scholarly journals Changes in Nanoscaled Mechanical and Rheological Properties of Asphalt Binders Caused by Aging

2015 ◽  
Vol 2015 ◽  
pp. 1-6 ◽  
Author(s):  
Ben Liu ◽  
Junan Shen ◽  
Xuyan Song
Keyword(s):  
Thin Film ◽  
Atomic Force Microscope ◽  
Rheological Properties ◽  
Asphalt Binder ◽  
Adhesive Force ◽  
Asphalt Binders ◽  
Dynamic Shear ◽  
Short Term ◽  
Atomic Force ◽  
Aged Asphalt

Aging of an asphalt binder causes the changes in the microstructure and, consequently, in the nanomechanical and rheological properties of the aged asphalt binder. Short-term aging on asphalt binders was simulated using rotating thin film oven (RTFO). These changes in the microstructure and nanomechanical and rheological properties were measured using atomic force microscope (AFM) and dynamic shear rheometer (DSR). The results indicated that (1) the adhesive force of the asphalt binder from AFM tests was increased after RTFO aging; (2)G*of the asphalt binder from DSR tests increased after RTFO aging; (3) the results from AFM were consistent with those from DSR, explaining the mechanism of the changes of rheological properties.

scholarly journals Effects of WMA Additive on the Rheological Properties of Asphalt Binder and High Temperature Performance Grade

2015 ◽  
Vol 2015 ◽  
pp. 1-7 ◽  
Author(s):  
Jiupeng Zhang ◽  
Guoqiang Liu ◽  
Li Xu ◽  
Jianzhong Pei
Keyword(s):  
Critical Temperature ◽  
Rheological Properties ◽  
Asphalt Binder ◽  
Aging Effect ◽  
Asphalt Binders ◽  
Short Term ◽  
Performance Grade ◽  
Temperature Performance ◽  
Effects Of Temperature ◽  
Increasing Temperature

Sasobit additives with different dosages were added into 70# and 90# virgin asphalt binders to prepare WMA binders. The rheological properties, includingG∗andδ, were measured by using DSR at the temperature ranging from 46°C to 70°C, and the effects of temperature, additive dosage and aging onG∗/sin⁡δ, critical temperature, and H-T PG were investigated. The results indicate that WMA additive improvesG∗but reducesδ, and the improvement on 70# virgin binder is more significant.G∗/sin⁡δexponentially decreases with the increasing temperature but linearly increases with the increasing additive dosage. Aging effect weakens the interaction between binder and additive but significantly increases the binder’s viscosity; that is whyG∗/sin⁡δis higher after short-term aging. In addition, the critical temperature increases with the increasing additive dosage, and the additive dosage should be more than 3% and 5% to improve H-T PG by one grade for 70# and 90# virgin binder, respectively.

Effects of Aging on the Physical and Rheological Properties of Asphalt Binder Incorporating Rediset®

2014 ◽  
Vol 70 (7) ◽  
Author(s):  
Mohamad Yusri Aman ◽  
Zulkurnain Shahadan ◽  
Munzilah Md. Ruhani ◽  
Rosnawati Buhari
Keyword(s):  
Statistical Analysis ◽  
Rheological Properties ◽  
Asphalt Binder ◽  
Dynamic Shear ◽  
Short Term ◽  
Rotational Viscometer ◽  
Aging Index ◽  
Modified Binders ◽  
Before And After ◽  
Effects Of Aging

This paper focuses on physical and rheological properties of virgin asphalt binder blended with different percentage of Rediset® content. The rheological properties of the Rediset® modified binders were characterized before and after being subjected to short-term aging using rotational viscometer (RV) and dynamic shear rheometer (DSR) according to SuperpaveTM test protocols. The results indicated that the penetration and softening point were consistently decreased and increased, respectively for unaged and short-term aged samples. The penetration index (PI) and viscosity aging index (VAI) were increased as the Rediset® modified binders aged and showed a high significance correlation. The addition of Rediset® in asphalt binder exhibited change in binder rheology after subjected to short-term aged which influenced the rutting parameter. A statistical analysis showed that Rediset® used as warm asphalt additive had significantly increased the G*/Sin δ parameter which indicated greater resistance to rutting.

scholarly journals Characterizing the Diffusion and Rheological Properties of Aged Asphalt Binder Rejuvenated with Bio-Oil Based on Molecular Dynamic Simulations and Laboratory Experimentations

