Mechanical and thermal properties of ABS/iron composite for fused deposition modeling

Author(s):  
Bartłomiej J. Podsiadły ◽  
Andrzej Skalski ◽  
Marcin Słoma
2021 ◽  
Vol 877 ◽  
pp. 67-72
Author(s):  
Niño B. Felices ◽  
Bryan B. Pajarito

Epoxysilane-treated muscovite (ETM) was used as reinforcing filler to 3D-printed acrylonitrile butadiene styrene (ABS) via fused deposition modeling (FDM). Its effects to the mechanical and thermal properties of ABS were investigated. ETM was loaded at 1, 3, and 5wt%. ABS/ETM composites were characterized via scanning electron microscopy (SEM), tensile test, differential scanning calorimetry (DSC) and thermogravimetric analysis (TGA). Mechanical reinforcement of ABS was observed for ABS/ETM composites loaded at 1 and 3 wt% wherein it was noted that the tensile strength and elastic modulus increased by up to 83.6% and 76.6%, respectively. Reinforcement was brought by interfacial adhesion of ETM with the ABS matrix. There was a sharp decline in mechanical properties for ABS/ETM composites loaded at 5wt% due to agglomeration of ETM in the matrix and discontinuities in the printed layers. The glass transition temperature (Tg) of ABS increased and the onset of its degradation shifted towards higher temperatures with the addition of ETM. It can be concluded that the addition of ETM to ABS for FDM 3D printing improved its mechanical and thermal properties.


2021 ◽  
Vol 877 ◽  
pp. 61-66
Author(s):  
Niño B. Felices ◽  
Bryan B. Pajarito

The effect of the addition of epoxysilane-treated wollastonite (ETW) to the mechanical and thermal properties of 3D-printed acrylonitrile butadiene styrene (ABS) via fused deposition modeling (FDM) was investigated. The loading of ETW was varied at 1, 3, and 5wt%. The 3D-printed composites were evaluated by scanning electron microscopy (SEM) tensile test, shore D hardness, differential scanning calorimetry (DSC) and thermogravimetric analysis (TGA). The addition of ETW increases the tensile strength, elastic modulus, and toughness of ABS by up to 46.6, 56.2, and 53.7 %, respectively. The shore D hardness increases with increasing ETW. Morphological analysis show that this improvement in mechanical properties is a result of the high aspect ratio of the fillers, the uniform dispersion of ETW in the ABS matrix, and the orientation of ETW particles toward the direction of tensile stress. The glass transition temperature (Tg) of the composites increases and the onset of degradation slightly shifted to higher temperature with an increase in filler loading. The addition of ETW to ABS matrix in FDM 3D printing improved the mechanical and thermal properties of ABS.


2018 ◽  
Vol 24 (9) ◽  
pp. 1455-1468 ◽  
Author(s):  
Rupinder Singh ◽  
Ranvijay Kumar ◽  
IPS Ahuja

Purpose This study aims to highlights the mechanical, thermal and melting behavior compatibility of aluminum (Al)-reinforced polyamide (PA) 6/acrylonitrile butadiene styrene (ABS)-based functional prototypes prepared using fused deposition modeling (FDM) from the friction welding point of view. Previous studies have highlighted the use of metallic/non-metallic fillers in polymer matrix for preparations of mechanically improved FDM feedstock filaments and functional prototypes. But hitherto, very less has been reported on fabrication of functional prototypes which fulfill the compatibility of two polymers for joining/welding-based applications. The compatibility of two dissimilar polymers enables the friction welding for maintenance applications. Design/methodology/approach The twin screw extrusion process has been used for mechanical mixing of metallic reinforcement in polymer matrix, and final blend of reinforced polymers in the form of extruded feed stock filament has been used on FDM for printing of functional prototypes (for friction welding). The methodology involves melt flow index (MFI) investigations, differential scanning calorimetry (DSC) investigations for thermal properties, tensile and hardness testing for mechanical properties and photo micrographic investigations for metallurgical properties on extruded samples. Findings It was observed that the reinforced ABS and PA6 polymers have better compatibility in the terms of similar melt flow, thermal properties and can lead to the better joint efficiency with friction welding. Originality/value In the present work composite feed stock filament composed of ABS and PA6 with reinforcement of Al powder has been successfully developed for preparation of functional prototype in friction welding applications.


2020 ◽  
Vol 10 (9) ◽  
pp. 3170 ◽  
Author(s):  
Elisa Padovano ◽  
Marco Galfione ◽  
Paolo Concialdi ◽  
Gianni Lucco ◽  
Claudio Badini

Fused-deposition modeling (FDM) is an additive manufacturing technique which is widely used for the fabrication of polymeric end-use products in addition to the development of prototypes. Nowadays, there is an increasing interest in the scientific and industrial communities for new materials showing high performance, which can be used in a wide range of applications. Ultem 9085 is a thermoplastic material that can be processed by FDM; it recently emerged thanks to such good properties as excellent flame retardancy, low smoke generation, and good mechanical performance. A deep knowledge of this material is therefore necessary to confirm its potential use in different fields. The aim of this paper is the investigation of the mechanical and thermal properties of Ultem 9085. Tensile strength and three-point flexural tests were performed on samples with XY, XZ, and ZX building orientations. Moreover, the influence of different ageing treatments performed by varying the maximum reached temperature and relative humidity on the mechanical behavior of Ultem 9085 was then investigated. The thermal and thermo-oxidative behavior of this material was also determined through thermal-gravimetric analyses.


Author(s):  
Michael A. Luzuriaga ◽  
Danielle R. Berry ◽  
John C. Reagan ◽  
Ronald A. Smaldone ◽  
Jeremiah J. Gassensmith

Biodegradable polymer microneedle (MN) arrays are an emerging class of transdermal drug delivery devices that promise a painless and sanitary alternative to syringes; however, prototyping bespoke needle architectures is expensive and requires production of new master templates. Here, we present a new microfabrication technique for MNs using fused deposition modeling (FDM) 3D printing using polylactic acid, an FDA approved, renewable, biodegradable, thermoplastic material. We show how this natural degradability can be exploited to overcome a key challenge of FDM 3D printing, in particular the low resolution of these printers. We improved the feature size of the printed parts significantly by developing a post fabrication chemical etching protocol, which allowed us to access tip sizes as small as 1 μm. With 3D modeling software, various MN shapes were designed and printed rapidly with custom needle density, length, and shape. Scanning electron microscopy confirmed that our method resulted in needle tip sizes in the range of 1 – 55 µm, which could successfully penetrate and break off into porcine skin. We have also shown that these MNs have comparable mechanical strengths to currently fabricated MNs and we further demonstrated how the swellability of PLA can be exploited to load small molecule drugs and how its degradability in skin can release those small molecules over time.


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