Design and Optimization of Biopolyester Bagasse Fiber Composites

2007 ◽  
Vol 1 (1) ◽  
pp. 46-55 ◽  
Author(s):  
Alma Hodzic ◽  
Richard Coakley ◽  
Ray Curro ◽  
Christopher C. Berndt ◽  
Robert A. Shanks
Keyword(s):  
Stress Transfer ◽  
Soxhlet Extraction ◽  
Interfacial Stress ◽  
Fiber Volume ◽  
Mechanical Reinforcement ◽  
Xylem Structure ◽  
Design And Optimization ◽  
The Matrix ◽  
Packaging Industry ◽  
Bagasse Fiber

Bagasse fiber, a by-product of the sugar making process, maintains a coherent xylem structure and can offer mechanical reinforcement to composite materials. Biopolyester bagasse composites were prepared with biodegradable matrices polyhydroxylbutyrate (PHB) and its copolymer containing polyhydroxyvalerate (PHBV). Both biopolymers were reinforced with treated and untreated bagasse fibers, as well as fiber volume fractions involving two fiber lengths. Optimized properties were achieved with PHB-bagasse composite surpassing the PHB flexural strength by 50% and achieving higher strength and modulus than the standard thermoplastics. The bagasse fibers were cleaned with boiling water and acetone soxhlet extraction to avoid using adhesive chemicals and, therefore, comply with biosafety standards in the packaging industry. A significant improvement in the interfacial stress transfer between the fiber and the matrix was achieved with the fibers subjected to both washing and acetone treatment. While the crystallization of PHBV was shown to be controllable by processing conditions, it was concluded that no transcrystalline region was formed with this particular resin in any of the composites. Bagasse was shown to be an effective filler for PHBV; although the results varied somewhat due to the surface treatment of the bagasse fibers. On average, long fiber bagasse composites displayed flexural moduli 33% higher than those of PHBV. Overall, the results demonstrated the positive potential of bagasse to reinforce both biopolyester matrices.

scholarly journals Interfacial Pathways in Wood

2000 ◽  
Vol 9 (1) ◽  
pp. 096369350000900 ◽  
Author(s):  
Caroline Baillie ◽  
Delphine Tual ◽  
Jean Christophe Terraillon
Keyword(s):  
Environmental Conditions ◽  
Materials Science ◽  
Interfacial Crack ◽  
Stress Transfer ◽  
High Strength ◽  
Interfacial Stress ◽  
Fibre Composites ◽  
The Matrix ◽  
Energy Absorbing ◽  
Crack Paths

Wood structure and properties have been established for many years. The interaction of structure with properties has also been studied, but rarely from a materials science perspective. This paper attempts to focus on a particular aspect of composite structure, that of the interface. In engineered fibre composites the interface is the most important feature as it is the medium by which the stress is transferred from the matrix to the fibres so that they may bear the load. Much research has been focused on solving the optimisation of the interfacial stress transfer, as it is always suggested that the interface needs to be weak for high toughness and strong for high strength of the composite. More recent studies have identified the fact that it may be more advantageous to create an interface, which is not destructive in its energy absorbing capacity. Another area of weakness at the interface is the resistance to water ingress in certain environmental conditions. Biomimetics is an emerging approach to solving scientific issues by looking to nature to see what solutions are offered for the particular concerns of engineers and their products. In this case wood is the subject of study. It is assumed that wood has optimised its internal interfaces to cope with strength and toughness requirements as well as harsh environmental conditions. The internal interfaces thus need to be firstly examined and identified. This paper looks in a qualitative way at the three different interfacial crack paths which may be likened to those occurring in engineered composites: interfacial, interlaminar and intercellular (bundle/bundle interaction) and their proposed relation to energy absorption mechanisms, It also explores the influence of moisture on these fracture paths.

