scholarly journals A Modified Method for Hardness Determination from Nanoindentation Experiments with Imperfect Indenters

2016 ◽  
Vol 2016 ◽  
pp. 1-8 ◽  
Author(s):  
Wei Chao Guo ◽  
Heng Xu ◽  
Xin Qin Gao ◽  
Xiao Li Hou ◽  
Yan Li
Keyword(s):  
Nondestructive Method ◽  
Experimental Investigations ◽  
Small Scale ◽  
New Approach ◽  
Modified Method ◽  
Properties Of Materials ◽  
Tip Radius ◽  
Hardness Values ◽  
Indenter Shape

Nanoindentation is an effective nondestructive method for small scale determination of mechanical properties of materials. However, indentation response of metallic materials is very sensitive to indenter tip roundness, size effects, loading rate, and so forth. This study will analyze the effect of indenter shape imperfections on hardness determination. For this purpose, experimental investigations and finite element simulations are carried out. At first, it is found that hardness values determined with Oliver and Pharr’s method are affected by errors caused by imperfect indenter tip: errors increase for imperfect indenters with larger tip radii. Afterwards, several commonly used methods accounting at different extents for tip radius variations are compared. However, most of those methods are found not to be accurate for shallow indentation. For this reason, a novel hardness determination method based on geometrical relations of the imperfect indenter tip is developed. Results show that the new approach is very effective even in the case of shallow indentation.

Determination of Contact Area During Small-Scale Friction Experiments by Means of Continuous Stiffness Measurements

2005 ◽  
Author(s):  
Andrei Rar ◽  
Yehuda Y. Braiman ◽  
Warren C. Oliver ◽  
David L. Goldsby ◽  
Terry E. Tullis ◽  
...  
Keyword(s):  
Linear Relationship ◽  
Friction Force ◽  
Direct Measurement ◽  
Contact Area ◽  
Dry Friction ◽  
Contact Stiffness ◽  
Small Scale ◽  
New Approach ◽  
Active Research

Despite the hallmark observation of the almost linear relationship between friction force and contact area in the case of “dry” friction, the direct measurement of this dependency is an area of active research [1, 2]. In this study, a new approach to the measurement of contact area during friction experiments is proposed. The method is based on the well known proportionality between the contact area and the contact stiffness raised to the second power [3]. The main benefit of the proposed method is its broad applicability. Preliminary measurements of the dependence between friction and contact area are discussed.

scholarly journals Analysis of the Generation of Vibration Signals under Uniaxial Loading of Materials Using the Coherent Properties of Laser Radiation

Materials ◽  
2020 ◽  
Vol 13 (9) ◽  
pp. 2046
Author(s):  
Petr Louda ◽  
Artem Sharko
Keyword(s):  
Strength Properties ◽  
Experimental Investigations ◽  
Strain Diagram ◽  
Physical Processes ◽  
Vibration Signals ◽  
Information Parameter ◽  
Vibrational Signals ◽  
Discrimination Level ◽  
Properties Of Materials

The present article describes the results of theoretical and experimental investigations of the force response of materials to external tensile stresses. The method used is based on remote precision measurements of the amplitudes of the harmonics of vibration signals and synchronous fixation of deformations under load. It was determined that the shape of the propagating acoustic signal depends not only on the bias time, but also on the frequency. In addition, fixation of the moments of occurrence of the vibrational signals and determination of the number of excesses in the amplitudes of harmonics over the discrimination level allows structural models to be studied in order to diagnose the strength properties of materials under dynamic loading of solids. The experimental setup consisted of a P100 Labtest-2 tearing machine providing a loading speed of 6.22 mm/min, a Polytech PSV–400 vibrometer including lasers, and a computer. Measurements were made at frequencies of 0.4, 1.6, and 40 kHz. An analysis of the mathematical models of the occurrence and propagation of acoustic signals in a material under load is presented, and the features of their application are reported. Transferring the moments of occurrence of vibrational signals to a strain diagram from the applied load allows the development of physical processes of hardening and destruction of materials to be traced. The occurrence of vibrational signals under load can be used as an information parameter for the diagnosis of developing defects in the structure of materials under load.

