scholarly journals Development and Performance Evaluation of Thin-Layer Color Antiwearing Paving Materials

2021 ◽  
Vol 2021 ◽  
pp. 1-12
Author(s):  
Zhaohui Liu ◽  
Xiangming Deng ◽  
Hao Guo ◽  
Yingchun Zhang ◽  
Di Wei ◽  
...  
Keyword(s):  
Thin Layer ◽  
Epoxy Resin ◽  
Bending Strength ◽  
Impact Load ◽  
Curing Agent ◽  
Mass Ratio ◽  
Bonding Performance ◽  
Strength Tests ◽  
Single Formula ◽  
Toughening Agent

To develop a color antiwearing wear layer based on epoxy resin adhesives, the effect of single formula composition on the properties of adhesives was analyzed through drawing strength tests, shear strength tests, and bending strength tests. It was found that when the mass ratio of the epoxy resin curing agent and the dosage of the toughening agent increased, the bonding performance and toughness of the adhesive firstly increased and then decreased. With the increase of the mass ratio of phenolic aldehyde amine to polyamide, the bonding performance and toughness of the adhesive were improved, but the effect was significantly reduced when the ratio was more than 2. With the increase of diluent content, the bonding performance and toughness of the adhesive were reduced. Based on response surface optimization, the optimum formulation was recommended. The content of the mass ratio of the epoxy resin to the curing agent and mass ratio of curing agent phenolic amine to polyamide, toughening agent content, and diluent content was determined to be 2.971%, 1.887%, 2.455%, and 1.000%, respectively. And, the dosage of each material was consistent with the effect of the dosage of a single formula on the properties of adhesives. The performance of the color antiwearing thin layer was tested by the adhesion test and antiwearing durability test. It was found that temperature had a significant effect on the adhesion, the adhesion of the thin layer was significantly reduced at low temperature, and the sensitivity to impact load was enhanced, while the adhesion and sensitivity to impact load were effectively improved at more than 20°C. At the same time, the antiwearing of the thin layer decreased rapidly at the initial stage under the reciprocating load but tended to be stable when the load exceeds 500 times.

Studies on Mechanical and Thermal Properties of Epoxy Resin Modified by Fluorine-Containing Silicone

2013 ◽  
Vol 401-403 ◽  
pp. 713-716
Author(s):  
Cheng Fang ◽  
Dong Bo Guan ◽  
Wei Guo Yao ◽  
Shou Jun Wang ◽  
Hui An
Keyword(s):  
Glass Transition ◽  
Thermal Properties ◽  
Epoxy Resin ◽  
Bending Strength ◽  
Mechanical And Thermal Properties ◽  
Curing Agent ◽  
Epoxy System ◽  
Resin Curing ◽  
The Impact ◽  
Modified Epoxy

The epoxy resin was modified with the mixture of α,ω-dihydroxy poly-(3,3,3-trifluoropropyl) siloxane (PTFPMS), KH560 and stannous octoate. KH560 can react with PTFPMS and also epoxy resin curing agent. The two reactions were characterized by FI-IR. The modified epoxy resin was characterized by FI-IR. The result showed that fluorine-containing silicone had been successfully introduced into the epoxy system. The mechanical and thermal properties of the modified epoxy resin were analyzed. The results showed that with the increase of PTFPMS the impact strength of epoxy resin increased, hardness and bending strength correspondingly reduced, slight decrease in the glass transition temperature.

Preparation and Properties of Polysiloxane Modified Epoxy Encapsulating Material

2014 ◽  
Vol 1021 ◽  
pp. 3-6
Author(s):  
Hao Ran Zhou ◽  
Hong Xia Li ◽  
Wei Miao Yu
Keyword(s):  
Epoxy Resin ◽  
Raw Materials ◽  
Curing Agent ◽  
Reaction Conditions ◽  
The Poor ◽  
Fatigue Durability ◽  
Ft Ir ◽  
Shock Resistance ◽  
Modified Epoxy ◽  
Toughening Agent

In order to solve the poor toughness, fatigue durability and shock resistance defects of the cured epoxy resin, in this paper, the epoxy resin was modified via dichlorodiphenyl silane as a modifier. Then the electronic packaging materials were prepared using the modified EP as matrix, a nitrile rubber (CTBN) as a toughening agent, methyl nadic anhydride (MNA) as a curing agent, and 2, 4, 6 - tris (dimethyl amino methyl) phenol as a curing accelerator. The effects of raw materials ratio on the cured products’ properties was investigated. FT-IR, TG-DTG and DMA were used to test and characterize the product. And we determined the best raw materials ratio and reaction conditions. Finally epoxy encapsulating materials which have excellent mechanical properties, electrical properties were prepared.

scholarly journals Mechanical Properties of Selected Epoxy Adhesive and Adhesive Joints of Steel Sheets

