ENHANCED FRACTURE TOUGHNESS OF ADHESIVE JOINTS WITH DOPING EPOXY BY GRAPHENE NANOPLATELETS

2021 ◽  
Author(s):  
SABRINE KHAMMASSI10.12783/asc36/35835 ◽  
MOSTAPHA TARFAOUI
Keyword(s):  
Fracture Toughness ◽  
Adhesive Bonding ◽  
Cohesive Zone Model ◽  
Numerical Study ◽  
Epoxy Adhesive ◽  
Diglycidyl Ether ◽  
Graphene Nanoplatelets ◽  
Zone Model ◽  
Bisphenol A Diglycidyl Ether ◽  
Bonded Composite

It is necessary to enhance the mechanical properties of adhesives to replace conventional joint methods with adhesive bonding. Epoxy in its pure state often suffers catastrophic damage due to its obvious brittleness and low fracture toughness. In this study, the double cantilever beam (DCB - Mode I) was used to characterize the fracture toughness of graphene/DGEBA-epoxy nanocomposite adhesive in bonded aluminium alloy joints and bonded composite joints. Adhesives based on an epoxy adhesive DGEBA (Bisphenol A diglycidyl ether) reinforced with two percentages (1wt.% and 2wt.%) of graphene nanoplatelets (GNP) were prepared. In this study, one shows that the fracture toughness of adhesive nanocomposites was significantly better than neat epoxy-bonded adhesives. Both types of joints contain graphene resulting in increased fracture toughness. Therefore, the maximum fracture toughness was observed until the GNP reached 1wt.%, and then it began to decrease, but it is still higher than that of the pure adhesive joint. On the other hand, this work aims to determine the influence of interfacial interactions on the behavior of enhanced bonded joints and how graphene nanoplatelets can enhance the rigidity of the interface between the substrate and the adhesive. In addition, a numerical study using ABAQUS was performed and compared with the experiments performed on DCB. For the modeling of the damage in an assembly joint, the Cohesive Zone Model (CZM) was used for the fracture behavior of the adhesive.

scholarly journals Environmental effects on mode II fracture toughness of unidirectional E-glass/vinyl ester laminated composites

2021 ◽  
Vol 28 (1) ◽  
pp. 382-393
Author(s):  
Mazaher Salamt-Talab ◽  
Fatemeh Delzendehrooy ◽  
Alireza Akhavan-Safar ◽  
Mahdi Safari ◽  
Hossein Bahrami-Manesh ◽  
...  
Keyword(s):  
Fracture Toughness ◽  
Sulfuric Acid ◽  
Vinyl Ester ◽  
Cohesive Zone Model ◽  
Flexural Modulus ◽  
Mode Ii ◽  
Zone Model ◽  
Sharp Drop ◽  
Mode Ii Fracture ◽  
Mode Ii Fracture Toughness

Abstract In this article, mode II fracture toughness ( G IIc {G}_{\text{IIc}} ) of unidirectional E-glass/vinyl ester composites subjected to sulfuric acid aging is studied at two different temperatures (25 and 90°C). Specimens were manufactured using the hand lay-up method with the [ 0 ] 20 {{[}0]}_{20} stacking sequence. To study the effects of environmental conditions, samples were exposed to 30 wt% sulfuric acid at room temperature (25°C) for 0, 1, 2, 4, and 8 weeks. Some samples were also placed in the same solution but at 90°C and for 3, 6, 9, and 12 days to determine the interlaminar fracture toughness at different aging conditions. Fracture tests were conducted using end notched flexure (ENF) specimens according to ASTM D7905. The results obtained at 25°C showed that mode II fracture toughness increases for the first 2 weeks of aging and then it decreases for the last 8 weeks. It was also found that the flexural modulus changes with the same trend. Based on the results of the specimens aged at 90°C, a sharp drop in fracture toughness and flexural modulus with a significant decrease in maximum load have been observed due to the aging. Finite element simulations were performed using the cohesive zone model (CZM) to predict the global response of the tested beams.

