scholarly journals Surface Modified Characteristics of the Tetracalcium Phosphate as Light-Cured Composite Resin Fillers

2014 ◽  
Vol 2014 ◽  
pp. 1-9
Author(s):  
Wen-Cheng Chen ◽  
Chia-Ling Ko ◽  
Chi-Jen Shih
Keyword(s):  
Thermal Cycling ◽  
Composite Resin ◽  
Composite Resins ◽  
Control Group ◽  
Tetracalcium Phosphate ◽  
Before And After ◽  
External Forces ◽  
Surface Modified ◽  
Dental Restorative ◽  
Diametral Tensile Strength

The objectives of this study are to characterize the properties of light-cured composite resins that are reinforced with whisker surface-modified particles of tetracalcium phosphate (TTCP) and to investigate the influence of thermal cycling on the reinforced composites properties. The characteristics of ultimate diametral tensile strength (DTS), moduli, pH values, and fracture surfaces of the samples with different amounts of surface-modified TTCP (30%–60%) were determined before and after thermal cycling between 5°C and 55°C in deionized water for 600 cycles. The trends of all groups were ductile prior to thermal cycling and the moduli of all groups increased after thermal cycling. The ductile property of the control group without filler was not significantly affected. Larger amounts of fillers caused the particles to aggregate, subsequently decreasing the resin’s ability to disperse external forces and leading to brittleness after thermal cycling. Therefore, the trend of composite resins with larger amounts of filler would become more brittle and exhibited higher moduli after thermal cycling. This developed composite resin with surface modified-TTCP fillers has the potential to be successful dental restorative materials.

Influence of Hydrogen Peroxide Bleaching Gels on Color, Opacity, and Fluorescence of Composite Resins

2012 ◽  
Vol 37 (5) ◽  
pp. 526-531 ◽  
Author(s):  
CRG Torres ◽  
CF Ribeiro ◽  
E Bresciani ◽  
AB Borges
Keyword(s):  
Hydrogen Peroxide ◽  
Composite Resin ◽  
Color Change ◽  
Composite Resins ◽  
Control Group ◽  
Peroxide Bleaching ◽  
Color Changes ◽  
Tukey Test ◽  
Bleaching Gels ◽  
Bleaching Treatment

SUMMARY The aim of the present study was to evaluate the effect of 20% and 35% hydrogen peroxide bleaching gels on the color, opacity, and fluorescence of composite resins. Seven composite resin brands were tested and 30 specimens, 3-mm in diameter and 2-mm thick, of each material were fabricated, for a total of 210 specimens. The specimens of each tested material were divided into three subgroups (n=10) according to the bleaching therapy tested: 20% hydrogen peroxide gel, 35% hydroxide peroxide gel, and the control group. The baseline color, opacity, and fluorescence were assessed by spectrophotometry. Four 30-minute bleaching gel applications, two hours in total, were performed. The control group did not receive bleaching treatment and was stored in deionized water. Final assessments were performed, and data were analyzed by two-way analysis of variance and Tukey tests (p<0.05). Color changes were significant for different tested bleaching therapies (p<0.0001), with the greatest color change observed for 35% hydrogen peroxide gel. No difference in opacity was detected for all analyzed parameters. Fluorescence changes were influenced by composite resin brand (p<0.0001) and bleaching therapy (p=0.0016) used. No significant differences in fluorescence between different bleaching gel concentrations were detected by Tukey test. The greatest fluorescence alteration was detected on the brand Z350. It was concluded that 35% hydrogen peroxide bleaching gel generated the greatest color change among all evaluated materials. No statistical opacity changes were detected for all tested variables, and significant fluorescence changes were dependent on the material and bleaching therapy, regardless of the gel concentration.

scholarly journals Effect of whitening dentifrices on the surface roughness of a nanohybrid composite resin

2016 ◽  
Vol 10 (02) ◽  
pp. 170-175 ◽  
Author(s):  
Gabriela Migliorin da Rosa ◽  
Luciana Mendonça da Silva ◽  
Márcio de Menezes ◽  
Hugo Felipe do Vale ◽  
Diego Ferreira Regalado ◽  
...  
Keyword(s):  
Surface Roughness ◽  
Composite Resin ◽  
Wilcoxon Test ◽  
Control Group ◽  
Mean Values ◽  
Short Period ◽  
Significant Difference ◽  
Before And After ◽  
Nanohybrid Composite ◽  
One Way Anova