Determination of fiber volume fraction in a cured laminate

2021 ◽  
pp. 002199832110112
Author(s):  
Qing Yang Steve Wu ◽  
Nan Zhang ◽  
Weng Heng Liew ◽  
Vincent Lim ◽  
Xiping Ni ◽  
...  
Keyword(s):  
Carbon Fiber ◽  
Fiber Volume Fraction ◽  
Evaluation Method ◽  
Volume Fraction ◽  
Matrix Material ◽  
Volume Ratio ◽  
Gravimetric Analysis ◽  
Fiber Volume ◽  
Laser Ultrasonic ◽  
The Matrix

Propagation of ultrasonic wave in Carbon Fiber Reinforced Polymer (CFRP) is greatly influenced by the material’s matrix, resins and fiber volume ratio. Laser ultrasonic broadband spectral technique has been demonstrated for porosity and fiber volume ratio extraction on unidirection aligned CFRP laminates. Porosity in the matrix materials can be calculated by longitudinal wave attenuation and accurate fiber volume ratio can be derived by combined velocity through the high strength carbon fiber and the matrix material with further consideration of porosity effects. The results have been benchmarked by pulse-echo ultrasonic tests, gas pycnometer and thermal gravimetric analysis (TGA). The potentials and advantages of the laser ultrasonic technique as a non-destructive evaluation method for CFRP carbon fiber volume fraction evaluation were demonstrated.

scholarly journals Stress Transfer from Axially Loaded Fiber to Matrix in a Microcomposite

1994 ◽  
Vol 365 ◽  
Author(s):  
Chun-Hway Hsueh
Keyword(s):  
Analytical Solutions ◽  
Volume Fraction ◽  
Axial Stress ◽  
Stress Transfer ◽  
Radial Dependence ◽  
Shear Lag ◽  
Shear Lag Model ◽  
The Matrix ◽  
Lag Model ◽  
Loaded Fiber

ABSTRACTThe shear lag model has been used extensively to analyze the stress transfer in a singe fiberreinforced composite (i.e., a microcomposite). To achieve analytical solutions, various simplifications have been adopted in the stress analysis. Questions regarding the adequacy of those simplifications are discussed in the present study for the following two cases: bonded interfaces and frictional interfaces. Specifically, simplifications regarding (1) Poisson's effect, and (2) the radial dependences of axial stresses in the fiber and the matrix are addressed. For bonded interfaces, the former can be ignored, and the latter can generally be ignored. However, when the volume fraction of the fiber is high, the radial dependence of the axial stress in the fiber should be considered. For frictional interfaces, the latter can be ignored, but the former should be considered; however, it can be considered in an average sense to simplify the analysis. Comparisons among results obtained from analyses with various simplifications are made.

Characterization of interfacial stress transfer ability in acetylation-treated wood fibre composites using X-ray microtomography

2017 ◽  
Vol 95 ◽  
pp. 43-49 ◽  
Author(s):  
Thomas Joffre ◽  
Kristoffer Segerholm ◽  
Cecilia Persson ◽  
Stig L. Bardage ◽  
Cris L. Luengo Hendriks ◽  
...  
Keyword(s):  
Treated Wood ◽  
Stress Transfer ◽  
Wood Fibre ◽  
Interfacial Stress ◽  
X Ray ◽  
Fibre Composites

scholarly journals KARAKTERISTIK KEKUATAN TARIK KOMPOSIT BERPENGUAT SERAT AMPAS TEBU DENGAN MATRIKS EPOXY

2019 ◽  
Vol 3 (1) ◽  
Author(s):  
Catur Pramono ◽  
Sri Widodo ◽  
Muhammad Galih Ardiyanto
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Tensile Test ◽  
Alkaline Solution ◽  
Sugar Industry ◽  
The Matrix ◽  
Bagasse Fiber

Composite is a material consisting of two or more components which have characteristics mild and relatively strong. This study used bagasse fiber which is widely produced in sugar industry. Treatment of bagasse fiber by soaked in alkaline solution (NaOH) for 2 hours to remove the cork / wax attached to the fiber. Manufacture of composite by hand lay up. The matrix used in this study is epoxy. The fraction volume of composite between bagasse fiber and epoxy are 4%: 96%, 8%: 92% and 12%: 88%. The mechanical properties tested is tensile strength. The tensile test refers to ASTM D638 type 4. The highest tensile test composite resulted at the fraction volume composite of bagasse fiber with epoxy 12%: 88% i.e. 28.43 MPa.

scholarly journals Utilization of vegetable fibers for production of reinforced cementitious materials

2018 ◽  
Vol 2 ◽  
pp. 145-154 ◽  
Author(s):  
Viviane Costa Correia ◽  
Sergio Francisco Santos ◽  
Holmer Savastano Jr ◽  
Vanderley Moacyr John
Keyword(s):  
Mechanical Performance ◽  
Stress Transfer ◽  
Cost Effective ◽  
Nanofibrillated Cellulose ◽  
Cementitious Materials ◽  
Vegetable Fibers ◽  
The Matrix ◽  
As Stress ◽  
Hybrid Reinforcement ◽  
Cellulosic Pulp

