scholarly journals Effect of Injection Molding Melt Temperatures on PLGA Craniofacial Plate Properties during In Vitro Degradation

2017 ◽  
Vol 2017 ◽  
pp. 1-11 ◽  
Author(s):  
Liliane Pimenta de Melo ◽  
Gean Vitor Salmoria ◽  
Eduardo Alberto Fancello ◽  
Carlos Rodrigo de Mello Roesler
Keyword(s):  
Mechanical Properties ◽  
Injection Molding ◽  
Melt Temperature ◽  
In Vitro Degradation ◽  
Molecular Weights ◽  
Ft Ir ◽  
Injection Molded ◽  
Higher Temperature ◽  
Lower Temperature

The purpose of this article is to present mechanical and physicochemical properties during in vitro degradation of PLGA material as craniofacial plates based on different values of injection molded temperatures. Injection molded plates were submitted to in vitro degradation in a thermostat bath at 37 ± 1°C by 16 weeks. The material was removed after 15, 30, 60, and 120 days; then bending stiffness, crystallinity, molecular weights, and viscoelasticity were studied. A significant decrease of molecular weight and mechanical properties over time and a difference in FT-IR after 60 days showed faster degradation of the material in the geometry studied. DSC analysis confirmed that the crystallization occurred, especially in higher melt temperature condition. DMA analysis suggests a greater contribution of the viscous component of higher temperature than lower temperature in thermomechanical behavior. The results suggest that physical-mechanical properties of PLGA plates among degradation differ per injection molding temperatures.

Experimental Study on the Crystallinity and Mechanical Properties of the Injection Molded Polypropylene

2011 ◽  
Vol 239-242 ◽  
pp. 2809-2812 ◽  
Author(s):  
Xiao Xun Zhang ◽  
Luo Wang ◽  
Qiu Hui Liao
Keyword(s):  
Mechanical Properties ◽  
Injection Molding ◽  
Diffraction Method ◽  
Processing Conditions ◽  
Mould Temperature ◽  
X Ray Diffraction ◽  
Melt Temperature ◽  
X Ray ◽  
Injection Speed ◽  
Injection Molded

Polypropylene specimens were made by the injection molding experiments under different processing conditions. The crystallinity of each polypropylene specimen was obtained using the X-ray diffraction method. The effects of the injection molding processes on the crystallinity of polypropylene were revealed: (1) the crystallinity decreases as the melt temperature increases, and the higher the melt temperature, the slower the crystallinity decreases, (2) the crystallinity decreases as the mould temperature increases, and the higher the mould temperature, the faster the crystallinity decreases, (3) the crystallinity increases as the injection speed increases, and the larger the injection speed, the faster the crystallinity increases. By the tensile experiments of the injection molded specimens, it is also found that the crystallinity has a major impact on the mechanical properties of polypropylene. The yield strength and tensile strength of polypropylene specimens increase as the crystallinity increases.

Correlation Between Mechanical Properties in Standard Test Specimens and Injection Molded Thin-Wall Parts

2013 ◽  
Author(s):  
Laurentiu I. Sandu ◽  
Felicia Stan ◽  
Catalin Fetecau
Keyword(s):  
Mechanical Properties ◽  
Elastic Modulus ◽  
Yield Strength ◽  
Injection Molding ◽  
Process Conditions ◽  
Thin Wall ◽  
Optimal Process ◽  
Melt Temperature ◽  
Molded Parts ◽  
Injection Molded

In this paper, we investigated the effect of injection molding parameters on the mechanical properties of thin-wall injection molded parts. A four-factor (melt temperature, mold temperature, injection speed and packing pressure) and three-level fractional experimental design was performed to investigate the influence of each factor on the mechanical properties and determine the optimal process conditions that maximize the mechanical properties of the part using the signal-to-noise (S/N) ratio response. The mechanical properties (e.g., elastic modulus, yield strength and strain at break) were measured by tensile tests at room temperature, at a crosshead speed of 5 mm/min, and compared with those of the injection-molded specimens. The experimental results showed that the tensile properties were highly dependent on the injection molding parameters, regardless of the type of the specimens. The values of Young modulus and yield strength of the injection-molded specimens were lower than those of the injection-molded parts, while the elongation at break was considerably lower for the injection-molded parts. The optimal process conditions were strongly dependent on the measured performance quantities (elastic modulus, yield strength and strain at break).

Mechanical properties and in vitro degradation of bioresorbable knitted stents

2002 ◽  
Vol 13 (12) ◽  
pp. 1313-1323 ◽  
Author(s):  
Juha-Pekka Nuutinen ◽  
Tero Välimaa ◽  
Claude Clerc ◽  
Pertti Törmälä
Keyword(s):  
Mechanical Properties ◽  
In Vitro Degradation

Effects of Sr Addition on Mechanical Properties and Microstructure of Mg-6Al Magnesium Alloy

2011 ◽  
Vol 686 ◽  
pp. 120-124
Author(s):  
Jin Ping Fan ◽  
She Bin Wang ◽  
Bing She Xu
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Magnesium Alloy ◽  
Strengthening Mechanism ◽  
Microstructure And Mechanical Properties ◽  
Higher Temperature ◽  
Lower Temperature

The effects of Sr addition on the mechanical properties and microstructure of Mg-6Al mag- nesium alloy both at 25 °C and at 175 °C were investigated by means of OM, SEM and EDS and XRD. Upon the Sr addition of 2%, the tensile strength was increased by 7.2% to 184.4MPa at 25 °C, while it was increased by 30% to 155.4MPa at 175 °C. The strengthening mechanism of Mg-6Al-xSr at lower temperature (25 °C) was different from that at higher temperature (175°C). The results show that the addition of strontium effectively improved the microstructure and mechanical properties of magnesium alloy.

