A Novel Micro Tensile Testing Instrument With Replaceable Testing Specimen of Gold and Aluminum by Parylene Passivation Technique

Author(s):  
Yung-Dong Lau ◽  
Hong Hocheng ◽  
Rongshun Chen ◽  
Weileun Fang

This study has successfully demonstrated a novel tensile testing approach to mount a thin film test specimen onto a MEMS instrument using microfabrication processes. The MEMS instrument consists of a thermal actuator, differential capacitance sensor, and supporting spring. The thermal actuator applies a tensile load on the test specimen to characterize the Young’s modulus and the residual stress of the thin film. As compare with the existing approaches, the problems and difficulties resulting from the alignment and assembly of a thin film test specimen with the testing instrument can be prevented. Furthermore, the parylene passivation technique with the MEMS fabrication process allows the user to change the test materials easily. In application, the present approach has been employed to determine the Young’s modulus and the residual stress of Au and Al films.

2007 ◽  
Vol 1052 ◽  
Author(s):  
Yung-Dong Lau ◽  
Tso-Chi Chang ◽  
Hong Hocheng ◽  
Rongshun Chen ◽  
Weileun Fang

AbstractThis study has successfully demonstrated a novel tensile testing approach to mount the thin film test specimen onto the MEMS instrument using microfabrication process. The MEMS instrument consists of thermal actuator, differential capacitance sensor, supporting spring. The thermal actuator applies tensile load on the test specimen to characterize the Young's modulus and the residual stress of thin films. As compare with the existing approaches, the problems and difficulties resulting from the alignment and assembly of thin film test specimens with the testing instrument can be prevented. Furthermore, the parylene passivation technique of MEMS fabrication process allows the changing of testing film materials easily. In application, the present approach has been employed to determine the Young's modulus and the residual stress of Al films.


2003 ◽  
Vol 795 ◽  
Author(s):  
Wang-Shen Su ◽  
Weileun Fang ◽  
Ming-Shih Tsai

ABSTRACTThis study reported a novel method for tuning thin film mechanical properties by means of plasma surface modification. In order to demonstrate the feasibility of this approach, various plasma treatments, including O2, H2, NH3 atmospheres, were implemented to tune the Young's modulus and residual stress of SiO2 film. Without plasma treatment, the static tip deflection of 200μm long SiO2 cantilever was 9.01μm. After treatment with H2, O2, and NH3 plasma, the tip deformation of the treated cantilevers became 10.22μm, 8.28μm, and -6.84μm respectively. The Young's modulus of the SiO2 cantilever without plasma treatment was 76.3GPa. After treated with H2, O2, NH3 plasma, the Young's modului of those treated cantilevers became 70.8 GPa, 74.7 GPa, and 71.4 GPa, respectively. Hence, after H2 and NH3 plasma treatment, the equivalent elastic modulus of SiO2 cantilever could be reduced about 7%.


2014 ◽  
Vol 23 (1-2) ◽  
pp. 15-19 ◽  
Author(s):  
Khaled A. Alnefaie

AbstractCarbon nanotubes (CNTs) were fabricated using low-pressure chemical vapor deposition and then embedded in epoxy polymer at several weight ratios, 0, 0.75, 1.5, and 3 wt%, for tensile testing and Young’s modulus determination using an Instron machine. The tensile strength and Young’s modulus of the epoxy resin were increased with the addition of CNTs to a certain extent, and then decreased with the increase in the weight fraction of CNTs. The best properties occurred at 1.5 wt% of CNTs. Scanning electron microscopy was used to reveal the dispersion status of CNTs in the nanocomposites.


2004 ◽  
Vol 15 (12) ◽  
pp. 2389-2394 ◽  
Author(s):  
Z M Zhou ◽  
Y Zhou ◽  
C S Yang ◽  
J A Chen ◽  
G F Ding ◽  
...  

1999 ◽  
Vol 594 ◽  
Author(s):  
T. Y. Zhang ◽  
Y. J. Su ◽  
C. F. Qian ◽  
M. H. Zhao ◽  
L. Q. Chen

AbstractThe present work proposes a novel microbridge testing method to simultaneously evaluate the Young's modulus, residual stress of thin films under small deformation. Theoretic analysis and finite element calculation are conducted on microbridge deformation to provide a closed formula of deflection versus load, considering both substrate deformation and residual stress in the film. Silicon nitride films fabricated by low pressure chemical vapor deposition on silicon substrates are tested to demonstrate the proposed method. The results show that the Young's modulus and residual stress for the annealed silicon nitride film are respectively 202 GPa and 334.9 MPa.


2008 ◽  
Vol 33-37 ◽  
pp. 969-974 ◽  
Author(s):  
Bong Bu Jung ◽  
Seong Hyun Ko ◽  
Hun Kee Lee ◽  
Hyun Chul Park

This paper will discuss two different techniques to measure mechanical properties of thin film, bulge test and nano-indentation test. In the bulge test, uniform pressure applies to one side of thin film. Measurement of the membrane deflection as a function of the applied pressure allows one to determine the mechanical properties such as the elastic modulus and the residual stress. Nano-indentation measurements are accomplished by pushing the indenter tip into a sample and then withdrawing it, recording the force required as a function of position. . In this study, modified King’s model can be used to estimate the mechanical properties of the thin film in order to avoid the effect of substrates. Both techniques can be used to determine Young’s modulus or Poisson’s ratio, but in both cases knowledge of the other variables is needed. However, the mathematical relationship between the modulus and Poisson's ratio is different for the two experimental techniques. Hence, achieving agreement between the techniques means that the modulus and Poisson’s ratio and Young’s modulus of thin films can be determined with no a priori knowledge of either.


2012 ◽  
Vol 18 (7-8) ◽  
pp. 945-953 ◽  
Author(s):  
Oliver Pabst ◽  
Michael Schiffer ◽  
Ernst Obermeier ◽  
Tolga Tekin ◽  
Klaus Dieter Lang ◽  
...  

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