Quantitative Characterization of Hydride Spacing for Cohesive-Zone Modelling of Fracture Toughness in Zr-2.5Nb Pressure Tubes

2016 ◽  
Author(s):  
Cheng Liu ◽  
Leonid Gutkin ◽  
Douglas Scarth
Keyword(s):  
Fracture Toughness ◽  
Cohesive Zone ◽  
Cohesive Zone Model ◽  
Model Development ◽  
Threshold Value ◽  
Pressure Tube ◽  
Zone Model ◽  
Empirical Distributions ◽  
Hydride Formation ◽  
Pressure Tubes

Zr-2.5Nb pressure tubes in CANDU 1 reactors are susceptible to hydride formation when the solubility of hydrogen in the pressure tube material is exceeded. As temperature decreases, the propensity to hydride formation increases due to the decreasing solubility of hydrogen in the Zr-2.5Nb matrix. Experiments have shown that the presence of hydrides is associated with reduction in the fracture toughness of Zr-2.5Nb pressure tubes below normal operating temperatures. Cohesive-zone approach has recently been used to address this effect. Using this approach, the reduction in fracture toughness due to hydrides was modeled by a decrease in the cohesive-zone restraining stress caused by the hydride fracture and subsequent failure of matrix ligaments between the fractured hydrides. As part of the cohesive-zone model development, the ligament thickness, as represented by the radial spacing between adjacent fractured circumferential hydrides, was characterized quantitatively. Optical micrographs were prepared from post-tested fracture toughness specimens, and quantitative metallography was performed to characterize the hydride morphology in the radial-circumferential plane of the pressure tube. In the material with a relatively low fraction of radial hydrides, further analysis was performed to characterize the radial spacing between adjacent fractured circumferential hydrides. The discrete empirical distributions were established and parameterized using continuous probability density functions. The resultant parametric distributions of radial hydride spacing were then used to infer the proportion of matrix ligaments, whose thickness would not exceed the threshold value for low-energy failure. This paper describes the methodology used in this assessment and discusses its results.

scholarly journals A Numerical and Experimental Study of Adhesively-Bonded Polyethylene Pipelines

Polymers ◽  
2019 ◽  
Vol 11 (9) ◽  
pp. 1531 ◽  
Author(s):  
Guilpin ◽  
Franciere ◽  
Barton ◽  
Blacklock ◽  
Birkett
Keyword(s):  
Cohesive Zone ◽  
Adhesive Bonding ◽  
Structural Integrity ◽  
Cohesive Zone Model ◽  
Low Cost ◽  
Element Model ◽  
Zone Model ◽  
Adhesively Bonded ◽  
Lap Shear ◽  
Lap Shear Test

Adhesive bonding of polyethylene gas pipelines is receiving increasing attention as a replacement for traditional electrofusion welding due to its potential to produce rapid and low-cost joints with structural integrity and pressure tight sealing. In this paper a mode-dependent cohesive zone model for the simulation of adhesively bonded medium density polyethylene (MDPE) pipeline joints is directly determined by following three consecutive steps. Firstly, the bulk stress–strain response of the MDPE adherend was obtained via tensile testing to provide a multi-linear numerical approximation to simulate the plastic deformation of the material. Secondly, the mechanical responses of double cantilever beam and end-notched flexure test specimens were utilised for the direct extraction of the energy release rate and cohesive strength of the adhesive in failure mode I and II. Finally, these material properties were used as inputs to develop a finite element model using a cohesive zone model with triangular shape traction separation law. The developed model was successfully validated against experimental tensile lap-shear test results and was able to accurately predict the strength of adhesively-bonded MPDE pipeline joints with a maximum variation of <3%.

scholarly journals Numerical Study of the Fatigue Crack in Welded Beam-To-Column Connection Using Cohesive Zone Model

2006 ◽  
Vol 324-325 ◽  
pp. 847-850 ◽  
Author(s):  
Cedric Lequesne ◽  
A. Plumier ◽  
H. Degee ◽  
Anne Marie Habraken
Keyword(s):  
Cohesive Zone ◽  
Cohesive Zone Model ◽  
Numerical Study ◽  
Damage Model ◽  
Three Dimensional ◽  
Fatigue Behaviour ◽  
Bending Test ◽  
Zone Model ◽  
Moment Resisting Frame ◽  
Moment Resisting

The fatigue behaviour of the welded beam-to-column connections of steel moment resisting frame in seismic area must be evaluated. The cohesive zone model is an efficient solution to study such connections by finite elements. It respects the energetic conservation and avoids numerical issues. A three-dimensional cohesive zone model element has been implemented in the home made finite element code Lagamine [1]. It is coupled with the fatigue continuum damage model of Lemaître and Chaboche [2]. The cohesive parameters are identified by the inverse method applied on a three points bending test modelling.

