scholarly journals Application of f1-Decoupled 2D-NMR Methods for Characterizing the Stereochemical Structure of tert-Butyl Acrylate Oligomers

1993 ◽  
Vol 25 (8) ◽  
pp. 789-805
Author(s):  
Miloš Suchopárek ◽  
Jiří Spěváček
Keyword(s):  
Butyl Acrylate ◽  
2D Nmr ◽  
Stereochemical Structure ◽  
Tert Butyl ◽  
Nmr Methods

Hydrogen Bonding-Derived Healable Polyacrylate Elastomers via On-demand Copolymerization of n-Butyl Acrylate and tert-Butyl Acrylate

2020 ◽  
Vol 12 (45) ◽  
pp. 50812-50822
Author(s):  
Wenyan Wang ◽  
Zongxu Liu ◽  
Zijian Guo ◽  
Junliang Zhang ◽  
Chunmei Li ◽  
...  
Keyword(s):  
Hydrogen Bonding ◽  
Butyl Acrylate ◽  
Tert Butyl ◽  
On Demand

scholarly journals Ambient-Temperature Synthesis of (E)-N-(3-(tert-Butyl)-1-methyl-1H-pyrazol-5-yl)-1-(pyridin-2-yl)methanimine

Molbank ◽  
10.3390/m1250 ◽  
2021 ◽  
Vol 2021 (3) ◽  
pp. M1250
Author(s):  
Diana Becerra ◽  
Justo Cobo ◽  
Juan-Carlos Castillo
Keyword(s):  
Mass Spectrometry ◽  
Nmr Spectroscopy ◽  
Ambient Temperature ◽  
Magnesium Sulfate ◽  
Elemental Analysis ◽  
Condensation Reaction ◽  
2D Nmr ◽  
2D Nmr Spectroscopy ◽  
Temperature Synthesis ◽  
Tert Butyl

We report the ambient-temperature synthesis of novel (E)-N-(3-(tert-butyl)-1-methyl-1H-pyrazol-5-yl)-1-(pyridin-2-yl)methanamine 3 in 81% yield by a condensation reaction between 3-(tert-butyl)-1-methyl-1H-pyrazol-5-amine 1 and 2-pyridinecarboxaldehyde 2 in methanol using magnesium sulfate as a drying agent. The N-pyrazolyl imine 3 was full characterized by IR, 1D, and 2D NMR spectroscopy, mass spectrometry, and elemental analysis.

Bacterial adhesion to toroidal nano-structures from poly(styrene)-block-poly(tert-butyl acrylate) diblock copolymer thin films

2010 ◽  
Vol 87 (5-8) ◽  
pp. 715-718 ◽  
Author(s):  
Shuyan Li ◽  
Andras Z. Komaromy ◽  
Dan V. Nicolau ◽  
Reinhard I. Boysen ◽  
Milton T.W. Hearn
Keyword(s):  
Thin Films ◽  
Diblock Copolymer ◽  
Butyl Acrylate ◽  
Bacterial Adhesion ◽  
Tert Butyl ◽  
Nano Structures

Three Novel Friedelane Triterpenes with Antimicrobial Activity from the Stems of Celastrus Monospermus

2013 ◽  
Vol 37 (1) ◽  
pp. 14-18 ◽  
Author(s):  
Haiping Xie ◽  
Mingxiang Chen ◽  
Dingyong Wang ◽  
Runlin Xu
Keyword(s):  
Antimicrobial Activity ◽  
2D Nmr ◽  
Moderate Activity ◽  
Luminescent Bacterium ◽  
Fish Meat ◽  
Photobacterium Leiognathi ◽  
Nmr Methods ◽  
Oleanane Triterpenoid

Three novel friedelane triterpenes, monospermonal, monospermonol and monospermondiol, along with six known friedelanes, 3-oxofriedelane, 3-oxofriedelan-28-al, 3,12-dioxofriedelane, 3-oxo-28-hydroxyfriedelane, 3-oxo-11 β-hydroxyfriedelane, 3-oxo-12 α-hydroxyfriedelane and an oleanane triterpenoid, 3 β-hydroxyolean-12-ene, were isolated from the stems of Celastrus monospermus Roxb. The structures of novel compounds, monospermonal, monospermonol and monospermondiol, were identified as 3,12-dioxofriedelan-28-al, 3,12-dioxo-28-hydroxyfriedelane and 3-oxo-12 α,28-dihydroxyfriedelane, respectively by spectroscopies including 2D NMR methods. These nine friedelane-type triterpenes were tested for antimicrobial activity against luminescent bacterium Photobacterium leiognathi N1 that had been isolated from “glowing” fish meat. Monospermonal and monospermonol showed moderate activity.

Base additives for use in a single layer 193-nm resist based upon poly(norbornene/maleic anhydride/acrylic acid/ tert -butyl acrylate)

2001 ◽  
Author(s):  
Francis M. Houlihan ◽  
Donna Person ◽  
Omkaram Nalamasu ◽  
Ilya Rushkin ◽  
Ognian N. Dimov ◽  
...  
Keyword(s):  
Maleic Anhydride ◽  
Acrylic Acid ◽  
Butyl Acrylate ◽  
Single Layer ◽  
Tert Butyl ◽  
193 Nm
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