ABSTRACT Objectives: The present study verified the influence of whitening dentifrices on the surface roughness of a nanohybrid composite resin. Materials and Methods: Thirty-two specimens were prepared with Filtek™ Z350 XT (3M/ESPE) and randomly divided into four groups (n = 08) that were subjected to brushing simulation equivalent to the period of 1 month. The groups assessed were a control group with distilled water (G1), Colgate Total 12 Professional Clean (G2), Sensodyne Extra Whitener Extra Fresh (G3), and Colgate Luminous White (G4). A sequence of 90 cycles was performed for all the samples. The initial roughness of each group was analyzed by the Surface Roughness Tester (TR 200-TIME Group Inc., CA, USA). After the brushing period, the final roughness was measured, and the results were statistically analyzed using nonparametric Kruskal–Wallis and Dunn tests for intergroup roughness comparison in the time factor. For intragroup and “Δ Final − Initial” comparisons, the Wilcoxon test and (one-way) ANOVA were, respectively, performed (α = 0.05). Results: The roughness mean values before and after brushing showed no statistically significant difference when the different dentifrices were used. None of the dentifrices analyzed increased significantly the nanohybrid composite resin surface roughness in a 1 month of tooth brushing simulation. Conclusions: These results suggest that no hazardous effect on the roughness of nanohybrid composite resin can be expected when whitening dentifrices are used for a short period. Similar studies should be conducted to analyze other esthetic composite materials.

scholarly journals Effect of thermal cycling and filling technique on leakage of composite resin restorations

2004 ◽  
Vol 12 (4) ◽  
pp. 307-311 ◽  
Author(s):  
Silvia Kenshima ◽  
Rosa Helena Miranda Grande ◽  
Julio da Motta Singer ◽  
Rafael Yagüe Ballester
Keyword(s):  
Thermal Cycling ◽  
Silver Nitrate ◽  
Composite Resin ◽  
Composite Resins ◽  
Fluorescent Light ◽  
Single Bond ◽  
Class V ◽  
Composite Resin Restorations ◽  
Nail Varnish

The objective of this study was to evaluate in vitro the effect on leakage of two incremental filling techniques and two composite resins with different elastic modulus and similar polymerization shrinkage. Eighty Class V cavities (4x4x2mm) were prepared in bovine incisors and were randomly restored with Z-250 (Z) or Durafill VS (D) + Single Bond in axial (a) or oblique (o) increments. The restorations were divided into two groups: Not Aged - N (4-hour-storage in water at 37ºC) and Aged - A (1-week storage in water at 37ºC + 1000 x - 5º-55ºC / 1-min dwell time). The specimens were covered with 2 coats of nail varnish so that only the restoration margins were exposed to silver nitrate 50% (2h) and developed under fluorescent light (8h). After they were sectioned twice in buccal-lingual direction, the four exposed surfaces were digitized (Vidcap) and the silver nitrate penetration was measured (ImageLab) at the incisal and gingival walls. Data were analyzed by a 3-way ANOVA (Resin, Filling Technique and Aging) separately for incisal and gingival walls (alpha=0.05). Resin and Aging were statistically significant either for the incisal and the gingival walls. The microfill composite resin infiltrated more than the hybrid composite. The thermal cycling caused an overall increase in silver nitrate penetration. The filling technique affected leakage depending on the composite resin and aging regimen.

scholarly journals Effect of irradiation mode and filling technique on resin/dentin bonding strength in class I cavities

2004 ◽  
Vol 18 (3) ◽  
pp. 260-265 ◽  
Author(s):  
Alex José Souza dos Santos ◽  
Marcelo Giannini ◽  
Luis Alexandre Maffei Sartini Paulillo ◽  
José Roberto Lovadino ◽  
Ricardo Marins de Carvalho
Keyword(s):  
Bonding Strength ◽  
Composite Resin ◽  
Composite Resins ◽  
Class I ◽  
Control Group ◽  
Human Teeth ◽  
Dentin Bonding ◽  
Soft Start ◽  
Microtensile Testing ◽  
Dunnett's Test

