scholarly journals Post-Heat Treatment and Mechanical Assessment of Polyvinyl Alcohol Nanofiber Sheet Fabricated by Electrospinning Technique

2014 ◽  
Vol 2014 ◽  
pp. 1-6 ◽  
Author(s):  
Mahir Es-saheb ◽  
Ahmed Elzatahry

Polyvinyl alcohol (PVA) sheets based nanofibers were produced by electrospinning technique. Postheat treatment of the produced PVA sheets with temperatures both below and above Tg to improve the mechanical properties of this material is conducted. The morphology, microstructures, and thermal degradation of the nanofibers sheets produced were investigated using scanning electron microscopy (SEM), transmission electron microscope (TEM), and thermal gravimetric analysis (TGA). Produced nanofibers are compact, and entangled with each other, with diameters from around 150 to 210. Some mechanical characteristics of the successfully produced PVA sheets, and heat-treated, are then conducted and assessed employing uniaxial tensile tests at different speeds ranging from 1 mm/min to 100 mm/min. The tensile test results obtained show that the PVA sheets are strain rate sensitive with increasing strength as the speed (i.e., strain rate) increases. The yield tensile stress ranges from 2.411 to 6.981 MPa, the ductility (i.e., elongation percent) from∼21 to 60%, and Young modulus ranges from 103 to 0.137 KPa. However, for heat-treated samples, it is found that the yield strength increases almost by∼35–40% more than the values of untreated cases with values reaching up to about 3.627–9.63 MPa.

2017 ◽  
Vol 52 (4) ◽  
pp. 226-238 ◽  
Author(s):  
Johanna Eisenträger ◽  
Konstantin Naumenko ◽  
Holm Altenbach ◽  
Elisabetta Gariboldi

This article aims to analyse the influence of temperature and strain rate on the mechanical behaviour of the high-chromium martensitic steel X20CrMoV12-1. The analysis is based on two series of high-temperature uniaxial tensile tests. In a first series, the tensile tests are conducted until rupture, and temperature as well as strain rate are varied systematically. The corresponding stress–strain curves show an extended softening stage. In order to examine softening, it is crucial to distinguish between microstructural changes and strain localisation due to necking. For this reason, a tensile test at low strain rate is performed several times, while the test is terminated at different strain levels in order to examine the onset of necking. Based on the test results and surface measurements of the deformed specimens, the strain level at which necking starts is determined, and possible interactions between softening and necking are discussed. The tensile tests have been conducted in order to calibrate a mechanical model which supplies reliable predictions on the material behaviour under different loading scenarios at elevated temperatures. For this reason, a framework based on microstructural processes is presented in the second part of the article. The model applies a binary mixture approach in conjunction with an iso-strain concept. Furthermore, backstress and softening variables are introduced to consider hardening and softening effects. This procedure results in a system of three differential equations describing the mechanical behaviour.


2015 ◽  
Vol 732 ◽  
pp. 161-164 ◽  
Author(s):  
Jan Vesely ◽  
Lukas Horny ◽  
Hynek Chlup ◽  
Milos Beran ◽  
Milan Krajicek ◽  
...  

The effects of the polyvinyl alcohol (PVA) concentration on mechanical properties of hydrogels based on blends of native or denatured collagen / PVA were examined. Blends of PVA with collagen were obtained by mixing the solutions in different ratios, using glycerol as a plasticizer. The solutions were cast on polystyrene plates and the solvent was allowed to evaporate at room temperature. Uniaxial tensile tests were performed in order to obtain the initial modulus of elasticity (up to deformation 0.1), the ultimate tensile stress and the deformation at failure of the material in the water-saturated hydrogel form. It was found that the material was elastic and the addition of PVA helped to enhance both the ultimate tensile stress and modulus of elasticity of the films. Samples prepared from denaturated collagen showed the higher ultimate tensile stress and the deformation at failure in comparison with those prepared from native collagen. The results suggest that we could expect successful application of the collagen/PVA biomaterial for tissue engineering.


