Fabrication and characterization of replicated and lacquer-coated grazing incidence optics for x-ray astronomy

1992 ◽  
Author(s):  
Melville P. Ulmer ◽  
Rudy H. Haidle ◽  
Robert I. Altkorn ◽  
P. Georgopoulos ◽  
Brian G. Rodricks ◽  
...  
Keyword(s):  
Grazing Incidence ◽  
X Ray ◽  
Grazing Incidence Optics ◽  
Fabrication And Characterization

Interface characterization of B4C-based multilayers by X-ray grazing-incidence reflectivity and diffuse scattering

2013 ◽  
Vol 20 (3) ◽  
pp. 449-454 ◽  
Author(s):  
Hui Jiang ◽  
Zhanshan Wang ◽  
Jingtao Zhu
Keyword(s):  
Diffuse Scattering ◽  
Aging Process ◽  
Grazing Incidence ◽  
X Rays ◽  
X Ray ◽  
Interface Characterization ◽  
Quantitative Results ◽  
Fabrication And Characterization ◽  
Stable Structures

B4C-based multilayers have important applications for soft to hard X-rays. In this paper, X-ray grazing-incidence reflectivity and diffuse scattering, combining various analysis methods, were used to characterize the structure of B4C-based multilayers including layer thickness, density, interfacial roughness, interdiffusion, correlation length,etc.Quantitative results for W/B4C, Mo/B4C and La/B4C multilayers were compared. W/B4C multilayers show the sharpest interfaces and most stable structures. The roughness replications of La/B4C and Mo/B4C multilayers are not strong, and oxidations and structure expansions are found in the aging process. This work provides guidance for future fabrication and characterization of B4C-based multilayers.

Reference-free, depth-dependent characterization of nanolayers and gradient systems with advanced grazing incidence X-ray fluorescence analysis

2015 ◽  
Vol 212 (3) ◽  
pp. 523-528 ◽  
Author(s):  
Philipp Hönicke ◽  
Blanka Detlefs ◽  
Matthias Müller ◽  
Erik Darlatt ◽  
Emmanuel Nolot ◽  
...  
Keyword(s):  
Fluorescence Analysis ◽  
Grazing Incidence ◽  
X Ray ◽  
Gradient Systems

scholarly journals Fabrication and characterization of Si-based soft x-ray mirrors

1991 ◽  
Author(s):  
Bernt Schmiedeskamp ◽  
Bernhard Heidemann ◽  
Ulf Kleineberg ◽  
Andreas Kloidt ◽  
Mikhael Kuehne ◽  
...  
Keyword(s):  
X Ray ◽  
Fabrication And Characterization

scholarly journals Fabrication and Characterization of Al/NiO Energetic Nanomultilayers

2015 ◽  
Vol 2015 ◽  
pp. 1-6 ◽  
Author(s):  
YiChao Yan ◽  
Wei Shi ◽  
HongChuan Jiang ◽  
Jie Xiong ◽  
WanLi Zhang ◽  
...  
Keyword(s):  
Photoelectron Spectroscopy ◽  
Total Thickness ◽  
X Ray Diffraction ◽  
Dc Magnetron Sputtering ◽  
Metallic Oxide ◽  
Promising Candidate ◽  
X Ray ◽  
Thermal Boundary Conductance ◽  
Fabrication And Characterization

The redox reaction between Al and metallic oxide has its advantage compared with intermetallic reaction and Al/NiO nanomutlilayers are a promising candidate for enhancing the performance of energetic igniter. Al/NiO nanomutlilayers with different modulation periods are prepared on alumina substrate by direct current (DC) magnetron sputtering. The thicknesses of each period are 250 nm, 500 nm, 750 nm, 1000 nm, and 1500 nm, respectively, and the total thickness is 3 μm. The X-ray diffraction (XRD) and scanning electron microscope (SEM) results of the as-deposited Al/NiO nanomutlilayers show that the NiO films are amorphous and the layered structures are clearly distinguished. The X-ray photoelectron spectroscopy (XPS) demonstrates that the thickness of Al2O3increases on the side of Al monolayer after annealing at 450°C. The thermal diffusion time becomes greater significantly as the amount of thermal boundary conductance across the interfaces increases with relatively smaller modulation period. Differential scanning calorimeter (DSC) curve suggests that the energy release per unit mass is below the theoretical heat of the reaction due to the nonstoichiometric ratio between Al and NiO and the presence of impurities.

scholarly journals Preparation and Characterization of Porous Ceramic Membranes for Micro-Filtration from Clay/CuZn Using Extrusion Methods

2018 ◽  
Vol 156 ◽  
pp. 08015 ◽  
Author(s):  
Muh Amin ◽  
Muhammad Subri
Keyword(s):  
Porous Ceramic ◽  
Ceramic Materials ◽  
Ceramic Membranes ◽  
Extrusion Process ◽  
X Ray Diffraction ◽  
Percentage Composition ◽  
X Ray ◽  
Ceramic Support ◽  
Fabrication And Characterization

In this study, fabrication and characterization of ceramic membranes preparation was carried out. Porous ceramic membranes were fabricated by extrusion process from different percentage composition of CuZn on (80 wt% Clay, 10 wt% TiO2, 5 wt% Carbon and 5 wt% PVA). The fabricated membranes were sintered at 900°C for 1 hour in an electrical box furnace with heating rate 1oC/min and holding time for 1 hour. Apparent density and porosity were determined by standar methods for ceramic materials. Phase composition of the ceramic support was established by X-Ray Diffraction analysis. SEM studies of the membranes added at different CuZn were carried out.

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