scholarly journals Thermal Analysis of Organic Medicinals. I. Detection of the Molecular Compound Formation by the Differential Thermal Analysis and by the Differential Scanning Calorimetry

1969 ◽  
Vol 17 (1) ◽  
pp. 191-199 ◽  
Author(s):  
KEIJI SEKIGUCHI ◽  
IKUZO HIMURO ◽  
ISAMU HORIKOSHI ◽  
TOSHIKO TSUKADA ◽  
TAKAKO OKAMOTO ◽  
...  
Keyword(s):  
Thermal Analysis ◽  
Differential Scanning Calorimetry ◽  
Differential Thermal Analysis ◽  
Molecular Compound ◽  
Scanning Calorimetry ◽  
Compound Formation

scholarly journals A thermal degradation study of Y and La methanesulfonates

2006 ◽  
Vol 71 (8-9) ◽  
pp. 905-915
Author(s):  
Moura de ◽  
Jivaldo Matos ◽  
Farias de
Keyword(s):  
Thermal Analysis ◽  
Differential Scanning Calorimetry ◽  
Differential Thermal Analysis ◽  
Thermal Degradation ◽  
Degradation Process ◽  
Oxide Formation ◽  
Scanning Calorimetry ◽  
Degradation Study ◽  
Thermogravimetric Data ◽  
Thermal Degradation Process

The synthesis, characterization and thermal degradation of yttrium and lanthanum methanesulfonates is reported. The prepared salts were characterized by elemental analysis and infrared spectroscopy. The thermal degradation study was performed using thermogravimetry (TG), differential thermal analysis (DTA) and differential scanning calorimetry (DSC).Using the thermogravimetric data, a kinetic study of the dehydration ofY and Lamethanesulfonates was performed employing the Coats-Redfern and Zsak?methods. It was verified that under heating, yttrium and lanthanum methanesulfonates undergo three main processes: dehydration, thermal degradation and oxide formation. Furthermore, depending on the nature of the atmosphere, i.e., inert or oxidant, the thermal degradation process could be endothermic (N2) or exothermic (air).

scholarly journals Thermal stability and thermal decomposition of sucralose

2018 ◽  
Vol 39 (4) ◽  
pp. 21
Author(s):  
Gilbert Bannach ◽  
Rafael R. Almeida ◽  
Luis G. Lacerda ◽  
Egon Schnitzler ◽  
Massao Ionashiro
Keyword(s):  
Thermal Stability ◽  
Thermal Analysis ◽  
Differential Scanning Calorimetry ◽  
Thermal Decomposition ◽  
Differential Thermal Analysis ◽  
Infrared Spectroscopy ◽  
Scanning Calorimetry ◽  
Thermoanalytical Techniques ◽  
Thermal Stability Of

Several papers have been described on the thermal stability of the sweetener, C12H19Cl3O8 (Sucralose). Nevertheless no study using thermoanalytical techniques was found in the literature. Simultaneous thermogravimetry and differential thermal analysis (TG-DTA), differential scanning calorimetry (DSC) and infrared spectroscopy, have been used to study the thermal stability and thermal decomposition of sweetener.

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