Incorporation of Fe3O4 Nanoparticles as Drilling Fluid Additives for Improved Drilling Operations

Author(s):  
Zisis Vryzas ◽  
Omar Mahmoud ◽  
Hisham Nasr-El-Din ◽  
Vassilis Zaspalis ◽  
Vassilios C. Kelessidis

A successful drilling operation requires an effective drilling fluid system. Due to the variety of downhole conditions across the globe, the fluid system should be designed to meet complex challenges such as High-Pressure/High-Temperature (HPHT) environments, while promoting better productivity with a minimum interference for completion operations. This study aims to improve the rheological and fluid loss properties of water-bentonite suspensions by using both commercial (C-NP) and custom-made (CM-NP) iron oxide (Fe3O4) nanoparticles (NP) as drilling fluid additives. Superparamagnetic Fe3O4 NP were synthesized by the co-precipitation method. Both types of nanoparticles were characterized by a High Resolution Transmission Electron Microscope (TEM) and X-ray Diffraction (XRD). Base fluid (BF), made of deionized water and bentonite at 7wt%, was prepared according to American Petroleum Institute (API) procedures and nanoparticles were added at 0.5wt%. A Couette-type viscometer was used to analyze the rheological characteristics of these fluids at different shear rates and various temperatures (up to 158°F). The rheological parameters were obtained from analysis of viscometric data using non-linear regression. The API Low-Pressure/Low-Temperature (LPLT) and HPHT fluid filtrate volumes were measured, using a standard API LPLT static filter press (100 psi, 77°F) and an API HPHT filter press (300 psi, 250°F). Observation of the porous matrix morphology of the produced filter cakes was done with Scanning Electron Microscope (SEM). TEM showed that the mean diameter of the CM-NP was 7–8 nm, with measured surface areas between 100–250 m2/g. The C-NP had an average diameter of <50 nm, as per manufacturer specifications. The XRD of the CM-NP revealed peaks corresponding to pure crystallites of magnetite (Fe3O4) with no impurities. Rheological analysis showed very good fitting by the Herschel-Bulkley model with coefficient of determination (R2) greater than 0.99. Rheological properties of all samples were affected by higher temperatures, with increase in yield stress, decrease in flow consistency index (K) and slight increase in flow behavior index (n). Fluid filtration results indicated a decrease in the LPLT fluid loss and an increase in the filter cake thickness compared to the BF upon addition of higher concentrations of C-NP, because of a decrease in filter cake permeability. At HPHT conditions, samples with 0.5wt% C-NP had a smaller fluid loss by 34.3%, compared to 11.9% at LPLT conditions. CM-NP exhibited even higher reduction in the fluid loss at HPHT conditions of 40%. Such drilling fluids can solve difficult drilling problems and aid in achieving the reservoir’s highest potential by eliminating the use of aggressive, potentially damaging chemicals. Exploitation of the synergistic interaction of the utilized components can produce a water-based system with excellent fluid loss characteristics while maintaining optimal rheological properties.

Author(s):  
Zisis Vryzas ◽  
Vassilios C. Kelessidis ◽  
Lori Nalbandian ◽  
Vassilios Zaspalis

Smart drilling fluids, which can change their properties according to the flow environment, must be carefully designed so that they can handle the difficult challenges of HP/HT drilling successfully. Due to their unique physico-chemical properties, nanoparticles (NP) are considered as very good candidates for the formulation of these smart drilling fluids. This study presents filtration and rheological results of newly developed high-performance water-based drilling fluid systems containing different nanoparticles, commercial (C) titanium oxide (TiO2) and commercial (C) copper oxide (CuO) NP and compares them with results from using custom-made (CM) iron oxide (Fe3O4) NP and commercial (C) iron oxide (Fe3O4) NP, previously reported. Novel nano-based drilling fluids were made of de-ionized water, 7 wt% commercial Na-bentonite (base fluid), and NP were added at 0.5 wt%. The rheological properties of the produced suspensions were measured at temperatures up to 60°C and at atmospheric pressure with a Couette-type viscometer. Filtration characteristics were determined at elevated pressures and temperatures in a HP/HT filter press (500 psi/176°C) using ceramic discs as filter media, of permeability, k = 775 mD. The results of this study showed that the samples containing 0.5 wt% C TiO2 caused a reduction in the fluid loss by 23%, while C CuO NP resulted in 16% reduction, when compared to that of the base fluid, at these HPHT conditions. This should be compared to the 47% and 34% reduction in fluid loss of 0.5% CM Fe3O4 NP and of 0.5% of C Fe3O4 NP, reported previously. Analysis of rheological data revealed shear-thinning behavior for all the tested novel drilling fluids. The samples containing TiO2 and CuO NP exhibited a yield stress less than that of the base fluid, compared to the increased yield stress observed for the C and CM Fe3O4 NP. This behavior can be attributed to the fact that TiO2 and CuO NP may also act as deflocculants and prevent the gelation of bentonite suspensions. This study shows that commercial nanoparticles of TiO2 and CuO do not perform as well as the Fe3O4 NP on filtration but provide drilling fluids with lower yield stresses, thus they could be considered as alternatives to Fe3O4 in situations where the rheological properties are critical.