Factors such as light-curing mode, filling technique and cavity configuration may affect the bonding strength to dentin. This study evaluated the effect of irradiation mode and filling technique on resin/dentin bonding strength on the buccal wall of class I cavities in human teeth. Occlusal enamel was removed to expose a flat dentin surface. Occlusal cavities (4 x 3 x 3 mm) were prepared in dentin. The adhesive Single Bond was applied according to the manufacturer's instructions and TPH Spectrum composite resin was placed using the following: oblique incremental, horizontal incremental or bulk filling techniques. The composite resin was light-cured either by continuous (600 mW/cm² for 40 s) or Soft-Start (250 mW/cm² for 10 s + 600 mW/cm² for 30 s) modes. Specimens of the control group were obtained by bonding the material to the flat exposed buccal wall of the cavity (C-factor = 1). The teeth were stored in water at 37ºC for 24 h and prepared for microtensile testing. Bonded beams of approximately 0.8 mm² were obtained from the buccal wall and tested with a tension of 0.5 mm/min. Results were analyzed by two-way ANOVA, Tukey's test and Dunnett's test (alpha = 0.05). Incremental placement techniques with both irradiation modes produced higher bonding strength values than the bulk technique (p < 0.05). Bonding strength tested in the cavities had lower values than those obtained in flat dentin surfaces (control group) (p < 0.05), except for incremental fillings using stepped irradiation. Bonding strength to the cavity walls depends on the filling technique and on the irradiation mode of composite resins.

scholarly journals Pengaruh kopi arabika terhadap perubahan warna resin komposit hybrid

e-GIGI ◽  
2017 ◽  
Vol 5 (1) ◽  
Author(s):  
Style V. Sirang ◽  
P. S. Anindita ◽  
. Juliatri
Keyword(s):  
Hybrid Composite ◽  
Composite Resin ◽  
Composite Resins ◽  
Control Group ◽  
Control Group Design ◽  
Arabica Coffee ◽  
Group Design ◽  
Hybrid Type ◽  
Post Test ◽  
One Way Anova

Abstract: Composite resin is one of the restorations used in the field of dentistry due to its good esthetic property. To date, the most commonly used composite resin is the hybrid type. Its weakness is the nature of fluid absorbance that can change its color. This discoloration can caused inter alia by food and beverage consumption. Arabica coffee is mostly consumed by our society, however, it has deposit of chlorogenic acid that might cause discoloration. This study was aimed to assess the influence of arabica coffee to the discoloration of hybrid composite resins. This was a true experimental study with a pre test and post test only control group design. Total samples were 24 composite resins of hybrid type (diameter 5 mm and height 2 mm). Each treatment group consisted of 6 samples. The samples were divided into 4 treatment groups, as follows: 0 day, 3 days, 5 days, and 7 days of immersion in arabica coffee solution. The one-way anova test showed that the influence of arabica coffee solution to discoloration of composite resins was significant (p=0.00). Conclusion: There was a significant influence of the duration of immersion in arabica coffee to discoloration of hybrid composite resinsKeywords: resin composite, discoloration, arabica coffee Abstrak: Resin komposit merupakan salah satu bahan restorasi yang sering digunakan di bidang kedokteran gigi karena memiliki nilai estetik yang baik. Saat ini jenis resin komposit yang sering digunakan yaitu resin komposit tipe hybrid. Resin komposit memiliki kekurangan yaitu sifat absorbansi cairan yang dapat menyebabkan perubahan warna. Salah satu penyebab perubahan warna yaitu makanan dan minuman. Kopi arabika merupakan minuman yang sering dikonsumsi oleh masyarakat dan memiliki kandungan asam klorogenik yang dapat memengaruhi perubahan warna. Penelitian ini bertujuan untuk mengetahui pengaruh kopi arabika terhadap perubahan warna resin komposit hybrid. Jenis penelitian ialaj eksperimental murni dengan pre test dan post test only control group design. Jumlah sampel penelitian yaitu 24 resin komposit tipe hybrid dengan ukuran diameter 5 mm dan tinggi 2 mm, dibagi dalam tiga kelompok. Masing-masing kelompok perlakuan terdiri dari 6 sampel. Sampel dibagi menjadi 4 kelompok yaitu kelompok perlakuan 0 hari, 3 hari, 5 hari, dan 7 hari perendaman dalam larutan kopi arabika. Hasil analisis data dengan uji one way Anova menunjukkan adanya pengaruh kopi arabika terhadap perubahan warna resin komposit (p=0,00). Simpulan: Terdapat pengaruh bermakna dari lama perendaman dalam kopi arabika terhadap perubahan warna resin komposit hybrid. Kata kunci : resin komposit, perubahan warna, kopi arabika