Interfacial Debonding and Stress Field Analysis on a Single Fiber Composite Using FEM

2008 ◽  
Author(s):  
Yi Pan ◽  
Assimina A. Pelegri
Keyword(s):  
Stress Field ◽  
Cohesive Zone ◽  
Cohesive Zone Model ◽  
Fiber Composite ◽  
Interfacial Strength ◽  
Interfacial Debonding ◽  
Field Analysis ◽  
Zone Model ◽  
Linear Elastic ◽  
Bonded Composite

Fiber debonding in a bundled fiber reinforced polymer composite is investigated by using finite element method and cohesive zone model. Fiber and matrix are modeled as isotropic and linear elastic materials. Fiber/matrix interface is represented by a cohesive zone model governed by the traction-separation law. Effects of interfacial strength on interfacial debonding and stress field in the bundled fiber composite are examined. The stress field of the debonding composite is compared to that of perfectly bonded composite.

Modeling Stable and Unstable Crack Growth Observed in Quasi-Static Adhesively Bonded Beam Tests

2004 ◽  
Author(s):  
Rakesh K. Kapania ◽  
Dhaval P. Makhecha ◽  
Eric R. Johnson ◽  
Josh Simon ◽  
David A. Dillard
Keyword(s):  
Crack Growth ◽  
Cohesive Zone Model ◽  
Computational Study ◽  
Stable Crack Growth ◽  
Epoxy Adhesive ◽  
Zone Model ◽  
Adhesively Bonded ◽  
Unstable Crack ◽  
Interface Elements ◽  
Unstable Crack Growth

An experimental and computational study of an adhesively bonded, double cantilevered beam (DCB) under quasi-static loading is presented. The polymeric adhesives are either an acrylic or an epoxy, and the adherends are 6061 aluminum alloy. DCB tests bonded with the acrylic exhibited stable crack growth, while the DCB tests bonded with the epoxy exhibited unstable crack growth. The responses of the DCB test speciments were modeled in the ABAQUS/Standard® software package. Interface finite elements were located between bulk elements to model crack initiation and crack growth in the adhesive. These interface elements are implemented as user-defined elements in ABAQUS®, and the material law relating the interfacial tractions to the separation displacements is based on a cohesive zone model (CZM). Using interface elements only to model the acrylic adhesive, the simulation correlates very well to the test. Good correlation between the simulation and the test for the epoxy adhesive is achieved if both bulk modeling of the adhesive and inertia of the specimen are included.

Experimental and numerical study of the dynamic response of an adhesively bonded automotive structure

2020 ◽  
Vol 234 (14) ◽  
pp. 3385-3397
Author(s):  
NDD Silva ◽  
JJM Machado ◽  
EAS Marques ◽  
PMGP Moreira ◽  
LFM da Silva
Keyword(s):  
Adhesive Bonding ◽  
Numerical Study ◽  
Low Cost ◽  
High Strength ◽  
Epoxy Adhesive ◽  
Lap Joints ◽  
Impact Response ◽  
Vehicle Body ◽  
Component Level ◽  
The Impact

Based on economic and environmental factors related to energy efficiency, the automotive industry is being increasingly encouraged to design lighter structures, making use of adhesive bonding in vehicle body frames. To meet the standards of the automotive sector, adhesive joints must provide high strength and stiffness, low cost and good energy absorption at a component level, thereby ensuring good impact strength and passenger safety. This work aims to study, at room temperature (24°C), the impact response of a real scale automotive structure bonded with a crash-resistant epoxy, allowing to access the suitability of adhesives for automotive structural purposes. The epoxy adhesive was found to successfully transfer the loads to the aluminium substrates and not to compromise the integrity of the structure, as its failure was dominated by the behaviour of aluminium. Results obtained with a numerical model of the component were found to be in close agreement with the experimental failure load, demonstrating that numerical analysis can be a viable tool to predict the structure’s behaviour. In addition, a polyurethane was used as an alternative to the epoxy system to bond the structure, proving that the joint behaves better in the presence of a more flexible adhesive, as no failure was found for this case. Aluminium single-lap joints with two adhesive thicknesses were tested as a complement to understand the influence of this parameter on the impact response of a joint, showing a 21% decrease in strength when the highest thickness was used.

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