viscometer experiment with the same fluid. Therefore, experiments are conducted with the capillary viscometer and compared at various pressure and temperature levels.


1969 ◽  
Vol 42 (3) ◽  
pp. 675-681 ◽  
Author(s):  
Gene A. Bialas ◽  
James L. White

Abstract The extrusion of molten plastics, elastomers and fibers represent an important industrial operation. The rate of extrusion of melts through dies is limited by the onset of a flow instability. This phenomenon consists of a change in flow from uniform to irregular that results in the production of rough and distorted extradates drastically different from the smooth cylinders obtained at lower rates. Extrusion melt flow instability is observed in the entire spectrum of polymer melts ranging from silicone gums through nylon and polyolefin plastics to raw elastomers. Since the first descriptions of this phenomena in the 1940's considerable research effort has been expended in this area with limited agreement. It is the purpose of part I to: (1) present new experimental data on capillary flow of polymer melts and extrudate distortion, and (2) to review critically the literature on extrudate distortion.


1972 ◽  
Vol 16 (2) ◽  
pp. 331-337 ◽  
Author(s):  
T. W. McHugh ◽  
E. R. Harrell ◽  
J. W. Powell ◽  
R. P. Chartoff

AIChE Journal ◽  
2004 ◽  
Vol 50 (1) ◽  
pp. 173-183 ◽  
Author(s):  
K. M. Van Geem ◽  
G. J. Heynderickx ◽  
G. B. Marin

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