2018 ◽  
Vol 2018 ◽  
pp. 1-12 ◽  
Author(s):  
Hui Chen ◽  
Jinjin Zhang ◽  
Jin Yang ◽  
Feilong Ye

The tensile behaviors of corroded steel bars are important in the capacity evaluation of corroded reinforced concrete structures. The present paper studies the mechanical behavior of the corroded high strength reinforcing steel bars under static and dynamic loading. High strength reinforcing steel bars were corroded by using accelerated corrosion methods and the tensile tests were carried out under different strain rates. The results showed that the mechanical properties of corroded high strength steel bars were strain rate dependent, and the strain rate effect decreased with the increase of corrosion degree. The decreased nominal yield and ultimate strengths were mainly caused by the reduction of cross-sectional areas, and the decreased ultimate deformation and the shortened yield plateau resulted from the intensified stress concentration at the nonuniform reduction. Based on the test results, reduction factors were proposed to relate the tensile behaviors with the corrosion degree and strain rate for corroded bars. A modified Johnson-Cook strength model of corroded high strength steel bars under dynamic loading was proposed by taking into account the influence of corrosion degree. Comparison between the model and test results showed that proposed model properly describes the dynamic response of the corroded high strength rebars.


Author(s):  
Micah Hodgins ◽  
Alexander York ◽  
Stefan Seelecke

This work presents the design, fabrication and testing of a comprehensive DEAP test station. The tester is designed to perform tensile tests of planar DEAPs while measuring quantities such as tensile force, stretch, film thickness and voltage/current. The work details the specimen preparation and how the specimen is placed in the clamps. While the assembly process is performed by hand features were built-in to the design of the specimen frame and clamps to enable reliable placement and specimen geometry. Test results of the pure-shear specimen demonstrated good performance of the testing device. Although the electrode surface was rough the thickness stretch was evident during the stretching/actuation of the DEAP actuator.


DYNA ◽  
2016 ◽  
Vol 83 (195) ◽  
pp. 77-83 ◽  
Author(s):  
María José Quintana Hernández ◽  
José Ovidio García ◽  
Roberto González Ojeda ◽  
José Ignacio Verdeja

The use of Cu and Ti in Zn alloys improves mechanical properties as solid solution and dispersoid particles (grain refiners) may harden the material and reduce creep deformation. This is one of the main design problems for parts made with Zn alloys, even at room temperature. In this work the mechanical behavior of a Zn-Cu-Ti low alloy is presented using tensile tests at different strain rates, as well as creep tests at different loads to obtain the value of the strain rate coefficient m in samples parallel and perpendicular to the rolling direction of the Zn strip. The microstructure of the alloy in its raw state, as well as heat treated at 250°C, is also analyzed, as the banded structure produced by rolling influences the strengthening mechanisms that can be achieved through the treatment parameters.


2021 ◽  
Author(s):  
Ciara Durcan ◽  
Mokarram Hossain ◽  
Gregory Chagnon ◽  
Djordje Peric ◽  
Lara Bsiesy ◽  
...  

Technological advancements in the field of robotics have led to endoscopic biopsy devices able to extract diseased tissue from between the layers of the gastrointestinal tract. Despite this, the layer-dependent properties of these tissues have yet to be mechanically characterised using human tissue. In this study, the ex vivo mechanical properties of the passive muscularis propia layer of the human oesophagus were extensively investigated. For this, a series of uniaxial tensile tests were conducted. The results displayed hyperelastic behaviour, while the differences between loading the tissue in both the longitudinal and circumferential directions showcased its anisotropy. The anisotropy of the muscular layer was present at different strain rates, with the longitudinal direction being consistently stiffer than the circumferential one. The circumferential direction was found to have little strain-rate dependency, while the longitudinal direction results suggest pronounced strain-rate-dependent behaviour. The repeated trials showed larger variation in terms of stress for a given strain in the longitudinal direction compared to the circumferential direction. The possible causes of variation between trials are discussed, and the experimental findings are linked to the histological analysis which was carried out via various staining methods. Finally, the direction-dependent experimental data was simulated using an anisotropic, hyperelastic model.