Influence of Different Cordless Light-emitting-diode Units and Battery Levels on Chemical, Mechanical, and Physical Properties of Composite Resin

2019 ◽  
Vol 45 (4) ◽  
pp. 377-386 ◽  
Author(s):  
IO Cardoso ◽  
AC Machado ◽  
DNR Teixeira ◽  
FC Basílio ◽  
A Marletta ◽  
...  
Keyword(s):  
Tensile Strength ◽  
Physical Properties ◽  
Composite Resin ◽  
Light Emitting Diode ◽  
Pearson Correlation ◽  
Composite Resins ◽  
Degree Of Conversion ◽  
Light Emitting ◽  
Mechanical And Physical Properties ◽  
Diametral Tensile Strength

Clinical Relevance Irradiance may decrease as the light-emitting diode (LED) is discharged. Therefore, the LED must be charged carefully to prevent the possibility of influencing the chemical, mechanical, and physical properties of composite resin. SUMMARY The aim of this study was to evaluate the influence of different light-emitting diode (LED) curing units and battery levels on the chemical, mechanical, and physical properties of composite resins. The irradiance for each cycle from full to completely discharged battery level was evaluated, for five different new cordless LED units: Optilight Color (Gnatus), Bluephase (Ivoclar), Valo (Ultradent), Radii Plus (SDI), and Radii Xpert (SDI). After the irradiance evaluation, composite resin specimens were prepared and light cured, while varying the battery level for each LED unit: high level (HL, 100%), medium level (ML, 50%), and low level (LL, 10%). The degree of conversion, diametral tensile strength, sorption, and solubility were also evaluated. Data were checked for homoscedasticity and submitted to two-way and three-way analysis of variance, depending on the test performed, followed by the Tukey test with a significance level of 95%. A negative correlation was found between irradiance and cycles of light curing, which was checked by the Pearson correlation test. Valo and Radii Xpert were not influenced by the battery level in any test performed. However, different battery levels for some LED units can influence the degree of conversion, diametral tensile strength, sorption, and solubility of composite resins.

scholarly journals Bond Strength Evaluation of Bulk- fill Composites to Dentin Under Different Surface Treatments

2020 ◽  
pp. 194-207
Author(s):  
Kazım Bas ◽  
Ebru Uslu Cender
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Composite Resin ◽  
Surface Preparation ◽  
Acid Group ◽  
High Viscosity ◽  
Composite Resins ◽  
Control Group ◽  
Significant Difference

Purpose: The aim of this study is to compare the shear bond strength of three high-viscosity bulk-fill composite resins applied as single layers of 4mm thickness and of one microhybrid composite resin applied incrementally with a thickness of 2mm on dentin surfaces prepared with different surface preparation methods. Materials and Methods: A total of 132 caries-free human molars whose dentines had been exposed were used. Three groups, each containing 44 teeth, were formed. The acid group was etched with 32% phosphoric acid; laser group was etched with Er, Cr; YSGG laser and the control group was prepared with silicon carbid paper. Following the application of bonding agent, composite resin materials were applied on teeth using teflon moulds of 4x4mm. The samples were then subjected to shear bond strength tests. Two-way variance analysis and Tukey HSD multiple comparison test were applied on collected data. Results: There was a significant difference between surface treatment methods used regarding shear bond strength (P<0.001). The highest shear bond strength values were detected in the “Acid” group while the lowest shear bond strength values were detected in the “control” group. On the other hand, there was no statistically significant difference among composite resins (P>0.05). Conclusions: Laser etching of the dentin tissues is not as effective as acid etching. Bulk-fill composites had similar effects compared with conventional composite resins with regard to bonding strength. More in vitro studies supported with clinical data are required to investigate the performance of bulk-fill composites and laser.

