Thermal analysis techniques: Part II. Differential thermal analysis and differential scanning calorimetry

1972 ◽  
Vol 49 (11) ◽  
pp. A624
Author(s):  
W. W. Wendlandt
Keyword(s):  
Thermal Analysis ◽  
Differential Scanning Calorimetry ◽  
Differential Thermal Analysis ◽  
Scanning Calorimetry ◽  
Analysis Techniques ◽  
Thermal Analysis Techniques

scholarly journals Identification test of elements remaining in the barrel after firing, using Differential Scanning Calorimetry

2021 ◽  
Vol 2090 (1) ◽  
pp. 012163
Author(s):  
A Plachá ◽  
P Prasula ◽  
J Recko
Keyword(s):  
Thermal Analysis ◽  
Differential Scanning Calorimetry ◽  
Scanning Calorimetry ◽  
Analysis Techniques ◽  
Metal Case ◽  
Identification Test ◽  
Thermal Analysis Techniques

Abstract The issue of elements remaining in the barrel after firing is crucial both for the safe use of munition, and its reliability. These elements maybe categorized as being part of a metal case or a projectile (for example, fragments of broken connectors between a metal band and a projectile), or those associated with a propelling charge (like unburnt propellant grains). Both groups are undesirable and reflect the ammunition improper work. During own shooting tests of a 120 mm mortar ammunition the problem of unburnt elements remaining in the barrel occurred. The collected material was tested using one of the thermal analysis techniques - Differential Scanning Calorimetry - to characterize and to identify the tested sample.

scholarly journals A thermal degradation study of Y and La methanesulfonates

2006 ◽  
Vol 71 (8-9) ◽  
pp. 905-915
Author(s):  
Moura de ◽  
Jivaldo Matos ◽  
Farias de
Keyword(s):  
Thermal Analysis ◽  
Differential Scanning Calorimetry ◽  
Differential Thermal Analysis ◽  
Thermal Degradation ◽  
Degradation Process ◽  
Oxide Formation ◽  
Scanning Calorimetry ◽  
Degradation Study ◽  
Thermogravimetric Data ◽  
Thermal Degradation Process

The synthesis, characterization and thermal degradation of yttrium and lanthanum methanesulfonates is reported. The prepared salts were characterized by elemental analysis and infrared spectroscopy. The thermal degradation study was performed using thermogravimetry (TG), differential thermal analysis (DTA) and differential scanning calorimetry (DSC).Using the thermogravimetric data, a kinetic study of the dehydration ofY and Lamethanesulfonates was performed employing the Coats-Redfern and Zsak?methods. It was verified that under heating, yttrium and lanthanum methanesulfonates undergo three main processes: dehydration, thermal degradation and oxide formation. Furthermore, depending on the nature of the atmosphere, i.e., inert or oxidant, the thermal degradation process could be endothermic (N2) or exothermic (air).

scholarly journals Thermal stability and thermal decomposition of sucralose

2018 ◽  
Vol 39 (4) ◽  
pp. 21
Author(s):  
Gilbert Bannach ◽  
Rafael R. Almeida ◽  
Luis G. Lacerda ◽  
Egon Schnitzler ◽  
Massao Ionashiro
Keyword(s):  
Thermal Stability ◽  
Thermal Analysis ◽  
Differential Scanning Calorimetry ◽  
Thermal Decomposition ◽  
Differential Thermal Analysis ◽  
Infrared Spectroscopy ◽  
Scanning Calorimetry ◽  
Thermoanalytical Techniques ◽  
Thermal Stability Of

Several papers have been described on the thermal stability of the sweetener, C12H19Cl3O8 (Sucralose). Nevertheless no study using thermoanalytical techniques was found in the literature. Simultaneous thermogravimetry and differential thermal analysis (TG-DTA), differential scanning calorimetry (DSC) and infrared spectroscopy, have been used to study the thermal stability and thermal decomposition of sweetener.

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