scholarly journals High Pressure Cell for Small-Angle Neutron and Light Scattering Studies of Phase Transitions in Complex Liquids

1997 ◽  
Vol 29 (11) ◽  
pp. 931-939 ◽  
Author(s):  
Hiroyuki Takeno ◽  
Michihiro Nagao ◽  
Yoshiaki Nakayama ◽  
Hirokazu Hasegawa ◽  
Takeji Hashimoto ◽  
...  
2001 ◽  
Vol 72 (6) ◽  
pp. 2679-2685 ◽  
Author(s):  
Tadanori Koga ◽  
Shuiqin Zhou ◽  
Benjamin Chu ◽  
John L. Fulton ◽  
Shu Yang ◽  
...  

1986 ◽  
Vol 40 (2) ◽  
pp. 217-223 ◽  
Author(s):  
J. J. Martin ◽  
R. Cavagnat ◽  
J. C. Cornut ◽  
M. Couzi ◽  
G. Daleau ◽  
...  

A variable-temperature hydrostatic high-pressure cell for Raman scattering experiments is presented; it can be commonly used for pressures up to about 6 kbars, in the temperature range between 340 and 80 K. Examples of applications are given, concerning conformational equilibriums in liquid tridecane on the one hand, and structural phase transitions in crystalline (CH3)4NMnCl3(TMMC) and (CH3)4NCdCl3 (TMCC), on the other hand.


1993 ◽  
Vol 03 (C8) ◽  
pp. C8-487-C8-490 ◽  
Author(s):  
M. LORENZEN ◽  
C. RIEKEL ◽  
A. EICHLER ◽  
D. HÄUSSERMANN

2019 ◽  
Vol 90 (2) ◽  
pp. 025106 ◽  
Author(s):  
Burkhard Annighöfer ◽  
Arnaud Hélary ◽  
Annie Brûlet ◽  
Alexandre Colas de la Noue ◽  
Camille Loupiac ◽  
...  

2008 ◽  
Vol 41 (1) ◽  
pp. 167-175 ◽  
Author(s):  
Nozomi Ando ◽  
Pascale Chenevier ◽  
Martin Novak ◽  
Mark W. Tate ◽  
Sol M. Gruner

A high-pressure cell for synchrotron small-angle X-ray scattering (SAXS) studies of protein solutions is described. The design was optimized for use at up to 400 MPa in liquid pressure and with 8−12 keV X-rays with particular emphasis on the ease of use. The high-pressure cell was fabricated from corrosion-resistant Inconel 725 (Special Metals Corporation, Huntington, WV, USA) and featured Poulter-type windows [Poulter (1932).Phys. Rev.40, 861–871]. Flat natural diamonds, 500 µm thick, were recycled from diamond anvil cells and were shown to perform well as high-pressure SAXS windows. For a simple and effective method of sample isolation, disposable plastic sample cells with a defined path length and reproducible parasitic scattering were designed. These sample cells enable efficient use of synchrotron time. The cells facilitate rapid and easy sample changes, eliminate the need to clean the cell between sample changes, and reduce the sample volume to as low as 12 µl. The disposable cells can also be used separately from the high-pressure cell for SAXS measurements at ambient pressure and temporary storage of samples. The performance of the apparatus is demonstrated with T4 lysozyme.


2009 ◽  
Vol 246 (3) ◽  
pp. 604-611 ◽  
Author(s):  
Sergey V. Ovsyannikov ◽  
Vladimir V. Shchennikov ◽  
Andrzej Misiuk ◽  
Ivan A. Komarovsky

1975 ◽  
Vol 29 (5) ◽  
pp. 393-396 ◽  
Author(s):  
D. M. Cantor ◽  
J. Schroeder ◽  
J. Jonas

Polarization scrambling by high pressure cell windows as a function of pressure up to 2 kbar has been measured for two window materials and two sizes of plug apertures. Measured scrambling was about 1% for quartz, 0.5% for float glass, and decreased with decreasing aperture size. The amount of scrambling decreased significantly with time when the cell was left pressurized. A qualitative explanation of the results, based on changes in the P44 Pockets coefficient with pressure is given.


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