scholarly journals Effect of Nitrogen Ion Implantation Energy on the Mechanical and Chemical Properties of AISI M50 Steel

2021 ◽  
Vol 2021 ◽  
pp. 1-8
Author(s):  
Xiangyu Xie ◽  
Chao Chen ◽  
Jun Luo ◽  
Jin Xu

Nitrogen ion implantation has shown its role in enhancing steel surface properties. In this work, AISI M50 steel was implanted with nitrogen ions by using the metal vapor vacuum arc technique with a dose of 2 × 1017 cm−2, and corresponding implanted energies were at 60 keV, 80 keV, and 100 keV, respectively. The distribution of implanted nitrogen ions was calculated, and the samples were tribologically tested and examined. As shown by the results, the microhardness in implanted samples was 1.17 times greater relative to that of the unimplanted sample. The implantation of the nitrogen ion leads to a change in the friction coefficient of the AISI M50 steel. Adhesive wear mechanism occurs in the unimplanted sample, and adhesion resistance tends to increase when nitrogen-implanted energy increases. The formation of oxides α-Fe2O3 and Fe3O4 further enhanced the tribological properties for implanted samples.

2019 ◽  
Vol 108 ◽  
pp. 79-83
Author(s):  
JACEK WILKOWSKI ◽  
MAREK BARLAK ◽  
ROMAN BÖTTGER ◽  
ZBIGNIEW WERNER

The effect of nitrogen ion implantation on nano-scale hardness and elastic modulus of WC-Co indexable knives for wood materials machining. The paper presents the results of a study investigating the effects of nitrogen ion implantation into the surface layer of WC-Co blades, used for machining wood materials, on their hardness and modulus of elasticity at the nano-scale. The modified blades were analyzed in six variants of implantation process parameters, and compared with control blades (virgin, unmodified). Three energies of accelerating nitrogen ions were used in the implantation process (5, 50 and 500 keV) and two doses of implanted ions (1e17 and 5e17 cm-2). The nano-hardness and elastic modulus of all blades were measured using an Anton Paar TriTec (UNHT) hardness tester.


Coatings ◽  
2021 ◽  
Vol 11 (7) ◽  
pp. 775
Author(s):  
Zhongyu Dou ◽  
Yinglu Guo ◽  
Faguang Zhang ◽  
Dianxi Zhang

To further improve the performance of the coated tools, we investigated the effects of low-energy nitrogen ion implantation on surface structure and wear resistance for TiC coatings deposited by ion plating. In this experiment, an implantation energy of 40 keV and a dose of 2 × 1017 to 1 × 1018 (ions/cm2) were used to implant N ions into the TiC coatings. The results indicate that the surface roughness of the coating increases first and then decreases with the increase of ion implantation dose. After ion implantation, the surface of the coating will soften and reduce the hardness, and the production of TiN phase will gradually increase the hardness. Nitrogen ion implantation can reduce the friction coefficient of the TiC coating and improve the friction performance. In terms of wear resistance, the coating with an implant dose of 1×1018 ions/cm2 has the greatest improvement in wear resistance. Tribological analysis shows that the improvement in the performance of TiC coatings implanted with N ions is mainly due to the effect of the lubricating implanted layer. The implanted layer mainly exists in the form of amorphous TiC, TiN phase, and sp2C–C phase.


Membranes ◽  
2021 ◽  
Vol 11 (11) ◽  
pp. 899
Author(s):  
Gene Sheu ◽  
Yu-Lin Song ◽  
Dupati Susmitha ◽  
Kutagulla Issac ◽  
Ramyasri Mogarala

This study presents an innovative, low-cost, mass-manufacturable ion implantation technique for converting thin film normally on AlGaN/GaN devices into normally off ones. Through TCAD (Technology Computer-Aided Design) simulations, we converted a calibrated normally on transistor into a normally off AlGaN/GaN transistor grown on a silicon <111> substrate using a nitrogen ion implantation energy of 300 keV, which shifted the bandgap from below to above the Fermi level. In addition, the threshold voltage (Vth) was adjusted by altering the nitrogen ion implantation dose. The normally off AlGaN/GaN device exhibited a breakdown voltage of 127.4 V at room temperature because of impact ionization, which showed a positive temperature coefficient of 3 × 10−3 K−1. In this study, the normally off AlGaN/GaN device exhibited an average drain current gain of 45.3%, which was confirmed through an analysis of transfer characteristics by changing the gate-to-source ramping. Accordingly, the proposed technique enabled the successful simulation of a 100-µm-wide device that can generate a saturation drain current of 1.4 A/mm at a gate-to-source voltage of 4 V, with a mobility of 1487 cm2V−1s−1. The advantages of the proposed technique are summarized herein in terms of processing and performance.