2021 ◽  
Vol 2 (1) ◽  
pp. 108-126
Author(s):  
Anna Rudawska
Keyword(s):  
Mechanical Properties ◽  
Epoxy Resin ◽  
Experimental Tests ◽  
Epoxy Adhesive ◽  
Adhesive Joints ◽  
Stoichiometric Ratio ◽  
Curing Agent ◽  
Steel Sheets ◽  
Epoxy Adhesives ◽  
Strength Tests

The article presents the issues of the mechanical properties of epoxy adhesives and the adhesive joints strength of steel sheets which were made using the epoxy adhesives. The aim of the paper is to study the mechanical properties of epoxy adhesive of different epoxy resin/curing agent ratios (within and above the recommended stoichiometric ratio) and their effect on mechanical properties of adhesive joints of steel sheets. In experimental tests three types of epoxy adhesives, containing a low molecular weight epoxy resin based on bisphenol A and polyamide curing agent, were used. A single-lap adhesive joint type of stainless-steel sheets was also applied. Two types of strength test were used: the compressive strength tests (DIN EN 196-1) for epoxy adhesive samples and the shear strength tests (DIN EN 1465) for adhesive joints. Both the analysis of the strength results of the samples of epoxy adhesive and adhesive joints as well as the failure analysis was carried out. On the basis of the results of strength tests it can be stated that the greatest deformation occurred for the samples of epoxy adhesive containing the modified epoxy resin (epoxy number—0.40) and the polyamide curing agent, and the smallest for the samples of epoxy adhesive containing the basic epoxy resin (epoxy number—0.49–0.52) and the polyamide curing agent. The epoxy adhesives with a smaller amount of curing agent were characterized by higher strength. This applies to all analyzed epoxy resins. The same dependences were obtained for the strength of adhesive joints of steel sheets made of the analyzed epoxy adhesive.

scholarly journals Preparation Optimization and Performance Evaluation of Waterborne Epoxy Resin for Roads

2021 ◽  
Vol 2021 ◽  
pp. 1-12
Author(s):  
Fei Wang ◽  
Hao Fu ◽  
Guixiang Liu ◽  
Chaohui Wang ◽  
Sixin Yu
Keyword(s):  
Epoxy Resin ◽  
Phase Inversion ◽  
Bending Strength ◽  
Impact Resistance ◽  
Inversion Method ◽  
Bonding Performance ◽  
Waterborne Epoxy ◽  
Bonding Properties ◽  
Waterborne Epoxy Resin ◽  
Phase Inversion Method

To further improve the road performance of waterborne epoxy resin, it was prepared by using the phase inversion method. The tensile properties, bending properties, impact resistance, and storage stability of waterborne epoxy resin were determined. The bonding properties of waterborne epoxy resin were analyzed. At the same time, their properties were compared with those of waterborne epoxy resin prepared by using the curing agent emulsification method. The performance of waterborne epoxy resin was comprehensively evaluated based on multi-index grey target decision model. The results show that the optimum preparation parameters for the preparation of waterborne epoxy resin by phase inversion method are shear time 1.5 h, shear temperature 60°C, and shear rate 1300–1500 r/min. The suitable contents of emulsifier A and B are 18% and 16%, respectively. The tensile strength, elongation at break, bending strength, bending deformation, and impact strength of waterborne epoxy resin prepared by emulsifier A can reach 34.46 MPa, 12.96%, 85.37 MPa, 19.42 mm, and 15.66 kJ/m2, respectively. It shows improved mechanical strength, deformation ability, impact resistance, and bonding performance. The comprehensive properties of waterborne epoxy resin prepared by emulsifier A are the best. It is suggested to use phase inversion method to prepare waterborne epoxy resin for roads.

Preparation and analysis of a flexible curing agent for epoxy resin

2009 ◽  
Vol 114 (5) ◽  
pp. 2706-2710 ◽  
Author(s):  
Y. Yang ◽  
Gong Chen ◽  
K. M. Liew
Keyword(s):  
Epoxy Resin ◽  
Curing Agent

scholarly journals Synthesis of antibacterial polyether biguanide curing agent and its cured antibacterial epoxy resin

2021 ◽  
Vol 24 (1) ◽  
pp. 63-72
Author(s):  
Rui Li ◽  
Guoxing Yang ◽  
Yudan Wang ◽  
Lijia Liu ◽  
Qiang Wang ◽  
...  
Keyword(s):  
Epoxy Resin ◽  
Curing Agent

scholarly journals Preparation and Thermal Conductivity of Epoxy Resin/Graphene-Fe3O4 Composites

Materials ◽  
2021 ◽  
Vol 14 (8) ◽  
pp. 2013
Author(s):  
Zhong Wu ◽  
Jingyun Chen ◽  
Qifeng Li ◽  
Da-Hai Xia ◽  
Yida Deng ◽  
...  
Keyword(s):  
Magnetic Field ◽  
Thermal Conductivity ◽  
Thermal Stability ◽  
Epoxy Resin ◽  
Thermomechanical Properties ◽  
Packaging Materials ◽  
Mass Ratio ◽  
Degree Of Orientation ◽  
Ep Matrix ◽  
Electrical Insulation Properties