The Dudley Lee Case: A new approach to factual causation and its implications for transformative jurisprudence

2017 ◽  
Vol 30 (1) ◽  
pp. 273-289
Author(s):  
Anmari Meerkotter
Keyword(s):  
Case Note ◽  
Constitutional Court ◽  
Recent Contribution ◽  
New Approach ◽  
State Accountability ◽  
The Law ◽  
Transformative Impact ◽  
Constitutional Jurisprudence ◽  
Law Of Delict

The Constitutional Court (CC) judgment of Lee v Minister of Correction Services 2013 2SA 144 (CC) is a recent contribution to transformative constitutional jurisprudence in the field of the law of delict. This matter turned on the issue of factual causation in the context of wrongful and negligent systemic omissions by the state. In this case note, I explore the law relating to this element of delictual liability with specific regard to the traditional test for factual causation – the conditio sine qua non (‘but-for’) test. In particular, I note the problems occasioned by formalistic adherence to this test in the context of systemic state omissions as evidenced by the SCA judgment in the same matter. I also consider the manner in which English courts have addressed this problem. Thereafter, I analyse the CC’s broader approach to the determination of factual causation as one based on common sense and justice. I argue that this approach endorses a break from a formalistic application of the test and constitutes a step towards an approach which resonates with the foundational constitutional values of freedom, dignity and equality. Furthermore, it presents an appropriate solution to the problems associated with factual causation where systemic omissions are concerned. I then consider the transformative impact of the Lee judgment. In particular, I argue that the broader enquiry favoured by the CC facilitates the realisation of constitutionally guaranteed state accountability, and amounts to an extension of the existing norm of accountability jurisprudence. Hence, I contend that the judgment presents a further effort by the Constitutional Court to effect wholesale the constitutionalisation of the law of delict, as well as a vindicatory tool to be used by litigants who have been adversely affected by systemic state omissions.

Automatic Determination of Optimal FIB Operations for Improved Circuit Probing and Fast Reconfiguration

2000 ◽  
Author(s):  
Romain Desplats ◽  
Timothee Dargnies ◽  
Jean-Christophe Courrege ◽  
Philippe Perdu ◽  
Jean-Louis Noullet
Keyword(s):  
Integrated Circuit ◽  
Focused Ion Beam ◽  
Ion Beam ◽  
Semiconductor Devices ◽  
Front Side ◽  
Automatic Determination ◽  
Metal Line ◽  
New Approach ◽  
Metal Layers

Abstract Focused Ion Beam (FIB) tools are widely used for Integrated Circuit (IC) debug and repair. With the increasing density of recent semiconductor devices, FIB operations are increasingly challenged, requiring access through 4 or more metal layers to reach a metal line of interest. In some cases, accessibility from the front side, through these metal layers, is so limited that backside FIB operations appear to be the most appropriate approach. The questions to be resolved before starting frontside or backside FIB operations on a device are: 1. Is it do-able, are the metal lines accessible? 2. What is the optimal positioning (e.g. accessing a metal 2 line is much faster and easier than digging down to a metal 6 line)? (for the backside) 3. What risk, time and cost are involved in FIB operations? In this paper, we will present a new approach, which allows the FIB user or designer to calculate the optimal FIB operation for debug and IC repair. It automatically selects the fastest and easiest milling and deposition FIB operations.

Adaptation of the AOAC Fluorine Method for Determining Fluoride in Fish Protein Concentrate

1970 ◽  
Vol 53 (1) ◽  
pp. 3-6
Author(s):  
R. Bruce Klemm ◽  
Mary E. Ambrose Klemm
Keyword(s):  
Steam Distillation ◽  
Silica Sand ◽  
Official Method ◽  
Protein Concentrate ◽  
Fish Protein ◽  
Direct Titration ◽  
Modified Method ◽  
Aoac Official ◽  
Aoac Official Method

Abstract The AOAC official method, 24.029–24.035, for the determination of fluorine in foods was modified slightly to o btain quantitative recoveries of fluorine from samples of fish protein concentrate (FPC). The most important alterations include the use of steam distillation, the addition of finely ground silica sand in the distillation, a decrease in the distillation temperature, and the utilization of direct titration. Recoveries of fluoride added to FPC before ashing, using this modified method, averaged 96.0 ± 3.0%. Our results are in agreement with those of several other analysts who used a variety of methods.

scholarly journals New Method for Analysis of the Temporomandibular Joint Using Cone Beam Computed Tomography