Effect of Thermal Cycling Aging on the Surface Microhardness and Roughness of Resin-Infiltrated Enamel Lesions

2021 ◽  
Vol 13 (3) ◽  
pp. 356-363
Author(s):  
Yu Wu Su ◽  
Chao Zhang ◽  
Shan Shan Liu ◽  
Liang Yue Pang ◽  
Huan Cai Lin ◽  
...  
Keyword(s):  
Surface Roughness ◽  
Thermal Cycling ◽  
Control Group ◽  
Surface Microhardness ◽  
Suitable Material ◽  
Resin Infiltration ◽  
Enamel Caries ◽  
Caries Model ◽  
Before And After ◽  
Infiltrant Resin

With the widespread use of resin infiltration, its properties have drawn increasing attention. The objective of this study was to investigate the effect of resin infiltration on the surface microhardness and roughness of enamel lesions after thermal cycling aging. Tooth blocks were made from extracted premolars and placed into a control group, resin-infiltrated group or demineralized group. Before and after the aging procedure, the surface microhardness and surface roughness was measured. Before the aging procedure, the surface microhardness of the control group, resin-infiltrated group and demineralized group was 302.14 (±9.77) HV, 146.62 (±8.22) HV, and 28.85 (±2.21) HV (p 0.001), respectively. After the aging procedure, the surface microhardness of the control group, resin-infiltrated group and demineralized group decreased by 9.42%, 16.59%, and 20.75% ( p 0.001), respectively. Before the aging procedure, the surface roughness of the control group, resin-infiltrated group and demineralized group was 0.29 (±0.04) μm, 0.32 (±0.04) μm, and 0.39 (±0.07) μm (p = 0.009), respectively. After the aging procedure, the surface roughness of the control group, resin-infiltrated group and demineralized group increased by 9.85%, 8.31%, and 17.37% (p = 0.634), respectively. Resin infiltration can improve the surface microhardness and surface roughness of demineralized teeth in an artificial enamel caries model. The treatment also shows good aging resistance after thermal cycling. The infiltrant resin provided a suitable material for early enamel caries.

The Effect of Finishing and Polishing Procedures on the Surface Roughness of Composite Resin Materials

2007 ◽  
Vol 8 (1) ◽  
pp. 27-35 ◽  
Author(s):  
Nuray Attar
Keyword(s):  
Surface Roughness ◽  
Composite Resin ◽  
Resin Composite ◽  
Composite Resins ◽  
Control Group ◽  
Surface Groups ◽  
Average Roughness ◽  
Strip Surface ◽  
Polishing Procedures ◽  
Surface Sealant

Abstract Aims The aims of this study were to evaluate the effect of various finishing and polishing procedures on the surface roughness of six different composite resin materials (Artemis Enamel, TPH Spectrum, Filtek A–110, Filtek Supreme Enamel, Solitaire 2, and Filtek P–60) as well as to evaluate the effectiveness of the surface sealant application (BisCover) on the surface roughness after finishing and polishing procedures of tested composites. Methods and Materials Specimens (n=168) measuring 5 mm in diameter x 2 mm in thickness were fabricated in a plexiglass well covered with a Mylar strip using six composite resins. A control group of seven specimens of each material received no polishing after being cured under the Mylar strip. Twenty-one specimens for each composite were randomly divided among three finishing and polishing groups (n=7). Each group was polished using a different system: Carbide bur/Sof-Lex disc, Carbide bur/Enhance disc with polishing paste, and Carbide bur/Edenta composite finishing kit. The average surface roughness (Ra, ìm) of the control and treated specimens were measured with the Mitutoyo Surftest–402 Surface Roughness tester. After a surface sealant (BisCover) was applied to all treated specimens, according to manufacturer's instructions, the average roughness (Ra) was measured again. Results were statistically analyzed using analysis of variance (ANOVA) and the post-hoc Scheffe's test at a p<0.05 significance level. Results Significant differences were found for the surface roughness (p<0.05) with interaction among composite resins and the finishing systems used (p<0.05). Enhance/Biscover finishing and polishing procedure surface was not significantly different from the Mylar strip surface groups (p>0.05). The Mylar strip group was not significantly different from the Sof-Lex/BisCover and Edenta/BisCover groups. The ranking of mean Ra values by materials was as follows: Filtek Supreme Enamel < Filtek A110 < TPH Spectrum < Artemis <Filtek P–60 < Solitaire 2. The ranking of mean Ra values by polishing systems was as follows: Enhance/BisCover < Mylar Strip < Sof-Lex/BisCover < Edenta/BisCover < Sof-Lex < Enhance < Edenta. Conclusion Smoother surfaces were recorded for the Enhance/BisCover and the Mylar strip-formed surface groups. The composite finishing kit Edenta significantly increased the Ra for all tested composites (p<0.05). But after finishing with Edenta, the use of a surface sealant (BisCover) significantly improved the surface smoothness of all tested composites (p<0.05). Use of BisCover surface sealant on anterior and posterior resin composite restorations after finishing and polishing procedures is recommended. Citation Attar N. The Effect of Finishing and Polishing Procedures on the Surface Roughness of Composite Resin Materials. J Contemp Dent Pract 2007 January;(8)1:027-035.