Vegetable fibers produced from agroindustrial resources in the macro, micro and nanometric scales have been used as reinforcement in cementitious materials. The cellulosic pulp, besides being used as the reinforcing element, is also the processing fiber that is responsible for the filtration system in the Hatcheck method. On the other hand, the nanofibrillated cellulose has the advantage of having good mechanical performance and high specific surface, which contributes to improve the adhesion between fiber and matrix. In the hybrid reinforcement, with micro and nanofibers, the cellulose performs bonding elements with the matrix and acts as stress transfer bridges in the micro and nano-cracking network with the corresponding strengthening and toughening of the cementitious composite. Some strategies are studied to mitigate the degradation of the vegetable fibers used in cost-effective and non-conventional fiber cement, as well as to reach a sustainable fiber cement production. As a practical example, the accelerated carbonation curing at early age is a developing technology to increase the durability of composite materials: it decreases porosity, promotes a higher density in the interface generating a good fiber–matrix adhesion and a better mechanical behavior. Thus, the vegetable fibers are potentially applicable to produce high mechanical performance and sustainable cementitious materials for use in the Civil Construction.

scholarly journals Characterization of continuous Hibiscus sabdariffa fibre reinforced epoxy composites

2022 ◽  
Vol 30 ◽  
pp. 096739112110609
Author(s):  
Atik Mubarak Kazi ◽  
Ramasastry DVA
Keyword(s):  
Fibre Orientation ◽  
Stress Transfer ◽  
Dynamic Mechanical Properties ◽  
Epoxy Composites ◽  
Neat Epoxy ◽  
Hibiscus Sabdariffa ◽  
Sem Images ◽  
Fibre Composites ◽  
The Matrix

The influence of fibre orientation on physical, mechanical and dynamic mechanical properties of Hibiscus sabdariffa fibre composites has been studied. The composites with longitudinal (0°), transverse (90°) and inclined (45°) fibre orientation were prepared using the hand layup technique. ASTM standards were used for characterization of continuous Hibiscus sabdariffa fibre composites. The composite with longitudinally placed fibres yields improved mechanical characteristics. The addition of longitudinal (0°) oriented continuous Hibiscus sabdariffa fibres to the epoxy enhances tensile strength by 460%, flexural strength by 160% and impact strength by 603% compared to neat epoxy. The longitudinal (0°) fibre oriented composite offers higher resistance to water absorption and thickness swelling compared to other types of composites. All continuous Hibiscus sabdariffa fibre epoxy composites possess an improved storage modulus than the neat epoxy resin. The glass transition temperature of continuous Hibiscus sabdariffa fibre composites is 8%–31% lower than that of neat epoxy. Scanning electron microscopy (SEM) images confirm the existence of voids in the matrix, fibre pullout and crack propagation near the fibre bundle, which indicates the stress transfer between fibre and matrix is non-uniform.

scholarly journals Characterization by TGA, SEM, and EDX of Polymeric Matrices Used as Cocaine Camouflages

2018 ◽  
Vol 12 (12) ◽  
pp. 119
Author(s):  
Carlos A. Díaz V ◽  
William F. Garzón M ◽  
Juan C. Higuita V ◽  
Elisabeth. Restrepo-Parra
Keyword(s):  
Surface Morphology ◽  
Thermo Gravimetric Analysis ◽  
Soxhlet Extraction ◽  
Structural Type ◽  
Extraction Process ◽  
Gravimetric Analysis ◽  
Before And After ◽  
The Matrix ◽  
Morphological Differences ◽  
Almost All

In this work, a study of samples that contained cocaine camouflaged inside unidentified polymers was performed. Samples were seized at the Dorado International airport in Colombia. Cocaine was adsorbed or occluded within the matrix. The objective of this research was to extract cocaine from the matrices using soxhlet extraction method. Thereafter matrices were analyzed to determine the surface morphology before and after the extraction. Several morphological differences were exhibited between samples including both adsorbed and occluded cocaine. Moreover, changes in the surface morphology were also observed before and after cocaine extraction. The chemical elemental composition of matrices was also studied using energy dispersive spectroscopy, observing that the alkaloid was totally removed in almost all samples after the extraction process. On the other hand, Thermo gravimetric analysis also allows comparing the results obtained for the samples with patterns of pure cocaine and other polymers as CMC, PVA and HEC, finding several similarities of structural type.

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