scholarly journals Post-Processing Time Dependence of Shrinkage and Mechanical Properties of Injection-Molded Polypropylene

Materials ◽  
2020 ◽  
Vol 14 (1) ◽  
pp. 22
Author(s):  
Artur Kościuszko ◽  
Dawid Marciniak ◽  
Dariusz Sykutera
Keyword(s):  
Mechanical Properties ◽  
Impact Strength ◽  
Injection Molding ◽  
Accelerated Aging ◽  
Mold Temperature ◽  
Degree Of Crystallinity ◽  
Injection Mold ◽  
Secondary Crystallization ◽  
Scanning Calorimetry ◽  
Injection Molded

Dimensions of the injection-molded semi-crystalline materials (polymeric products) decrease with the time that elapses from their formation. The post-molding shrinkage is an effect of secondary crystallization; the increase in the degree of polymer crystallinity leads to an increase in stiffness and decrease in impact strength of the polymer material. The aim of this study was to assess the changes in the values of post-molding shrinkage of polypropylene produced by injection molding at two different temperatures of the mold (20 °C and 80 °C), and conditioned for 504 h at 23 °C. Subsequently, the samples were annealed for 24 h at 140 °C in order to conduct their accelerated aging. The results of shrinkage tests were related to the changes of mechanical properties that accompany the secondary crystallization. The degree of crystallinity of the conditioned samples was determined by means of density measurements and differential scanning calorimetry. It was found that the changes in the length of the moldings that took place after removal from the injection mold were accompanied by an increase of 20% in the modulus of elasticity, regardless of the conditions under which the samples were made. The differences in the shrinkage and mechanical properties of the samples resulting from mold temperature, as determined by tensile test, were removed by annealing. However, the samples made at two different injection mold temperature values still significantly differed in impact strength, the values of which were clearly higher for the annealed samples compared to the results determined for the samples immediately after the injection molding.

Mechanical Properties of Injection Molded Rubber Testing Samples

2015 ◽  
Vol 752-753 ◽  
pp. 308-311
Author(s):  
Adam Skrobak ◽  
Michal Stanek ◽  
David Manas ◽  
Martin Ovsik ◽  
Vojtech Senkerik ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Injection Molding ◽  
Standardized Testing ◽  
Rubber Compound ◽  
Testing Sample ◽  
Synthetic Rubber ◽  
Injection Molded

The aim of this article is to demonstrate and asses to what extent there is an impact on the mechanical properties of a standardized testing sample made of rubber compound based on synthetic rubber EPDM and produced by injection molding in comparison with a sample produced by classic preparation (cutting off a compression molded plate) according to the standard ISO 23529.

scholarly journals Effects of Injection Molding Screw Tips on Polymer Mixing

2018 ◽  
Vol 62 (3) ◽  
pp. 241-246 ◽  
Author(s):  
Dániel Török ◽  
József Gábor Kovács
Keyword(s):  
Injection Molding ◽  
Processing Parameters ◽  
Raw Material ◽  
Molding Machine ◽  
Surface Color ◽  
Melt Temperature ◽  
Injection Molding Machine ◽  
Aesthetic Appearance ◽  
Molded Parts ◽  
Injection Molded

In all fields of industry it is important to produce parts with good quality. Injection molded parts usually have to meet strict requirements technically and aesthetically. The aim of the measurements presented in our paper is to investigate the aesthetic appearance, such as surface color homogeneity, of injection molded parts. It depends on several factors, the raw material, the colorants, the injection molding machine and the processing parameters. In this project we investigated the effects of the injection molding machine on surface color homogeneity. We focused on injection molding screw tips and investigated five screw tips with different geometries. We produced flat specimens colored with a masterbatch and investigated color homogeneity. To evaluate the color homogeneity of the specimens, we used digital image analysis software developed by us. After that we measured the plastication rate and the melt temperature of the polymer melt because mixing depends on these factors. Our results showed that the screw tips (dynamic mixers) can improve surface color homogeneity but they cause an increase in melt temperature and a decrease in the plastication rate.

Microstructure, Hardness, and Wear Resistance of Powder-Injection-Molded Products of Fe-Based Metamorphic Powders

2007 ◽  
Vol 26-28 ◽  
pp. 355-358
Author(s):  
Chang Kyu Kim ◽  
Chang Young Son ◽  
Dae Jin Ha ◽  
Tae Sik Yoon ◽  
Sung Hak Lee
Keyword(s):  
Mechanical Properties ◽  
Stainless Steel ◽  
Wear Resistance ◽  
Injection Molding ◽  
Powder Injection Molding ◽  
Powder Injection ◽  
Thermally Stable ◽  
Austenitic Matrix ◽  
Amorphous Phases ◽  
Injection Molded

Powder injection molding (PIM) process was applied to Fe-based metamorphic alloy powders, and microstructure, hardness, and wear resistance of the PIM products were analyzed and compared with those of conventional PIM stainless steel products. When Fe-based metamorphic powders were injection-molded and then sintered at 1200 oC, completely densified products with almost no pores were obtained. They contained 34 vol.% of (Cr,Fe)2B borides dispersed in the austenitic matrix without amorphous phases. Since these (Cr,Fe)2B borides were very hard and thermally stable, hardness, and wear resistance of the PIM products of Fe-based metamorphic powders were twice as high as those of conventional PIM stainless steel products. Such property improvement suggested new applicability of the PIM products of Fe-based metamorphic powders to structures and parts requiring excellent mechanical properties.

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