Intrinsic Heat Treatment Induced Graded Surficial Microstructure and Tribological Properties of Selective Laser Melted Titanium

2021 ◽  
Vol 143 (5) ◽  
Author(s):  
Nan Kang ◽  
Nicolas Coniglio ◽  
Yang Cao ◽  
Chunling Zhao ◽  
Mohamed El Mansori ◽  
...  
Keyword(s):  
Heat Treatment ◽  
Lath Martensite ◽  
Microstructural Characterization ◽  
Layer By Layer ◽  
Element Analysis ◽  
Near Surface ◽  
The Coefficient Of Friction ◽  
Cp Ti ◽  
Region Ii ◽  
Specific Sliding

Abstract In the course of the selective laser melting (SLM) process, the part is built layer by layer involving partial remelting/heating of the previous layer, called as intrinsic heat treatment. Therefore, superficial properties of as-built parts are somewhat different from that of the inside of the part. In this work, the nano-tribological behavior of the commercial pure Ti (CP-Ti) sample built using SLM was investigated considering the near-surface regions with focus on the effect of intrinsic heat treatment. Microstructure and nano-testing allow identifying specific sliding behaviors in three attitude regions: (I) surface (0–50 µm), (II) subsurface (50–200 µm), and (III) inner-part (below 200 µm). The average hardness drops slightly when moving from Regions I and II (3.35 GPa) to Region III (3.09 GPa). The coefficient of friction (COF) values vary from 0.18 to 0.45 for all three regions, and the Region III presents highest worn trace width of 5.8 μm. Regions I and III promote a stick-and-slip behavior while sliding is smooth and continuous in Region II. This gradient microstructural characterization enables associating the behavior of Region II to large-sized lath martensite α′ morphology, which is different from the Regions I and III with finer microstructure. A finite element analysis (FEA) thermal model suggests that the existence of the three identified regions is the consequence of the intrinsic heat treatment induced by the SLM process, in which the remelting/heating and recrystallization have been considered as the main reasons for microstructure coarsening and refinement between Regions I and II, Regions II and III, respectively.

Development and Characterization of New Ti-25Ta-Zr Alloys for Biomedical Applications

2021 ◽  
Vol 1016 ◽  
pp. 137-144
Author(s):  
Pedro Akira Bazaglia Kuroda ◽  
Fernanda de Freitas Quadros ◽  
Mycaela Vieira Nascimento ◽  
Carlos Roberto Grandini
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Elastic Modulus ◽  
Biomedical Applications ◽  
Solution Heat Treatment ◽  
High Hardness ◽  
Microstructural Characterization ◽  
Β Phase ◽  
Cp Ti ◽  
Microscopy Techniques

This paper deals with the study of the development, structural and microstructural characterization and, selected mechanical properties of Ti-25Ta-50Zr alloy for biomedical applications. The alloy was melted in an arc furnace and various solution heat treatments were performed to analyze the influence of the temperature and time on the structure, microstructure, microhardness and elastic modulus of the samples. The structural and microstructural results, obtained by X-ray diffraction and microscopy techniques, showed that the solution heat treatment performed at high temperatures induces the formation of the β phase, while solution heat treatment performed at low temperatures induces the formation of the α” and ω metastable phases. Regarding the effect of time, samples subjected to heat treatment for 6 hours have only the β phase, indicating that lengthy treatments suppress the α” phase. Regarding the hardness and elastic modulus, the alloy with the α” and ω phases, after treatment performed at a temperature of 500 °C, has a high hardness value and elastic modulus due to the presence of the ω phase that hardens and weakens alloys. The titanium alloys developed in this study have excellent mechanical properties results for use in the orthopedic area, better than many commercial materials such as cp-Ti, stainless steel and Co-Cr alloys.

Microstructural characterization of CoPtCr/Cr thin film disks by cross-section TEM and elongated probe micro-diffraction

1991 ◽  
Vol 49 ◽  
pp. 762-763
Author(s):  
M.A. Parker ◽  
K.E. Johnson ◽  
C. Hwang ◽  
A. Bermea
Keyword(s):  
Magnetic Recording ◽  
Electron Probe ◽  
Microstructural Characterization ◽  
Crystallographic Structure ◽  
Recording Media ◽  
Layer By Layer ◽  
Cross Sectional ◽  
New Techniques ◽  
Polished Side

We have reported the dependence of the magnetic and recording properties of CoPtCr recording media on the thickness of the Cr underlayer. It was inferred from XRD data that grain-to-grain epitaxy of the Cr with the CoPtCr was responsible for the interaction observed between these layers. However, no cross-sectional TEM (XTEM) work was performed to confirm this inference. In this paper, we report the application of new techniques for preparing XTEM specimens from actual magnetic recording disks, and for layer-by-layer micro-diffraction with an electron probe elongated parallel to the surface of the deposited structure which elucidate the effect of the crystallographic structure of the Cr on that of the CoPtCr.XTEM specimens were prepared from magnetic recording disks by modifying a technique used to prepare semiconductor specimens. After 3mm disks were prepared per the standard XTEM procedure, these disks were then lapped using a tripod polishing device. A grid with a single 1mmx2mm hole was then glued with M-bond 610 to the polished side of the disk.

