Effects of Applied Voltage on Morphology and Crystal Orientation of Mg(OH)[sub 2] Coating on Pt by Electrochemical Synthesis

2009 ◽  
Vol 156 (2) ◽  
pp. E29 ◽  
Author(s):  
Ching-Fei Li ◽  
Wen-Hsien Ho ◽  
Shiow-Kang Yen
Keyword(s):  
Applied Voltage ◽  
Electrochemical Synthesis ◽  
Crystal Orientation

Controlled Release Electrochemical Synthesis and Cytotoxicity Study of Copper(II) Nanoparticles in Copper(II) Decanoate Complex

NANO ◽  
2018 ◽  
Vol 13 (05) ◽  
pp. 1850048 ◽  
Author(s):  
Norazzizi Nordin ◽  
Wan Zurina Samad ◽  
Egi Kardia ◽  
Badrul Hisham Yahaya ◽  
Muhammad Rahimi Yusop ◽  
...  
Keyword(s):  
Cell Death ◽  
Controlled Release ◽  
Hela Cells ◽  
Applied Voltage ◽  
Electrochemical Synthesis ◽  
Cytotoxic Effect ◽  
Decanoic Acid ◽  
Normal Cells ◽  
Apoptosis Assay

In the present study, a controlled release electrochemical (CRE) technique based on the controlled release of Cu[Formula: see text] ion from Cu anode in the presence of decanoic acid (HDe) has been used to synthesize Cu(II) decanoate (CuDe2) complex. The effect of applied voltages (1–10[Formula: see text]V) and electrolyte concentrations (0.1–2.0[Formula: see text]M CH3COONH4) during the electrolysis on the nanoparticles obtained was studied using TEM. The results reveal that small-sized nanoparticles ([Formula: see text][Formula: see text]nm) were obtained by using lowest applied voltage and CH3COONH4 concentration (1[Formula: see text]V and 0.1[Formula: see text]M, respectively). The smallest nanoparticle obtained was then used in the cytotoxicity study against A549 and HeLa cells. The synthesized complex gives moderate cytotoxic effect on the selected cells (IC[Formula: see text]M and 20.89[Formula: see text][Formula: see text]M, respectively) and low cytotoxic effect on normal cells (IMR90). Apoptosis is the mode of cell death based on the apoptosis assay that has been conducted.

Spherulitic crystal growth in the prodissoconch larval of Crassostrea virginica

1983 ◽  
Vol 41 ◽  
pp. 518-519
Author(s):  
George G. Cocks ◽  
Louis Leibovitz ◽  
DoSuk D. Lee
Keyword(s):  
Crystal Structure ◽  
Crassostrea Virginica ◽  
Crystal Orientation ◽  
Developmental Changes ◽  
Gastrula Stage ◽  
Orthorhombic Crystal ◽  
Orthorhombic Crystal Structure ◽  
Stages Of Growth ◽  
Early Stages ◽  
Initial Deposition

Our understanding of the structure and the formation of inorganic minerals in the bivalve shells has been considerably advanced by the use of electron microscope. However, very little is known about the ultrastructure of valves in the larval stage of the oysters. The present study examines the developmental changes which occur between the time of conception to the early stages of Dissoconch in the Crassostrea virginica(Gmelin), focusing on the initial deposition of inorganic crystals by the oysters.The spawning was induced by elevating the temperature of the seawater where the adult oysters were conditioned. The eggs and sperm were collected separately, then immediately mixed for the fertilizations to occur. Fertilized animals were kept in the incubator where various stages of development were stopped and observed. The detailed analysis of the early stages of growth showed that CaCO3 crystals(aragonite), with orthorhombic crystal structure, are deposited as early as gastrula stage(Figuresla-b). The next stage in development, the prodissoconch, revealed that the crystal orientation is in the form of spherulites.

The Interpretation of Crystal Lattice Images

1972 ◽  
Vol 30 ◽  
pp. 550-551
Author(s):  
J. M. Cowley ◽  
Sumio Iijima
Keyword(s):  
Crystal Orientation ◽  
Diffraction Theory ◽  
Phase Changes ◽  
Electron Wave ◽  
Crystal Lattices ◽  
Heavy Atoms ◽  
Lattice Images ◽  
The Right ◽  
Intuitive Interpretation ◽  
Suitable Approximation

The imaging of detailed structures of crystal lattices with 3 to 4Å resolution, given the correct conditions of microscope defocus and crystal orientation and thickness, has been used by Iijima (this conference) for the study of new types of crystal structures and the defects in known structures associated with fluctuations of stoichiometry. The image intensities may be computed using n-beam dynamical diffraction theory involving several hundred beams (Fejes, this conference). However it is still important to have a suitable approximation to provide an immediate rough estimate of contrast and an evaluation of the intuitive interpretation in terms of an amplitude object.For crystals 100 to 150Å thick containing moderately heavy atoms the phase changes of the electron wave vary by about 10 radians suggesting that the “optimum defocus” theory of amplitude contrast for thin phase objects due to Scherzer and others can not apply, although it does predict the right defocus for optimum imaging.

FIM OBSERVATION ON THE REACTION OF METALS ( W, Mo ) WITH n-OCTANOL UNDER AN APPLIED VOLTAGE

1987 ◽  
Vol 48 (C6) ◽  
pp. C6-499-C6-504 ◽  
Author(s):  
T. Terao ◽  
F. Iwatsu ◽  
H. Morikawa ◽  
Y. Yashiro
Keyword(s):  
Applied Voltage

PARAMETRIC MODEL OF RESISTANCE OF PLASMA-EROSIVE LOAD, ADEQUATE IN THE WIDE RANGE OF CHANGE OF APPLIED VOLTAGE

2017 ◽  
Vol 2017 (3) ◽  
pp. 3-12 ◽  
Author(s):  
N.A. Shydlovska ◽  
◽  
S.M. Zakharchenko ◽  
O.P. Cherkaskyi ◽  
◽  
...  
Keyword(s):  
Applied Voltage ◽  
Parametric Model ◽  
Wide Range
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