2012 ◽  
pp. 1-22
Author(s):  
Issham Ismail ◽  
Rosli Illias ◽  
Amy Shareena Abd. Mubin ◽  
Masseera Machitin

The effective cleanup of filter cakes in long, horizontal open-hole completions can maximize an oil well’s productivity. A cleaning solution was formulated which comprised effective microorganisms and a viscoelastic surfactant in order to degrade filter cakes of water-based mud. Generally, the effectiveness of the microorganisms in degrading filter cakes is influenced by temperature and its concentration. To overcome the problem, the viscoelastic surfactant has been used to extend the application of temperature range and increase the viscosity of the cleaning solution. Laboratory studies were conducted to examine the effectiveness of the microorganisms in degrading filter cakes. The apparent viscosity of cleaning solution was measured as a function of shear rate (102.2 s and 1022 s ) and temperature (25 to 80°C). The surface tension of the cleaning solution was measured at room temperature. Static fluid loss tests were performed using the HPHT Filter Press in order to determine the effectiveness of the cleaning solution in degrading filter cake at different temperatures ranging from 100°F to 300°F. Experimental results showed that the cleaning solution could effectively degrade the filter cake. Soaking process was performed until 48 hours and it showed that at temperature 200°F and below, the pure effective microorganisms achieved the highest efficiency of filter cake degradation, i.e. 34.9%. However, at temperature 300°F, cleaning solution that contained effective microorganisms and higher concentration of viscoelastic surfactant was found to perform better. The viscoelastic surfactant succeeded in increasing the viscosity of the cleaning solution, thus enhanced the rate of degradation of filter cakes, i.e. 33.4% at 300°F. The surface tension of the cleaning solution did not change significantly at various concentrations at room temperature.


2020 ◽  
Vol 10 (8) ◽  
pp. 3389-3397 ◽  
Author(s):  
Nayem Ahmed ◽  
Md. Saiful Alam ◽  
M. A. Salam

Abstract Loss of drilling fluid commonly known as mud loss is considered as one of the critical issues during the drilling operation as it can cause severe formation damage. To minimize fluid loss, researchers introduced numerous additives but did not get the expected result. Recently, the use of nanoparticles (NPs) in drilling fluid gives a new hope to control the fluid loss. A basic KCl–Glycol–PHPA polymer-based mud is made, and six different concentrations of 0.1, 0.5, 1.0, 1.5, 2.0, 3.0 wt% iron (III) oxide or Hematite (Fe2O3) NPs are mixed with the basic mud. The experimental observations reveal that fluid loss of basic mud is 5.9 ml after 30 min and prepared nano-based drilling mud results in a less fluid loss at all concentrations. Nanoparticles with a concentration of 0.5 wt% result in a 5.1 ml fluid loss at the API LTLP filter press test. On the other hand, nanoparticles with a concentration of 3.0 wt% enhance the plastic viscosity, yield point, and 10 s gel strength by 15.0, 3.0, and 12.5%, respectively. The optimum concentration of hematite NPs is found to be 0.5 wt% which reduces the API LPLT filtrate volume and filter cake thickness by 13.6 and 40%, respectively, as well as an improvement of plastic viscosity by 10%.


2018 ◽  
Vol 8 (8) ◽  
pp. 1386 ◽  
Author(s):  
Hazlina Husin ◽  
Khaled Abdalla Elraies ◽  
Hyoung Jin Choi ◽  
Zachary Aman

Water-based mud is known as an environmental-friendly drilling fluid system. The formulation of water-based mud is designed to have specific rheological properties under specific oil field conditions. In this study, graphene nanoplatelet and silver nanoparticle (nanosilver) were added to a water-based mud formulation in which they act as drilling mud additives. Rheological properties measurements and filtration tests were conducted for evaluating the influence of the added nanoparticles. The results showed that the graphene nanoplatelet and the nanosilver increased the plastic viscosity (PV) by up to 89.2% and 64.2%, respectively. Meanwhile, both the yield point (YP) and the fluid loss values were reduced. In addition, we believe this is the first result ever report where nanosilver is utilized for enhancing-enhanced water-based mud’s performance.