scholarly journals Optimization Study of Post-Weld Heat Treatment for 12Cr1MoV Pipe Welded Joint

Metals ◽  
2021 ◽  
Vol 11 (1) ◽  
pp. 127
Author(s):  
Zichen Liu ◽  
Xiaodong Hu ◽  
Zhiwei Yang ◽  
Bin Yang ◽  
Jingkai Chen ◽  
...  
Keyword(s):  
Heat Treatment ◽  
Residual Stress ◽  
Stress Reduction ◽  
Simulation Method ◽  
Post Weld Heat Treatment ◽  
Residual Stress Field ◽  
Element Analysis ◽  
Tempering Treatment ◽  
Temper Heat Treatment ◽  
Weld Heat

In order to clarify the role of different post-weld heat treatment processes in the manufacturing process, welding tests, post-weld heat treatment tests, and finite element analysis (FEA) are carried out for 12C1MoV steel pipes. The simulated temperature field and residual stress field agree well with the measured results, which indicates that the simulation method is available. The influence of post-weld heat treatment process parameters on residual stress reduction results is further analyzed. It is found that the post weld dehydrogenation treatment could not release residual stress obviously. However, the residual stress can be relieved by 65% with tempering treatment. The stress relief effect of “post weld dehydrogenation treatment + temper heat treatment” is same with that of “temper heat treatment”. The higher the temperature, the greater the residual stress reduction, when the peak temperature is at 650–750 °C, especially for the stress concentration area. The longer holding time has no obvious positive effect on the reduction of residual stress.

scholarly journals Evaluation on the Bond Capacity of the Fire-Protected FRP Bonded to Concrete Under High Temperature

2021 ◽  
Vol 15 (1) ◽  
Author(s):  
Soo-yeon Seo ◽  
Jong-wook Lim ◽  
Su-hyun Jeong
Keyword(s):  
High Temperature ◽  
Critical Temperature ◽  
Temperature Variation ◽  
Fire Resistance ◽  
Fire Protection ◽  
Element Analysis ◽  
External Temperature ◽  
Near Surface ◽  
Board Type ◽  
The Face

AbstractTo figure out the change in the reinforcing effect of FRP system used for the retrofit of RC beam when it is exposed to high temperature, it is required to evaluate not only the behavior of the entire beam, but also the bond performance at anchorage zone through a bond test according to the increase of external temperature. Moreover, the study to find various fire-protection methods is necessary to prevent the epoxy from reaching the critical temperature during an exposure to high temperature. In this manner, the fire-resistance performances of externally bonded (EB) FRP and near-surface-mounted (NSM) FRP to concrete block were evaluated by high-temperature exposure tests after performing a fire-protection on the surface in this paper. Board-type insulation with mortar was considered for the fire-protection of FRP system. After the fire-protection of the FRPs bonded to concrete blocks, an increasing exposure temperature was applied to the specimens with keeping a constant shear bond stress between concrete and the FRP. Based on the result, the temperature when the bond strength of the FRP disappears was evaluated. In addition, a finite element analysis was performed to find a proper method for predicting the temperature variation of the epoxy which is fire-protected with board-type insulation during the increase of external temperature. As a result of the test, despite the same fire-protection, NSM specimens were able to resist 1.54–2.08 times higher temperature than EB specimens. In the design of fire-protection of FRP system with the board-type insulation, it is necessary to consider the transfer from sides as well as the face with FRP. If there is no insulation of FP boards on the sides, the epoxy easily reaches its critical temperature by the heat penetrated to the sides, and increasing the thickness of the FP board alone for the face with FRP does not increase the fire-resistance capacity. As a result of the FE analysis, the temperature variation at epoxy can be predicted using the analytical approach with the proper thermal properties of FP mortar and board.

scholarly journals The Effect of Co-Deposition of SiC Sub-Micron Particles and Heat Treatment on Wear Behaviour of Ni–P Coatings

Coatings ◽  
2021 ◽  
Vol 11 (2) ◽  
pp. 180
Author(s):  
Donya Ahmadkhaniha ◽  
Lucia Lattanzi ◽  
Fabio Bonora ◽  
Annalisa Fortini ◽  
Mattia Merlin ◽  
...  
Keyword(s):  
Heat Treatment ◽  
Friction Coefficient ◽  
Wear Mechanisms ◽  
Composite Coatings ◽  
Wear Behaviour ◽  
Maximum Hardness ◽  
Sic Particles ◽  
Heat Treated ◽  
The Coefficient Of Friction ◽  
The Difference

