scholarly journals A high pressure cell for small angle X-ray scattering

1993 ◽  
Vol 03 (C8) ◽  
pp. C8-487-C8-490 ◽  
Author(s):  
M. LORENZEN ◽  
C. RIEKEL ◽  
A. EICHLER ◽  
D. HÄUSSERMANN
Keyword(s):  
High Pressure ◽  
Small Angle ◽  
High Pressure Cell ◽  
X Ray ◽  
Pressure Cell ◽  
X Ray Scattering ◽  
Ray Scattering

High hydrostatic pressure small-angle X-ray scattering cell for protein solution studies featuring diamond windows and disposable sample cells

2008 ◽  
Vol 41 (1) ◽  
pp. 167-175 ◽  
Author(s):  
Nozomi Ando ◽  
Pascale Chenevier ◽  
Martin Novak ◽  
Mark W. Tate ◽  
Sol M. Gruner
Keyword(s):  
High Pressure ◽  
Small Angle ◽  
Ambient Pressure ◽  
X Rays ◽  
High Pressure Cell ◽  
X Ray ◽  
Pressure Cell ◽  
X Ray Scattering ◽  
Solution Studies ◽  
Ray Scattering

A high-pressure cell for synchrotron small-angle X-ray scattering (SAXS) studies of protein solutions is described. The design was optimized for use at up to 400 MPa in liquid pressure and with 8−12 keV X-rays with particular emphasis on the ease of use. The high-pressure cell was fabricated from corrosion-resistant Inconel 725 (Special Metals Corporation, Huntington, WV, USA) and featured Poulter-type windows [Poulter (1932).Phys. Rev.40, 861–871]. Flat natural diamonds, 500 µm thick, were recycled from diamond anvil cells and were shown to perform well as high-pressure SAXS windows. For a simple and effective method of sample isolation, disposable plastic sample cells with a defined path length and reproducible parasitic scattering were designed. These sample cells enable efficient use of synchrotron time. The cells facilitate rapid and easy sample changes, eliminate the need to clean the cell between sample changes, and reduce the sample volume to as low as 12 µl. The disposable cells can also be used separately from the high-pressure cell for SAXS measurements at ambient pressure and temporary storage of samples. The performance of the apparatus is demonstrated with T4 lysozyme.

A Pressure-Induced Phase Transition in a Ternary Microemulsion with an Assembly of a New High-Pressure Cell and Small-Angle X-Ray Scattering Apparatus

1999 ◽  
Vol 38 (Part 1, No. 2A) ◽  
pp. 951-956 ◽  
Author(s):  
Hideki Seto ◽  
Daisuke Okuhara ◽  
Michihiro Nagao ◽  
Shigehiro Komura ◽  
Takayoshi Takeda
Keyword(s):  
Phase Transition ◽  
High Pressure ◽  
Small Angle ◽  
High Pressure Cell ◽  
X Ray ◽  
Pressure Cell ◽  
X Ray Scattering ◽  
Ray Scattering

High-pressure cell for simultaneous small-angle x-ray scattering and laser light scattering measurements

2001 ◽  
Vol 72 (6) ◽  
pp. 2679-2685 ◽  
Author(s):  
Tadanori Koga ◽  
Shuiqin Zhou ◽  
Benjamin Chu ◽  
John L. Fulton ◽  
Shu Yang ◽  
...  
Keyword(s):  
High Pressure ◽  
Light Scattering ◽  
Small Angle ◽  
Laser Light ◽  
Laser Light Scattering ◽  
High Pressure Cell ◽  
X Ray ◽  
Pressure Cell ◽  
X Ray Scattering ◽  
Scattering Measurements

High pressure cell for small- and wide-angle x-ray scattering

1997 ◽  
Vol 68 (12) ◽  
pp. 4588-4592 ◽  
Author(s):  
K. Pressl ◽  
M. Kriechbaum ◽  
M. Steinhart ◽  
P. Laggner
Keyword(s):  
High Pressure ◽  
Wide Angle ◽  
High Pressure Cell ◽  
X Ray ◽  
Pressure Cell ◽  
X Ray Scattering ◽  
Ray Scattering

scholarly journals Single-crystal CVD diamonds as small-angle X-ray scattering windows for high-pressure research

2012 ◽  
Vol 45 (3) ◽  
pp. 453-457 ◽  
Author(s):  
Suntao Wang ◽  
Yu-fei Meng ◽  
Nozomi Ando ◽  
Mark Tate ◽  
Szczesny Krasnicki ◽  
...  
Keyword(s):  
High Pressure ◽  
Chemical Vapor Deposition ◽  
Single Crystal ◽  
Small Angle ◽  
Vapor Deposition ◽  
Chemical Vapor ◽  
High Optical Quality ◽  
X Ray ◽  
X Ray Scattering ◽  
Ray Scattering

Small-angle X-ray scattering (SAXS) was performed on single-crystal chemical vapor deposition (CVD) diamonds with low nitrogen concentrations, which were fabricated by microwave plasma-assisted chemical vapor deposition at high growth rates. High optical quality undoped 500 µm-thick single-crystal CVD diamonds grown without intentional nitrogen addition proved to be excellent as windows on SAXS cells, yielding parasitic scattering no more intense than a 7.5 µm-thick Kapton film. A single-crystal CVD diamond window was successfully used in a high-pressure SAXS cell.

scholarly journals Effects of High Pressure on Internally Self-Assembled Lipid Nanoparticles: A Synchrotron Small-Angle X-ray Scattering (SAXS) Study

Langmuir ◽  
2016 ◽  
Vol 32 (45) ◽  
pp. 11907-11917 ◽  
Author(s):  
Chandrashekhar V. Kulkarni ◽  
Anan Yaghmur ◽  
Milos Steinhart ◽  
Manfred Kriechbaum ◽  
Michael Rappolt
Keyword(s):  
High Pressure ◽  
Small Angle ◽  
Lipid Nanoparticles ◽  
X Ray ◽  
X Ray Scattering ◽  
Self Assembled ◽  
Ray Scattering
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