Author(s):  
Chinwuba Kevin Igwilo ◽  
Nnaemeka Uwaezuoke ◽  
Emeka Emmanuel Okoro ◽  
Veronica Chika Nwachukwu ◽  
Nnanna Okoli

Pleurotus as a fluid loss control additive in synthetic based mud for oil and gas operations was conducted in the laboratory in accordance with API standards using high temperature-high pressure filter press. The effectiveness and compatibility of Pleurotus to synthetic based mud was also evaluated. Its rheological properties were also carried out. Sodium Asphalt Sulfonate was used as a control sample. Synthetic base mud was formulated and the concentrations of 2ppb, 4ppb, 6ppb and 8ppb of Pleurotus were used in four mud formulations with the same materials and in equal concentrations. 4.6ml, 4.0ml, 3.5ml and 3.1ml of fluid loss volumes were obtained respectively. 1mm thick filter cake, with increase in electrical stability was observed. From the laboratory measurement, the optimum effective concentration of Pleurotus to be applied as a fluid loss control agent for fresh non-aqueous mud for field operation is 2ppb which gave the fluid loss volume less than 5ml. The result was compared with the field standard of less than or equal to 5ml fluid loss volume. These results were comparable with control sample and field standard. Also, the thin impermeable filter cake obtained reflects one of the qualities of a good fluid loss control agent. It also showed that Pleurotus contribute very minimal effect on the rheological properties of the synthetic base mud. Improved electrical stability which is the function of emulsion stability confirmed the compatibility property of Pleurotus as fluid loss control additive in the synthetic based mud. The volume of the filtrate improved in geometric progression with the concentrations of the additive applied which summarizes the characteristics of a good fluid loss control agent.


2021 ◽  
Author(s):  
Zhao Xionghu ◽  
Saviour Bassey Egwu ◽  
Deng Jingen ◽  
Miao Liujie

Abstract The effect of corrosion inhibitor Benzotriazole on synthetic-based mud system was studied. Rheological performance of the benzotriazole enhanced synthetic-based fluid system was studied and compared against the base mud. To study its effect on dynamic wellbore conditions, different drilling fluid compositions were placed in a hot rolling oven for 16 hours at temperatures 150 °C and 170°C and the effect of temperature on mud properties were studied. Tests carried out include rheological test (before and after hot rolling), filtrate pH, lubricity test, and fluid loss test. The corrosion penetration rate was studied using the weight loss method. Based on experiment results, the synthetic-based mud system which comprised of benzotriazole displayed a reduction in coefficient of friction up to 95.93%. At ambient condition, optimal ratio of mineral oil:benzotriazole (M:B) which gives best lubricity performance on synthetic-based mud system is 80:20. This leads to improved corrosion inhibition and lubricity of the synthetic-based fluid by reducing the coefficient of friction up to 90.13%. Increased temperature led to further decrease in coefficient of friction with a % torque reduction of 95.93 displayed by the 80:20 ratio M:B mud composition at 170 °C. Significant alterations of the mud composition rheological and fluid loss parameters before and after exposure to high temperature in hot rolling oven were not observed. pH values were maintained ≥7 at the dynamic conditions highlighting solubility of the formulated fluid composition and absence of contaminants which can pose significant threats to the rates of corrosion in drill pipes. Increasing the concentration of Benzotriazole led to a reduction in corrosion rate. However, as the temperature effect increased, the corrosion rate elevated. Based on results from this investigation, it was concluded that Benzotriazole can be applied as a corrosion inhibitor in a synthetic-based drilling fluid system as an alternative corrosion inhibitor without significant alteration of the base mud properties. Benefits of this will be the optimization of extended reach well drilling operations due to excellent lubricity performance, corrosion rate reduction, compatibility with HPHT wellbore condition and fluid loss control.