2017 ◽  
Vol 1142 ◽  
pp. 31-36
Author(s):  
De Weng Tang ◽  
Wen Ming Zhang ◽  
Rui Lan Zhao ◽  
Xi Jian Lv

To improve medical pure magnesium corrosion and wear resistance, the advanced plasma implantation technology were used to implanted medical pure magnesium with nitrogen ions under certain conditions, obtaining a certain depth of nitrogen ion implantation layer, and to study the surface properties of the implantation layer. The sample after ion implanted, the surface morphology, phase composition were analyzed, and have electro chemical corrosion tests, friction and wear tests, the results showed that: pure magnesium by nitrogen ion implantation, can be obtained a surface organizations which whole flat, compact, no surface cracks and holes; the surface implantation layer mainly composed of Mg and MgO, also found a small amount of Mg3N2, which is also the main reason for corrosion and wear resistance improved; compared to pure magnesium base, nitrogen ion implantation (process conditions: implantation energy: 40KeV, implantation dose: 3×1017ions/cm2, control temperature: 200°C) improved the corrosion resistance of the sample, but not obvious, about 1.2%; however, the friction coefficient decreased significantly, approximately 61%, the amount of wear also reduced significantly, about 74%, this means that, its wear resistance has been improved significantly. This study provides a reference to improve the surface properties of pure magnesium and be learned to develop a more reasonable parameters for further study of medical pure magnesium by ion implantation of nitrogen.


2008 ◽  
Vol 373-374 ◽  
pp. 342-345 ◽  
Author(s):  
Hai Zhou ◽  
Fei Chen ◽  
Ying Ge Yang ◽  
Han Cheng Wan ◽  
Shuo Cai

Ti ion and C ion is implanted into AZ31 magnesium alloy surface by metal vapor vacuum arc (MEVVA) implanter operating with a modified cathode. This metal arc ion source has a broad beam and high current capabilities. Implantation energy is fixed at 45K eV and dose is 9×1017 cm-2 and 3×1017 cm-2 respectively. Through ion implantation, Ti ion implantation layer approximately 1000nm thick is directly formed on the surface of AZ31 magnesium alloy, by which its surface property is greatly improved. Microstructure, the component distribution and phase composition are analyzed using scanning electron microscopy (SEM) and X-ray diffraction (XRD). The property of hardness of the ion implantation layer was studied by HMV-1T Vickers micro hardness tester. The results show that Ti ion implantation layer of a magnesium alloy surface is mainly composed of TiO2, MgO and a little of TiO. The Ti-C double ions implantation layer is composed of MgO, TiC. The hardness of ion implantation layer is improved.


Materials ◽  
2021 ◽  
Vol 14 (9) ◽  
pp. 2324
Author(s):  
Mirosław Szala ◽  
Dariusz Chocyk ◽  
Anna Skic ◽  
Mariusz Kamiński ◽  
Wojciech Macek ◽  
...  

From the wide range of engineering materials traditional Stellite 6 (cobalt alloy) exhibits excellent resistance to cavitation erosion (CE). Nonetheless, the influence of ion implantation of cobalt alloys on the CE behaviour has not been completely clarified by the literature. Thus, this work investigates the effect of nitrogen ion implantation (NII) of HIPed Stellite 6 on the improvement of resistance to CE. Finally, the cobalt-rich matrix phase transformations due to both NII and cavitation load were studied. The CE resistance of stellites ion-implanted by 120 keV N+ ions two fluences: 5 × 1016 cm−2 and 1 × 1017 cm−2 were comparatively analysed with the unimplanted stellite and AISI 304 stainless steel. CE tests were conducted according to ASTM G32 with stationary specimen method. Erosion rate curves and mean depth of erosion confirm that the nitrogen-implanted HIPed Stellite 6 two times exceeds the resistance to CE than unimplanted stellite, and has almost ten times higher CE reference than stainless steel. The X-ray diffraction (XRD) confirms that NII of HIPed Stellite 6 favours transformation of the ε(hcp) to γ(fcc) structure. Unimplanted stellite ε-rich matrix is less prone to plastic deformation than γ and consequently, increase of γ phase effectively holds carbides in cobalt matrix and prevents Cr7C3 debonding. This phenomenon elongates three times the CE incubation stage, slows erosion rate and mitigates the material loss. Metastable γ structure formed by ion implantation consumes the cavitation load for work-hardening and γ → ε martensitic transformation. In further CE stages, phases transform as for unimplanted alloy namely, the cavitation-inducted recovery process, removal of strain, dislocations resulting in increase of γ phase. The CE mechanism was investigated using a surface profilometer, atomic force microscopy, SEM-EDS and XRD. HIPed Stellite 6 wear behaviour relies on the plastic deformation of cobalt matrix, starting at Cr7C3/matrix interfaces. Once the Cr7C3 particles lose from the matrix restrain, they debond from matrix and are removed from the material. Carbides detachment creates cavitation pits which initiate cracks propagation through cobalt matrix, that leads to loss of matrix phase and as a result the CE proceeds with a detachment of massive chunk of materials.


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