The purpose of the study is to assess the influence of SiC particles and heat treatment on the wear behaviour of Ni–P coatings when in contact with a 100Cr6 steel. Addition of reinforcing particles and heat treatment are two common methods to increase Ni–P hardness. Ball-on-disc wear tests coupled with SEM investigations were used to compare as-plated and heat-treated coatings, both pure and composite ones, and to evaluate the wear mechanisms. In the as-plated coatings, the presence of SiC particles determined higher friction coefficient and wear rate than the pure Ni–P coatings, despite the limited increase in hardness, of about 15%. The effect of SiC particles was shown in combination with heat treatment. The maximum hardness in pure Ni–P coating was achieved by heating at 400 °C for 1 h while for composite coatings heating for 2 h at 360 °C was sufficient to obtain the maximum hardness. The difference between the friction coefficient of composite and pure coatings was disclosed by heating at 300 °C for 2 h. In other cases, the coefficient of friction (COF) stabilised at similar values. The wear mechanisms involved were mainly abrasion and tribo-oxidation, with the formation of lubricant Fe oxides produced at the counterpart.

scholarly journals Multi-Stage Cold Forging Process for Manufacturing a High-Strength One-Body Input Shaft

Materials ◽  
2021 ◽  
Vol 14 (3) ◽  
pp. 532
Author(s):  
A Jo ◽  
Myeong Jeong ◽  
Sang Lee ◽  
Young Moon ◽  
Sun Hwang
Keyword(s):  
High Strength ◽  
Microstructural Characterization ◽  
Fatigue Tests ◽  
Machining Process ◽  
Cold Forging ◽  
Element Analysis ◽  
Forging Process ◽  
Input Shaft ◽  
Multi Stage ◽  
The One

A multi-stage cold forging process was developed and complemented with finite element analysis (FEA) to manufacture a high-strength one-body input shaft with a long length body and no separate parts. FEA showed that the one-body input shaft was manufactured without any defects or fractures. Experiments, such as tensile, hardness, torsion, and fatigue tests, and microstructural characterization, were performed to compare the properties of the input shaft produced by the proposed method with those produced using the machining process. The ultimate tensile strength showed a 50% increase and the torque showed a 100 Nm increase, confirming that the input shaft manufactured using the proposed process is superior to that processed using the machining process. Thus, this study provides a proof-of-concept for the design and development of a multi-stage cold forging process to manufacture a one-body input shaft with improved mechanical properties and material recovery rate.

Three Turnaround Heat Treating Studies

2003 ◽  
Author(s):  
Jaan Taagepera ◽  
Marty Clift ◽  
D. Mike DeHart ◽  
Keneth Marden
Keyword(s):  
Heat Treatment ◽  
Finite Element Analysis ◽  
Finite Element ◽  
Thermal Stress ◽  
Thermal Stresses ◽  
Heat Treating ◽  
Element Analysis ◽  
Stress Profiles ◽  
Insight Into

Three vessel modifications requiring heat treatment were analyzed prior to and during a planned turnaround at a refinery. One was a thick nozzle that required weld build up. This nozzle had been in hydrogen service and required bake-out to reduce the potential for cracking during the weld build up. Finite element analysis was used to study the thermal stresses involved in the bake-out. Another heat treatment studied was a PWHT of a nozzle replacement. The heat treatment band and temperature were varied with location in order to minimize cost and reduction in remaining strength of the vessel. Again, FEA was used to provide insight into the thermal stress profiles during heat treatment. The fmal heat treatment study was for inserting a new nozzle in a 1-1/4Cr-1/2Mo reactor. While this material would ordinarily require PWHT, the alteration was proposed to be installed without PWHT. Though accepted by the Jurisdiction, this nozzle installation was ultimately cancelled.

Determination of Critical Crack Size Utilizing a Fracture Mechanics Test in Equipment Under Fatigue

2009 ◽  
Author(s):  
Irene Garcia Garcia ◽  
Radoslav Stefanovic
Keyword(s):  
Heat Treatment ◽  
Fracture Mechanics ◽  
Crack Size ◽  
Operational Experience ◽  
Element Analysis ◽  
Critical Crack ◽  
Circumferential Welds ◽  
Fea Model ◽  
Critical Crack Size

Equipment that is exposed to severe operational pressure and thermal cycling, like coke drums, usually suffer fatigue. As a result, equipment of this sort develop defects such as cracking in the circumferential welds. Operating companies are faced with the challenges of deciding what is the best way to prevent these defects, as well as determining how long they could operate if a defect is discovered. This paper discusses a methodology for fracture mechanics testing of coke drum welds, and calculations of the critical crack size. Representative samples are taken from production materials, and are welded employing production welding procedures. The material of construction is 1.25Cr-0.5Mo low alloy steel conforming to ASME SA-387 Gr 11 Class 2 in the normalized and tempered condition (N&T). Samples from three welding procedures (WPS) are tested: one for production, one for a repair with heat treatment, and one for repair without heat treatment. The position and orientation of test specimen are chosen based on previous surveys and operational experience on similar vessels that exhibited cracks during service. Fracture mechanics toughness testing is performed. Crack finite element analysis (FEA) model is used to determine the path-independed JI-integral driving force. Methodology for the determination of critical crack size is developed.