2018 ◽  
Author(s):  
Ζήσης Βρύζας

Η γεώτρηση αποτελεί την πλέον δαπανηρή εργασία σε μια καμπάνια εξεύρεσης και παραγωγής υδρογονανθράκων. Πέραν αυτού συνιστά και την μοναδική διεργασία που δίνει τη δυνατότητα ακριβούς προσδιορισμού των αποθεμάτων στο υπέδαφος. Ο πολφός (γεωτρητικά ρευστά) είναι το ‘αίμα’ της γεώτρησης: παρέχει πίεση, μεταφορά τριμμάτων/θραυσμάτων από τον πυθμένα του φρέατος, ψύξη και λίπανση κοπτικού και στήλης, καθώς επίσης διατηρεί τα θραύσματα εν αιωρήσει όταν υπάρχει διακοπή της κυκλοφορίας. Ως ρευστό γεώτρησης (drilling fluid) χρησιμοποιείται συνήθως ένα αιώρημα πηλού και άλλων υλικών σε νερό. Τα ρευστά διάτρησης με βάση το νερό αποτελούνται από α) νερό, το οποίο αποτελεί την συνεχή φάση και παρέχει το αρχικό ιξώδες (φρέσκο ή θαλασσινό), β) ενεργά στερεά για την ενίσχυση του ιξώδους και του σημείου διαρροής (μπεντονίτης, που συνιστάται στην περίπτωση του φρέσκου νερού και ατταπουλγίτης, αμίαντος ή σιπιόλιθος, που συνιστώνται στην περίπτωση του θαλασσινού νερού), και γ) αδρανή στερεά για την επίτευξη της απαιτούμενης πυκνότητας (βαρύτης, θειούχος μόλυβδος, σιδηρομεταλλεύματα ή χαλαζιακά υλικά).Τα γεωτρητικά ρευστά αποτελούν το 10-20% του συνολικού κόστους κατά την διάρκεια μιας γεώτρησης. Ποσοστό πολύ υψηλό όταν μιλάμε για επενδύσεις εκκατομυρίων δολλαρίων. Λόγω των ολοένα πιο βαθιών αλλά και περίπλοκων γεωλογικών σχηματισμών υπάρχει τεράστια ανάγκη από την πετρελαική βιομηχανία για καινούργια και περισσότερο αποδοτικά γεωτρητικά ρευστά τα οποία θα μπορούν να ανταπεξέλθουν στα ολοένα και πιο απαιτητικά περβάλλοντα θερμοκρασίας και πίεσης. Τα σημαντικότερα ζητήματα τα οποία καλούνται να ανταποκριθούν τα ρευστά είναι οι ολοένα αυξανόμενες συνθήκες πίεσης και θερμοκρασίας στο υπέδαφος που είναι απόροια της αναζήτησης υδρογονανθράκων σε πλέον δύσβατες περιοχές με μεγαλύτερα βάθη που αυξάνουν τους κινδύνους και το κόστος για μια γεώτρηση. Η απώλεια ρευστού κυκλοφορίας (fluid loss) είναι ένα από τα σημαντικότερα και πλέον δαπανηρά προβλήματα κατά την διαδικασία μιας γεώτρησης. Ως απώλεια ρευστού κυκλοφορίας ορίζεται η συνολική ή μερική απώλεια των ρευστών της γεώτρησης σε εξαιρετικά διαπερατές ζώνες (porous sands), σε σπηλαιώδεις σχηματισμούς (cavernous zones), σε φυσικές ρηγματώσεις (natural fractures) και σε ρηγματώσεις προκαλούμενες κατά τη διάτρηση (induced fractures). Τα τελευταία χρόνια έχουν γίνει αρκετές προσπάθειες για την βελτίωση των γεωτρητικών ρευστών με την χρήση νανοσωματιδίων, τα οποία έχουν τη δυνατότητα να βελτιώσουν τις ιδιότητες των γεωτρητικών ρευστών όταν προστίθενται ακόμα και σε χαμηλές συγκεντρώσεις (<1 wt%). Οι μοναδικές τους ιδιότητες σχετίζονται με το μικρό τους μέγεθος και επομένως τον εξαιρετικά μεγάλο λόγο επιφάνειας προς όγκο.