Effect of Preheating and Fatiguing on Mechanical Properties of Bulk-fill and Conventional Composite Resin

2019 ◽  
Vol 45 (4) ◽  
pp. 387-395
Author(s):  
AA Abdulmajeed ◽  
TE Donovan ◽  
R Cook ◽  
TA Sulaiman
Keyword(s):  
Mechanical Properties ◽  
Fracture Toughness ◽  
Tensile Strength ◽  
Elastic Modulus ◽  
Flexural Strength ◽  
Composite Resin ◽  
Statistical Significance ◽  
Composite Resins ◽  
Significant Difference ◽  
Diametral Tensile Strength

Clinical Relevance Bulk-fill composite resins may have comparable mechanical properties to conventional composite resin. Preheating does not reduce the mechanical properties of composite resins. SUMMARY Statement of Problem: Bulk-fill composite resins are increasingly used for direct restorations. Preheating high-viscosity versions of these composites has been advocated to increase flowability and adaptability. It is not known what changes preheating may cause on the mechanical properties of these composite resins. Moreover, the mechanical properties of these composites after mastication simulation is lacking. Purpose: The purpose of this study was to evaluate the effect of fatiguing and preheating on the mechanical properties of bulk-fill composite resin in comparison to its conventional counterpart. Methods and Materials: One hundred eighty specimens of Filtek One Bulk Fill Restorative (FOBR; Bulk-Fill, 3M ESPE) and Filtek Supreme Ultra (FSU; Conventional, 3M ESPE) were prepared for each of the following tests: fracture toughness (International Organization for Standardization, ISO 6872), diametral tensile strength (No. 27 of ANSI/ADA), flexural strength, and elastic modulus (ISO Standard 4049). Specimens in the preheated group were heated to 68°C for 10 minutes and in the fatiguing group were cyclically loaded and thermocycled for 600,000 cycles and then tested. Two-/one-way analysis of variance followed by Tukey Honest Significant Difference (HSD) post hoc test was used to analyze data for statistical significance (α=0.05). Results: Preheating and fatiguing had a significant effect on the properties of both FSU and FOBR. Fracture toughness increased for FOBR specimens when preheated and decreased when fatigued (p=0.016). FOBR had higher fracture toughness value than FSU. Diametral tensile strength decreased significantly after fatiguing for FSU (p=0.0001). FOBR had a lower diametral tensile strength baseline value compared with FSU (p=0.004). Fatiguing significantly reduced the flexural strength of both FSU and FOBR (p=0.011). Preheating had no effect on the flexural strength of either FSU or FOBR. Preheating and fatiguing significantly decreased the elastic modulus of both composite resins equally (p&gt;0.05). Conclusions: Preheating and fatiguing influenced the mechanical properties of composite resins. Both composites displayed similar mechanical properties. Preheating did not yield a major negative effect on their mechanical properties; the clinical implications are yet to be determined.

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