Molecules ◽  
2021 ◽  
Vol 26 (23) ◽  
pp. 7080
Author(s):  
Xiaorui Zhang ◽  
Chao Han ◽  
Xinxing Zhou ◽  
Frédéric Otto ◽  
Fan Zhang
Keyword(s):  
Soybean Oil ◽  
Rheological Properties ◽  
Chemical Structure ◽  
Asphalt Binder ◽  
Asphalt Binders ◽  
Dynamic Simulations ◽  
Bio Oil ◽  
Aged Asphalt ◽  
Complex Shear ◽  
Potential Use

Soybean-derived bio-oil is one of the vegetable-based oils that is gaining the most interest for potential use in the rejuvenation of aged asphalt binders. This laboratory study was conducted to characterize and quantify the diffusion and rheological properties of bio-oil-rejuvenated aged asphalt binder (BRAA) using soybean oil. In the study, the chemical structure of the soybean oil was comparatively characterized using an element analyzer (EA), gel permeation chromatography (GPC), and a Fourier infrared (FTIR) spectrometer, respectively. Based on the chemical structure of the bio-oil, BRAA molecular models were built for computing the diffusion parameters using molecular dynamic simulations. Likewise, a dynamic shear rheometer (DSR) test device was used for measuring and quantifying the rheological properties of the aged asphalt binder rejuvenated with 0%, 1%, 2%, 3%, 4%, and 5% soybean oil, respectively. The laboratory test results indicate that bio-oil could potentially improve the diffusion coefficients and phase angle of the aged asphalt binder. Similarly, the corresponding decrease in the complex shear modulus has a positive effect on the low-temperature properties of BRAA. For a bio-oil dosage 4.0%, the diffusion coefficients of the BRAA components are 1.52 × 10−8, 1.33 × 10−8, 3.47 × 10−8, 4.82 × 10−8 and 3.92 × 10−8, respectively. Similarly, the corresponding reduction in the complex shear modulus from 1.27 × 107 Pa to 4.0 × 105 Pa suggests an improvement in the low-temperature properties of BRAA. Overall, the study contributes to the literature on the potential use of soybean-derived bio-oil as a rejuvenator of aged asphalt binders.

Rejuvenation of short-term aged asphalt-binder using waste engine oil

2020 ◽  
Vol 47 (7) ◽  
pp. 822-832 ◽  
Author(s):  
Tao Bai ◽  
Zi-ang Hu ◽  
Xiaodi Hu ◽  
Yang Liu ◽  
Luis Fuentes ◽  
...  
Keyword(s):  
Asphalt Binder ◽  
Engine Oil ◽  
Morphological Properties ◽  
Asphalt Binders ◽  
Test Results ◽  
Short Term ◽  
Waste Engine Oil ◽  
Laboratory Test Results ◽  
Aged Asphalt ◽  
Significant Milestone

The work presented in this paper aims to improve the rheological properties and ductility characteristics of aged (short-term) asphalt-binder using waste engine oil (WEO). The WEO was injected into the aged asphalt-binder as three rejuvenators, namely A, B, and C — with Rejuvenator A being the treated WEO only. Rejuvenator B consists of treated WEO and furfural extraction oil. Rejuvenator C consists of Rejuvenator B composition plus epoxy resin. The asphalt-binder physical, ductility, rheological, and morphological properties were measured using the standard penetration, softening point, ductility, dynamic shear rheometer, bending beam rheometer, and Fourier transform infrared spectroscopy tests, respectively. Overall, the laboratory test results, with Rejuvenator C exhibiting superiority, indicated that, if properly preprocessed and treated with additive modifications, WEO can be beneficially used to rejuvenate short-term aged asphalt-binders, which can be a significant milestone towards “green” asphalt and environmental conservatism.