Σε αυτή την εργασία, εξετάστηκαν διάφορα εμπορικά νανοσωματίδια (Fe2O3, Fe3O4, SiO2) καθώς επίσης συντέθηκαν, με την μέθοδο της συγκαταβύθισης, νανοσωματιδία μαγνητίτη (custom-made Fe3O4), με και χωρίς επικάλυψη κιτρικού οξέος, τα οποία ερευνήθηκαν ως προς την ικανότητα τους να βελτιώσουν τις ρεολογικές ιδιότητες και την απώλεια ρευστών σε αιωρήματα μπετονίτη. Προκειμένου να χαρακτηρισθούν φυσικοχημικά τα αιωρήματα υπέστησαν ξήρανση με κοκκοποίηση σε θερμοκρασία υγρού Ν2 και κρυοξήρανση. Η μορφολογία, η κρυσταλλική δομή και οι επιφανειακές ομάδες των ξηρών κόνεων εξετάσθηκαν με ηλεκτρονική μικροσκοπία HR-TΕM, περίθλαση ακτίνων Χ (XRD), φυσική ρόφηση Ν2 και φασματοσκοπία FTIR. Οι αλληλεπιδράσεις των σωματιδίων μπετονίτη με τα νανοσωματίδια και οι διάφορες δομές που δημιουργούνται και πως τελικά αυτές επηρεάζουν τις ρεολογικές ιδιότητες των αιωρημάτων εξετάστηκαν με το HR-TEM στους 25°C και 60°C. Με βάση τις εικόνες από το HR-TEM, ένα μοντέλο αλληλεπιδράσεων μεταξύ των διαφορετικών τύπων νανοσωματιδίων και σωματιδίων μπετονίτη δημιουργήθηκε για πρώτη φορά για τέτοια αιωρήματα. Οι ρεολογικές ιδιότητες των παραγόμενων δειγμάτων εξετάστηκαν και σε συνθήκες ατμοσφαιρικής πίεσης (μέχρι 70°C) με την χρήση περιστροφικού ιξωδόμετρου (Grace M3600-Couette type geometry) αλλά και σε συνθήκες υψηλής πίεσης και θερμοκρασίας (69 bar-121°C) (Chandler 7600 HPHT viscometer). Το μοντέλο Herschel-Bulkley χρησιμοποιήθηκε για να περιγράψει τη μεταβολή του ιξώδους με τη μεταβολή των ρεολογικών παραμέτρων δείχνοντας εξαιρετική εφαρμογή για τις διαφορετικές πειραματικές μετρήσεις με συντελεστές συσχέτισης (R2) >0.99 σε όλες τις περιπτώσεις. Οι ρεολογικές μετρήσεις έδειξαν ότι η προσθήκη των νανοσωματιδίων βελτιώνει σημαντικά τις ρεολογικές ιδιότητες των αιωρημάτων μπετονίτη στις διάφορες συνθήκες πίεσης και θερμοκρασίας. Οι απώλειες ρευστών (fluid loss) εξετάστηκαν με φιλτροπρέσες υψηλής πίεσης και θερμοκρασίας (20.7 bar και 121°C) οι οποίες υπολογίζουν τον ρυθμό διήθησης του πολφού μέσω του χρησιμοποιούμενου φίλτρου (κεραμικός δίσκος). Η μεγαλύτερη μείωση στην απώλεια ρευστών επιτεύχθηκε για το δείγμα που περιείχε 0.5 wt% custom-made Fe3O4 με μείωση -40% σε σχέση με το αρχικό δείγμα μπετονίτη που δείχνει την τεράστια ικανότητα των νανοσωματιδίων να βελτιώσουν σημαντικά τις απώλειες ρευστών ακόμα και σε τόσο μικρές συγκεντρώσεις. Τέλος, εξετάστηκε η ικανότητα των παραγόμενων ρευστών να αλλάζουν τις ρεολογικές τους ιδιότητες υπό την επίδραση διάφορων μαγνητικών πεδίων (μέχρι 0.7 Tesla). Τα αποτελέσματα έδειξαν ότι τα καινούργια γεωτρητικά ρευστά έχουν την ικανότητα να αυξάνουν την τάση διολίσθησης (yield stress) έως και 300% σε σχέση με αυτή που μετρήθηκε χωρίς την εφαρμογή μαγνητικού πεδίου. Αυτό είναι κάτι πολύ σημαντικό που επιτρέπει την χρήση έξυπνων ρευστών (smart drilling fluids) τα οποία μπορούν να εξοικονομήσουν και χρόνο αλλά και κόστη κατά την διάρκεια μιας γεώτρησης.Τα νανοσωματίδια δείχνουν πολλές ελπιδοφόρες δυνατότητες σε εφαρμογές γεωτρήσεων αφού έχουν τη δυνατότητα να βελτιώσουν ή και να λύσουν το πρόβλημα της απώλειας ρευστών, όταν προστίθενται ακόμα και σε χαμηλές συγκεντρώσεις (>0.5 wt%), ενώ ταυτόχρονα βελτιστοποιούν τις ρεολογικές ιδιότητες των γεωτρητικών ρευστών. Η χρήση τους για την ανάπτυξη βελτιωμένων γεωτρητικών ρευστών υπόσχεται να αλλάξει την βιομηχανία των γεωτρήσεων και να την βοηθήσει να εξορυχθούν πολύπλοκοι γεωλογικοί σχηματισμοί πιο αποδοτικά αλλά και οικονομικά.


