In Situ X-Ray Study of the Electrochemical Reaction of Li with ηʹ-Cu[sub 6]Sn[sub 5]

2000 ◽  
Vol 147 (5) ◽  
pp. 1658 ◽  
Author(s):  
D. Larcher ◽  
L. Y. Beaulieu ◽  
D. D. MacNeil ◽  
J. R. Dahn
Keyword(s):  
Electrochemical Reaction ◽  
X Ray

Distinct nanoscale reaction pathways in a sulfide material for sodium and lithium batteries

2017 ◽  
Vol 5 (23) ◽  
pp. 11701-11709 ◽  
Author(s):  
Matthew G. Boebinger ◽  
Michael Xu ◽  
Xuetian Ma ◽  
Hailong Chen ◽  
Raymond R. Unocic ◽  
...  
Keyword(s):  
Lithium Batteries ◽  
Copper Sulfide ◽  
Electrochemical Reaction ◽  
Cycle Life ◽  
Reaction Pathways ◽  
X Ray Diffraction ◽  
X Ray

Copper sulfide is found to exhibit excellent cycle life in Na-ion batteries, and multiscale in situ techniques (TEM and X-ray diffraction) are used to reveal unique aspects of the electrochemical reaction of sodium with this material.

The Use of Advanced Analytical Techniques for Characterization of the Chemical, Physical, and Crystallographic Nature of a Surface

1973 ◽  
Vol 31 ◽  
pp. 132-133 ◽  
Author(s):  
R. E. Herfert
Keyword(s):  
Surface Characterization ◽  
Analytical Techniques ◽  
X Ray Diffraction ◽  
Depth Of Penetration ◽  
X Ray ◽  
The Past ◽  
Transmission Electron ◽  
Scanning Electron

Studies of the nature of a surface, either metallic or nonmetallic, in the past, have been limited to the instrumentation available for these measurements. In the past, optical microscopy, replica transmission electron microscopy, electron or X-ray diffraction and optical or X-ray spectroscopy have provided the means of surface characterization. Actually, some of these techniques are not purely surface; the depth of penetration may be a few thousands of an inch. Within the last five years, instrumentation has been made available which now makes it practical for use to study the outer few 100A of layers and characterize it completely from a chemical, physical, and crystallographic standpoint. The scanning electron microscope (SEM) provides a means of viewing the surface of a material in situ to magnifications as high as 250,000X.

In Situ X-Ray Absorption Studies of the Electrochemical Reduction of Hydroxocobalamin

1997 ◽  
Vol 7 (C2) ◽  
pp. C2-619-C2-620 ◽  
Author(s):  
M. Giorgett ◽  
I. Ascone ◽  
M. Berrettoni ◽  
S. Zamponi ◽  
R. Marassi
Keyword(s):  
Electrochemical Reduction ◽  
X Ray ◽  
Absorption Studies ◽  
X Ray Absorption
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