Modelling short-term aging of asphalt binders using the rolling thin film oven test

2002 ◽  
Vol 29 (1) ◽  
pp. 135-144 ◽  
Author(s):  
Ahmed Shalaby
Keyword(s):  
Thin Film ◽  
Shear Modulus ◽  
Phase Angle ◽  
Asphalt Binder ◽  
Temperature Shift ◽  
Test Methods ◽  
Asphalt Binders ◽  
Aging Effects ◽  
Short Term ◽  
Oven Test

Simulation of short-term aging of asphalt binders is a widely used procedure in asphalt binder characterization for predicting the binder response to plant mixing and paving under controlled laboratory conditions. There are two laboratory test methods for evaluating the short-term aging of asphalt binders: (i) a method using rotating pans filled with a thin asphalt film termed thin film oven test (TFOT) and (ii) a method using rolling cylindrical asphalt containers termed rolling thin film oven test (RTFOT). In this paper, an attempt is made to develop generalized models for short-term aging effects using the RTFOT aging time as a benchmark. Six binder types representing two PG grades and three source suppliers are conditioned to varying levels of RTFOT aging and tested using the dynamic shear rheometer (DSR). Aging effects are modelled using independent temperature shift models for the shear modulus and phase angle. The paper discusses the sources of errors in producing generalized models and some potential applications of aging models. The research revealed that it is possible to develop and implement such models for unmodified binders.Key words: asphalt, aging, RTFOT, DSR, binder rheology, shear modulus, phase angle.

Effects of Preheating on the Rheological Properties of Rejuvenated Asphalt Binder

2019 ◽  
Vol 2673 (4) ◽  
pp. 546-557 ◽  
Author(s):  
Yang Liu ◽  
Hainian Wang ◽  
Susan Tighe ◽  
Guangyuan Zhao ◽  
Zhanping You
Keyword(s):  
Rheological Properties ◽  
Asphalt Pavement ◽  
Asphalt Binder ◽  
Fatigue Properties ◽  
Dynamic Shear ◽  
Recycled Asphalt ◽  
Reclaimed Asphalt ◽  
Aged Asphalt ◽  
Asphalt Materials

Hot in-place recycling (HIR) is a process that reuses reclaimed asphalt materials to benefit the environment and conserve natural resources. HIR has not yet been widely applied in China because of technical drawbacks such as reclaimed materials’ fatigue properties and poor cracking resistance. Preheating is the first procedure in HIR and significantly affects the diffusion of rejuvenators within the aged asphalt and the remixing of virgin and aged mixtures. This study focuses on the effects of preheating on the rheological properties of rejuvenated asphalt binder using dynamic shear rheometer (DSR) testing. Three types of rejuvenators (Reju-A, Reju-B and Reju-C), three types of base asphalt binder (#50, #70, and #90), recovered asphalt from recycled asphalt pavement, and laboratory-aged asphalt were investigated to analyze the rheological properties under different heating conditions. The results show that (1) rejuvenators contain little in the way of viscous characteristics and have a viscosity-reducing effect on aged asphalt; (2) field-aged asphalt loses cohesion and gains rutting resistance during aging; and (3) preheating has a significant effect on diffusion of rejuvenators within aged asphalt as well as on rheological properties. In short, a good controlled preheating operation is critical to the quality of the asphalt rejuvenation process.

Graphite Particle Adhesion to Hastelloy X: Measurements of the Adhesive Force with an Atomic Force Microscope

2014 ◽  
Vol 186 (1) ◽  
pp. 45-59 ◽  
Author(s):  
Naphtali M. Mokgalapa ◽  
Tushar K. Ghosh ◽  
Sudarshan K. Loyalka
Keyword(s):  
Atomic Force Microscope ◽  
Graphite Particle ◽  
Adhesive Force ◽  
Particle Adhesion ◽  
Hastelloy X ◽  
Atomic Force

Anin situatomic force microscope for normal-incidence nanofocus X-ray experiments

2016 ◽  
Vol 23 (5) ◽  
pp. 1110-1117 ◽  
Author(s):  
M. V. Vitorino ◽  
Y. Fuchs ◽  
T. Dane ◽  
M. S. Rodrigues ◽  
M. Rosenthal ◽  
...  
Keyword(s):  
Thin Film ◽  
Atomic Force Microscope ◽  
High Speed ◽  
Normal Incidence ◽  
Organic Thin Film ◽  
X Ray ◽  
Atomic Force ◽  
Synchrotron Beamlines

A compact high-speed X-ray atomic force microscope has been developed forin situuse in normal-incidence X-ray experiments on synchrotron beamlines, allowing for simultaneous characterization of samples in direct space with nanometric lateral resolution while employing nanofocused X-ray beams. In the present work the instrument is used to observe radiation damage effects produced by an intense X-ray nanobeam on a semiconducting organic thin film. The formation of micrometric holes induced by the beam occurring on a timescale of seconds is characterized.

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