2021 ◽  
Author(s):  
Farqad Hadi ◽  
Ali Noori ◽  
Hussein Hussein ◽  
Ameer Khudhair

Abstract It is well known that drilling fluid is a key parameter for optimizing drilling operations, cleaning the hole, and managing the rig hydraulics and margins of surge and swab pressures. Although the experimental works present valid and reliable results, they are expensive and time consuming. On the other hand, continuous and regular determination of the rheological mud properties can perform its essential functions during well construction. More uncertainties in planning the drilling fluid properties meant that more challenges may be exposed during drilling operations. This study presents two predictive techniques, multiple regression analysis (MRA) and artificial neural networks (ANNs), to determine the rheological properties of water-based drilling fluid based on other simple measurable properties. While mud density (MW), marsh funnel (MF), and solid% are key input parameters in this study, the output functions or models are plastic viscosity (PV), yield point (YP), apparent viscosity (AV), and gel strength. The prediction methods were demonstrated by means of a field case in eastern Iraq, using datasets from daily drilling reports of two wells in addition to the laboratory measurements. To test the performance ability of the developed models, two error-based metrics (determination coefficient R2 and root mean square error RMSE) have been used in this study. The current results of this study support the evidence that MW, MF, and solid% are consistent indexes for the prediction of rheological properties. Both mud density and solid content have a relative-significant effect on increasing PV, YP, AV, and gel strength. However, a scattering around each fit curve is observed which proved that one rheological property alone is not sufficient to estimate other properties. The results also reveal that both MRA and ANN are conservative in estimating the fluid rheological properties, but ANN is more precise than MRA. Eight empirical mathematical models with high performance capacity have been developed in this study to determine the rheological fluid properties based on simple and quick equipment as mud balance and marsh funnel. This study presents cost-effective models to determine the rheological fluid properties for future well planning in Iraqi oil fields.


Sensors ◽  
2020 ◽  
Vol 20 (10) ◽  
pp. 2787
Author(s):  
Ahmed Gowida ◽  
Salaheldin Elkatatny ◽  
Khaled Abdelgawad ◽  
Rahul Gajbhiye

High-bentonite mud (HBM) is a water-based drilling fluid characterized by its remarkable improvement in cutting removal and hole cleaning efficiency. Periodic monitoring of the rheological properties of HBM is mandatory for optimizing the drilling operation. The objective of this study is to develop new sets of correlations using artificial neural network (ANN) to predict the rheological parameters of HBM while drilling using the frequent measurements, every 15 to 20 min, of mud density (MD) and Marsh funnel viscosity (FV). The ANN models were developed using 200 field data points. The dataset was divided into 70:30 ratios for training and testing the ANN models respectively. The optimized ANN models showed a significant match between the predicted and the measured rheological properties with a high correlation coefficient (R) higher than 0.90 and a maximum average absolute percentage error (AAPE) of 6%. New empirical correlations were extracted from the ANN models to estimate plastic viscosity (PV), yield point (YP), and apparent viscosity (AV) directly without running the models for easier and practical application. The results obtained from AV empirical correlation outperformed the previously published correlations in terms of R and AAPE.


2016 ◽  
Vol 835 ◽  
pp. 15-19 ◽  
Author(s):  
Yu Xiu An ◽  
Guan Cheng Jiang ◽  
You Rong Qi ◽  
Qing Ying Ge

In this paper, the nano flexible polymer was synthesized and the plugging property of the polymer in the drilling fluid was studied. The characterization and properties of nano flexible polymer were invested by Particle Size Analyzer and Transmission Electron Microscopy. The nano flexible polymer was synthesized successfully and it was flexible nano material both in water and in drilling fluid. The filtration ability of the polymer was studied by drilling fluid filter press and the results indicated that the filtration property was equal to commonly used fluid loss agent in drilling fluid. The plugging ability was studied by specific surface and porosity physical adsorption instrument (BET). The surface area reduced after treated with the polymer, indicating the nano flexible polymer entered into nanopores of shale formation due to the adsorption in the surface of shale. It was further exhibited that nanopores of shale were plugged by the nano flexible polymer.


Sign in / Sign up

Export Citation Format

Share Document