Performance of Low-Cost 3D Printer in Medical Application

2021 ◽  
Author(s):  
Nor Aiman Sukindar ◽  
Azib Azhari Awang Dahan ◽  
Sharifah Imihezri Syed Shaharuddin ◽  
Nor Farah Huda Abd Halim
Keyword(s):  
Low Cost ◽  
Medical Application ◽  
Fused Deposition Modelling ◽  
3D Printer ◽  
Layer By Layer ◽  
Total Deformation ◽  
Element Analysis ◽  
Porosity Level ◽  
Fused Deposition ◽  
Printing Parameters

Abstract Fused Deposition Modelling (FDM) is an additive manufacturing (AM) process that produces a physical object directly from a CAD design using layer-by-layer deposition of the filament material that is extruded via a nozzle. In industry, FDM has become one of the most used AM processes for the production of low batch quantity and functional prototypes, due to its safety, efficiency, reliability, low cost, and ability to process manufacturing-grade engineering thermoplastic. Recently, the market is flooded with the availability of low-cost printers produced by numerous companies. This research aims to investigate the effect of different porosity levels on a scaffold structure produced using a low-cost 3D printer. Comparisons of these porous structures were made in terms of Von-Mises strain, total deformation, as well as compressive stress. Various porosity levels were created by varying printing parameters, including layer height, infill density, and shell thickness by slicing the initial solid CAD file using Repetier Host 3D printing software. Finite Element Analysis (FEA) simulation was then performed on the created scaffold structures by using Ansys Workbench 19.2. The simulation result indicates that the greater porosity level will result in higher total deformation of the structure. Meanwhile, the compression test shows that the minimum strength value obtained was favourable at 22 MPa and had exceeded that of the trabecular femur (15 MPa). However, its porosity level (maximum at 52%) was still below that of the minimum threshold of porosity level of 70 percent. However, the printing parameters currently used can be adjusted in the future. Therefore, it was deduced that the low-cost 3D printer offers promising potential to fabricate different porosity structures with multiple outcomes.

The Site Tilt and Lander Transfer Function from the Short-Period Seismometer of InSight on Mars

2021 ◽  
Author(s):  
Alexander E. Stott ◽  
Constantinos Charalambous ◽  
Tristram J. Warren ◽  
William T. Pike ◽  
Robert Myhill ◽  
...  
Keyword(s):  
Young’S Modulus ◽  
Young's Modulus ◽  
Dust Devils ◽  
Total Change ◽  
Noise Sources ◽  
Element Analysis ◽  
Near Surface ◽  
Seismic Experiment ◽  
Short Period ◽  
Sensitivity Changes

ABSTRACT The National Aeronautics and Space Administration InSight mission has deployed the seismic experiment, SEIS, on the surface of Mars, and has recorded a variety of signals including marsquakes and dust devils. This work presents results on the tilt and local noise sources, which provide context to aid interpretation of the observed signals and allow an examination of the near-surface properties. Our analysis uses data recorded by the short-period sensors on the deck, throughout deployment and in the final configuration. We use thermal decorrelation to provide an estimate of the sol-to-sol tilt. This tilt is examined across deployment and over a Martian year. After each modification to the site, the tilt is seen to stabilize over 3–20 sols depending on the action, and the total change in tilt is <0.035°. Long-term tilt over a Martian year is limited to <0.007°. We also investigate the attenuation of lander-induced vibrations between the lander and SEIS. Robotic arm motions provide a known lander source in the 5–9 Hz bandwidth, yielding an amplitude attenuation of lander signals between 100 and 1000 times. The attenuation of wind sensitivity from the deck to ground presents a similar value in the 1.5–9 Hz range, thus favoring a noise dominated by lander vibrations induced by the wind. Wind sensitivities outside this bandwidth exhibit different sensitivity changes, indicating a change in the coupling. The results are interpreted through a finite-element analysis of the regolith with a depth-dependent Young’s modulus. We argue that discrepancies between this model and the observations are due to local compaction beneath the lander legs and/or anelasticity. An estimate for the effective Young’s modulus is obtained as 62–81 MPa, corroborating previous estimates for the top layer duricrust.

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