2018 ◽  
Vol 37 (9-10) ◽  
pp. 873-888 ◽  
Author(s):  
Nitin Kotkunde ◽  
Hansoge Nitin Krishnamurthy ◽  
Swadesh Kumar Singh ◽  
Gangadhar Jella

AbstractA thorough understanding of hot deformation behavior plays a vital role in determining process parameters of hot working processes. Firstly, uniaxial tensile tests have been performed in the temperature ranges of 150 °C–600 °C and strain rate ranges of 0.0001–0.01s−1 for analyzing the deformation behavior of ASS 304 and ASS 316. The phenomenological-based constitutive models namely modified Fields–Backofen (m-FB) and Khan–Huang–Liang (KHL) have been developed. The prediction capability of these models has been verified with experimental data using various statistical measures. Analysis of statistical measures revealed KHL model has good agreement with experimental flow stress data. Through the flow stresses behavior, the processing maps are established and analyzed according to the dynamic materials model (DMM). In the processing map, the variation of the efficiency of the power dissipation is plotted as a function of temperature and strain rate. The processing maps results have been validated with experimental data.


2007 ◽  
Vol 551-552 ◽  
pp. 539-544 ◽  
Author(s):  
S. Ding ◽  
Kai Feng Zhang ◽  
Guo Feng Wang

Nanocrystalline pure nickel (nc-Ni) was produced by pulse electrodeposition and its superplastic properties at and above room temperature were investigated. The electrodeposited nickel has a narrow grain size distribution with a mean grain size of 70nm. Uniaxial tensile tests at room temperature showed that nc-Ni has a limited plasticity but high tensile strength up to 1GPa at strain rates between 10-5 and 10-2s-1. However, when the temperature increased to 420 and higher, test specimens showed uniform deformation and the elongation value was larger than 200%. A maximum elongation value of 380% was observed at 450°C and a strain rate of 1.67x10-3s-1, SEM and TEM were used to examine the microstructures of the as-deposited and deformed specimens. The results indicated that fracture was caused by intergranular cracking and most cracks were originated from the brittle oxide formed during the tensile test. Grain coarsening was observed in the deformed specimen. The role of temperature and strain on grain growth was evaluated by comparing the microstructure of deformed samples with that of samples statically annealed. Deformation mechanism was discussed based upon the deformed microstructure and strain rate jump tests.


Author(s):  
Cunjian Miao ◽  
Yaxian Li ◽  
Jinyang Zheng

Cold stretching (pressure strenghtening) technique has been widely used in austenitic stainless steel pressure vessels in order to increase the proof strength and lighten the weight of the vessels. Cold stretching technique is performed by applying the strengthening pressure under a specified strain rate. Plastic deformation in the process will lead to martensite transformation and may influence material’s strength and ductility. Cold stretching tests of EN 1.4301 stainless steel are carried out at different quasi-static strain rates of 10−3 and 10−5/s, following the uniaxial tensile tests at the same strain rate of 2.5×10−3/s. The α′-martensite transformation is detected by magnetic measurement, meanwhile the work-hardening rate, the flow stress and the mechanical properties of material are studied and the results are presented.


Metals ◽  
2019 ◽  
Vol 10 (1) ◽  
pp. 38 ◽  
Author(s):  
Jihyun Jun ◽  
Hogeon Seo ◽  
Kyung-Young Jhang

The structures in high-temperature environments are prone to undergo hardening and embrittlement as a result of thermal aging; this can cause variations in their mechanical properties. Because these changes occur at the microstructural level, it is difficult to evaluate them through linear ultrasonic techniques. In this work, a surface acoustic wave (SAW) was used to measure and compare the acoustic nonlinearity and mechanical properties of Al6061 alloys heat-treated at 220 °C for different durations (0 min, 20 min, 40 min, 1 h, 2 h, 10 h, 100 h, 1000 h). The SAW was generated by a pulsed laser and then received by an interferometer. Moreover, the yield strength, ultimate strength, and elongation to failure were measured by tensile tests. The results demonstrate that the critical variations in the mechanical properties can be detected by monitoring the variation features in the acoustic nonlinearity. Transmission electron microscopy images were captured to observe the microstructural changes, which shows that the acoustic nonlinearity varied according to the change in the precipitation phase. This supports the acoustic nonlinearity measurement using the laser-generated SAW being an effective technique for the fully noncontact nondestructive evaluation of material degradations as well as changes in mechanical properties.


Sign in / Sign up

Export Citation Format

Share Document