Clay Mineralogy of Shale Gas Reservoirs through Integrating Infrared Spectroscopy and X-Ray Diffraction

Author(s):  
Hanieh Jafary Dargahi ◽  
Reza Rezaee ◽  
Bobby Pejcic
Energies ◽  
2020 ◽  
Vol 13 (2) ◽  
pp. 388 ◽  
Author(s):  
Yapei Ye ◽  
Shuheng Tang ◽  
Zhaodong Xi

The brittleness index (BI) is a key parameter used to identify the desirable fracturing intervals of shale gas reservoirs. Its correlation with fracability is still controversial. There have been a variety of methods proposed that can estimate BI. The brittleness evaluation method based on stress-strain curves according to the energy-balanced law is the most suitable and reliable in this study. Triaxial compression test, optical microscopy and scanning electron microscopy (SEM) observation, and X-ray diffraction analysis (XRD) were performed on nine drill core samples from well SY3 located in the peripheral regions of Sichuan Basin, China. These tests further evaluated several commonly used methods (brittleness indices based on rock elastic parameters, rock mineral compositions) and determined the relationship between brittleness, rock elastic parameters, and the content of minerals. The results obtained indicate that for sedimentary rocks, a higher Young’s modulus reduces the brittleness of rock, and Poisson’s ratio weakly correlates with brittleness. Excessive amounts of quartz or carbonate minerals can increase the cohesiveness of rock, leading to poor brittleness. Furthermore, the most suitable fracturing layers possess a high brittleness index and low minimum horizontal stress.


Author(s):  
Roger Yuan ◽  
Fa Dwan ◽  
Navpreet Singh ◽  
Liang Jin ◽  
Danny Soo ◽  
...  

Minerals ◽  
2021 ◽  
Vol 11 (1) ◽  
pp. 71
Author(s):  
Andrew Hurst ◽  
Michael Wilson ◽  
Antonio Grippa ◽  
Lyudmyla Wilson ◽  
Giuseppe Palladino ◽  
...  

Mudstone samples from the Moreno (Upper Cretaceous-Paleocene) and Kreyenhagen (Eocene) formations are analysed using X-ray diffraction (XRD) and X-ray fluorescence (XRF) to determine their mineralogy. Smectite (Reichweite R0) is the predominant phyllosilicate present, 48% to 71.7% bulk rock mineralogy (excluding carbonate cemented and highly bio siliceous samples) and 70% to 98% of the <2 μm clay fraction. Opal CT and less so cristobalite concentrations cause the main deviations from smectite dominance. Opal A is common only in the Upper Kreyenhagen. In the <2 μm fraction, the Moreno Fm is significantly more smectite-rich than the Kreyenhagen Fm. Smectite in the Moreno Fm was derived from the alteration of volcaniclastic debris from contemporaneous rhyolitic-dacitic magmatic arc volcanism. No tuff is preserved. Smectite in the Kreyenhagen Fm was derived from intense sub-tropical weathering of granitoid-dioritic terrane during the hypothermal period in the early to mid-Eocene; the derivation from local volcanism is unlikely. All samples had chemical indices of alteration (CIA) indicative of intense weathering of source terrane. Ferriferous enrichment and the occurrence of locally common kaolinite are contributory evidence for the intensity of weathering. Low concentration (max. 7.5%) of clinoptilolite in the Lower Kreyenhagen is possibly indicative of more open marine conditions than in the Upper Kreyenhagen. There is no evidence of volumetrically significant silicate diagenesis. The main diagenetic mineralisation is restricted to low-temperature silica phase transitions.


2020 ◽  
Vol 11 (1) ◽  
pp. 219
Author(s):  
Jing Zeng ◽  
Alexey Stovas ◽  
Handong Huang ◽  
Lixia Ren ◽  
Tianlei Tang

Paleozoic marine shale gas resources in Southern China present broad prospects for exploration and development. However, previous research has mostly focused on the shale in the Sichuan Basin. The research target of this study is expanded to the Lower Silurian Longmaxi shale outside the Sichuan Basin. A prediction scheme of shale gas reservoirs through the frequency-dependent seismic attribute technology is developed to reduce drilling risks of shale gas related to complex geological structure and low exploration level. Extracting frequency-dependent seismic attribute is inseparable from spectral decomposition technology, whereby the matching pursuit algorithm is commonly used. However, frequency interference in MP results in an erroneous time-frequency (TF) spectrum and affects the accuracy of seismic attribute. Firstly, a novel spectral decomposition technology is proposed to minimize the effect of frequency interference by integrating the MP and the ensemble empirical mode decomposition (EEMD). Synthetic and real data tests indicate that the proposed spectral decomposition technology provides a TF spectrum with higher accuracy and resolution than traditional MP. Then, a seismic fluid mobility attribute, extracted from the post-stack seismic data through the proposed spectral decomposition technology, is applied to characterize the shale reservoirs. The application result indicates that the seismic fluid mobility attribute can describe the spatial distribution of shale gas reservoirs well without well control. Based on the seismic fluid mobility attribute section, we have learned that the shale gas enrich areas are located near the bottom of the Longmaxi Formation. The inverted velocity data are also introduced to further verify the reliability of seismic fluid mobility. Finally, the thickness map of gas-bearing shale reservoirs in the Longmaxi Formation is obtained by combining the seismic fluid mobility attribute with the inverted velocity data, and two favorable exploration areas are suggested by analyzing the thickness, structure, and burial depth. The present work can not only be used to evaluate shale gas resources in the early stage of exploration, but also help to design the landing point and trajectory of directional drilling in the development stage.


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