By modifying the bonding of graphene (GR) and Fe3O4, a stable structure of GR-Fe3O4, namely magnetic GR, was obtained. Under the induction of a magnetic field, it can be orientated in an epoxy resin (EP) matrix, thus preparing EP/GR-Fe3O4 composites. The effects of the content of GR and the degree of orientation on the thermal conductivity of the composites were investigated, and the most suitable Fe3O4 load on GR was obtained. When the mass ratio of GR and Fe3O4 was 2:1, the thermal conductivity could be increased by 54.8% compared with that of pure EP. Meanwhile, EP/GR-Fe3O4 composites had a better thermal stability, dynamic thermomechanical properties, and excellent electrical insulation properties, which can meet the requirements of electronic packaging materials.

Adhesive properties of bio-based epoxy resin reinforced by cellulose nanocrystal additives

2020 ◽  
Vol 40 (4) ◽  
pp. 314-320 ◽  
Author(s):  
Tariq Aziz ◽  
Hong Fan ◽  
Xiangwei Zhang ◽  
Farman Ullah Khan ◽  
Shah Fahad ◽  
...  
Keyword(s):  
Epoxy Resin ◽  
Tensile Modulus ◽  
The Self ◽  
Environmental Engineering ◽  
Interface Area ◽  
Adhesive Properties ◽  
Composite Matrix ◽  
Bonding Performance ◽  
Good Expansion ◽  
Application Prospects

AbstractThe adhesive properties of a self-prepared bio-based epoxy resin with native cellulose nanocrystals (CNCs) are evaluated in this article. The porosity of actual CNCs is high. The most promising finding is the acquisition of high tensile modulus. The addition of CNC composites significantly increased the tensile modulus at lower wt.%, and the maximum crystallinity of CNCs was obtained. Bearing in mind the advantages of CNCs, scanning electron microscopy (SEM) showed a uniform distribution of concentrated CNCs. Clusters were formed at higher CNCs ratios, and the composite matrix content with high CNCs produced good expansion, low crystallinity, and increased elongation. Our analysis showed that the original CNCs were more evenly distributed in the self-prepared bio-based epoxy resin, which enhanced transformation, supported by improved dispersion of native CNCs. The presence of native CNCs greatly improved and enhanced the bonding performance of the bio-based epoxy resin in the interface area. Enhancing the mechanical properties of native CNCs has broad application prospects in environmental areas. This suggests that the widespread use of native CNCs in environmental engineering applications is feasible, especially in terms of adhesives properties.

EFFECTS OF NUMBER OF PLIES ON LIGHTNING STRIKE PROTECTION OF ELECTRICALLY CONDUCTIVE LAYER-WISE HYBRID LAMINATES

2021 ◽  
Author(s):  
SIWAT MANOMAISANTIPHAP ◽  
TOMOHIRO YOKOZEK YOKOZEKI
Keyword(s):  
Epoxy Resin ◽  
Composite Laminates ◽  
Bending Strength ◽  
Fuel Efficiency ◽  
Lightning Strike ◽  
Conductive Layer ◽  
Electrically Conductive ◽  
Hybrid Laminates ◽  
Conductive Polyaniline ◽  
Pani Layer

With the development of composite technologies, aircraft become lighter and more fuel efficiency. The composite aircraft, however, become susceptible to lightning strike. Developing lightning strike protection (LSP) system need to couple with composite technologies. The authors present a concept of LSP using layer-wise hybrid laminates (CF/Hybrid) in this study. The aim of the study is to validate the effectiveness of layer-wise hybrid laminates structure for lightning strike application by using conventional epoxy-resin CFRP for main structure and electrically conductive layer as a cover layer. The composite laminates include two different types of resin in each layer: conductive polyaniline-based matrix (CF/PANI) and conventional epoxy resin (CF/epoxy). CF/PANI layers varied from 1, 2, and 4 layers with corresponding 7, 6, and 4 layers of CF/epoxy to find out the least effective number of CF/PANI that can prevent lightning strike damage. The specimens were characterized for their mechanical properties and underwent simulated lightning strike test to realize their effectiveness. The result of simulated lightning strike has shown that a layer of conductive CF/PANI can help to avoid catastrophic damage on CF/epoxy. With a greater number of CF/PANI, the less detectable damage in CF/PANI layer became. In the case of CF/Hybrid with 4 layers of CF/PANI shows 70% residual bending strength after the lightning strike. With the aid of nondestructive inspection tools, i.e., thermography and ultrasonic test, the mechanism of damage on the composite panels were observed and analyzed. From this study, CF/Hybrid with 4 layers shows the optimal properties for lightning strike protection.

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