Sensors ◽  
2021 ◽  
Vol 21 (9) ◽  
pp. 3070
Author(s):  
Sebastian Iwaszenko ◽  
Jakub Munk ◽  
Stefan Baron ◽  
Adam Smoliński
Keyword(s):  
Computed Tomography ◽  
Temporomandibular Joint ◽  
Cross Section ◽  
Cone Beam Computed Tomography ◽  
Cone Beam ◽  
Section Plane ◽  
New Approach ◽  
Volume Of Interest ◽  
Gap Width

Modern dentistry commonly uses a variety of imaging methods to support diagnosis and treatment. Among them, cone beam computed tomography (CBCT) is particularly useful in presenting head structures, such as the temporomandibular joint (TMJ). The determination of the morphology of the joint is an important part of the diagnosis as well as the monitoring of the treatment results. It can be accomplished by measurement of the TMJ gap width at three selected places, taken at a specific cross-section. This study presents a new approach to these measurements. First, the CBCT images are denoised using curvilinear methods, and the volume of interest is determined. Then, the orientation of the vertical cross-section plane is computed based on segmented axial sections of the TMJ head. Finally, the cross-section plane is used to determine the standardized locations, at which the width of the gap between condyle and fossa is measured. The elaborated method was tested on selected TMJ CBCT scans with satisfactory results. The proposed solution lays the basis for the development of an autonomous method of TMJ index identification.

scholarly journals A New Approach to Quantifying Bioaccumulation of Elements in Biological Processes

Biology ◽  
2021 ◽  
Vol 10 (4) ◽  
pp. 345
Author(s):  
Kinga Proc ◽  
Piotr Bulak ◽  
Monika Kaczor ◽  
Andrzej Bieganowski
Keyword(s):  
Element Concentration ◽  
Experimental System ◽  
Small Scale ◽  
New Approach ◽  
Realistic Situation ◽  
Initial Load ◽  
Test Elements ◽  
Organism Growth ◽  
Bioaccumulation Index ◽  
Phosphorous Concentration

Bioaccumulation, expressed as the bioaccumulation factor (BAF), is a phenomenon widely investigated in the natural environment and at laboratory scale. However, the BAF is more suitable for ecological studies, while in small-scale experiments it has limitations, which are discussed in this article. We propose a new indicator, the bioaccumulation index (BAI). The BAI takes into account the initial load of test elements, which are added to the experimental system together with the biomass of the organism. This offers the opportunity to explore the phenomena related to the bioaccumulation and, contrary to the BAF, can also reveal the dilution of element concentration in the organism. The BAF can overestimate bioaccumulation, and in an extremal situation, when the dilution of element concentration during organism growth occurs, the BAF may produce completely opposite results to the BAI. In one of the examples presented in this work (Tschirner and Simon, 2015), the concentration of phosphorous in fly larvae was lower after the experiment than in the younger larvae before the experiment. Because the phosphorous concentration in the feed was low, the BAF indicated a high bioaccumulation of this element (BAF = 14.85). In contrast, the BAI showed element dilution, which is a more realistic situation (BAI = −0.32). By taking more data into account, the BAI seems to be more valid in determining bioaccumulation, especially in the context of entomoremediation research.

Improved Method for the Determination of Ethylenebisdithiocarbamate Residues in Plants, Fruits, and Vegetables

1967 ◽  
Vol 50 (5) ◽  
pp. 1102-1108
Author(s):  
Charles F Gordon ◽  
Richard J Schuckert ◽  
William E Bornak
Keyword(s):  
Sulfuric Acid ◽  
Fruits And Vegetables ◽  
Analytical Procedure ◽  
Improved Method ◽  
Modified Method ◽  
Fungicide Residues ◽  
Crop Types ◽  
Large Representative

Abstract A modified method for the determination of dithiocarbamate fungicide residues on crops is presented. A large representative subsample of the frozen crop is blended in ice-cold deaerated water and an aliquot of the homogenate is added to the analytical apparatus containing hot 5 0% sulfuric acid. Dithiocarbamates are decomposed to evolve CS2 which is removed by a continuous gentle air-sweep from the digestion flask. Variations in technique allow the analysis of dithiocarbamate fungicide residues in several ranges, 1-10, 10-200, and 200-1000 /ig maneb. Recoveries from a wide variety of crops averaged 70 to 103%. Certain crop types present low recoveries and/or high apparent control values, but modifications in the analytical procedure are successful in solving these problems.

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