Stress–Strain Relationship of Polycaprolactone in Liquid Nitrogen for Finite Element Simulation of Cryogenic Micropunching Process

Author(s):  
Amrit Sagar ◽  
Christopher Nehme ◽  
Anil Saigal ◽  
Thomas P. James

Abstract In pursuit of research to create a synthetic tissue scaffold by a micropunching process, material properties of polycaprolactone (PCL) in liquid nitrogen were determined experimentally and used for finite element modeling of cryogenic micropunching process. Specimens were prepared using injection molding and tested under compression to determine the stress–strain relationship of PCL below its glass transition temperature. Cryogenic conditions were maintained by keeping the PCL specimens submerged in liquid nitrogen throughout the loading cycle. Specimens of two different aspect ratios were used for testing. Yield strength, strength coefficient, and strain hardening exponent were determined for different specimen aspect ratios and extrapolated for the case with zero diameter to length ratio. Material properties were also determined at room temperature and compared against results available in the literature. Results demonstrate that PCL behaves in a brittle manner at cryogenic temperatures with more than ten times increase in Young's modulus from its value at room temperature. The results were used to predict punching forces for the design of microscale hole punching dies and for validation of a microscale hole punching model that was created with a commercially available finite element software package, deform 3D. The three parameters, yield strength, strength coefficient, and strain hardening exponent, used in Ludwik's equation to model flow stress of PCL in deform 3D were determined to be 94.8 MPa, 210 MPa, and 0.54, respectively. The predicted peak punching force from finite element simulations matched with experimentally determined punching force results.

Author(s):  
Amrit Sagar ◽  
Christopher Nehme ◽  
Anil Saigal ◽  
Thomas P. James

Abstract In pursuit of research to create a synthetic tissue scaffold by a micropunching process, material properties of Polycaprolactone (PCL) in liquid nitrogen were determined experimentally. Specimens were prepared using injection molding and tested under compression to determine the stress-strain relationship of PCL below its glass transition temperature. Cryogenic conditions were maintained by keeping the PCL specimens submerged in liquid nitrogen throughout the loading cycle. Specimens of two different aspect ratios were used for testing. Yield Strength, Strength Coefficient, and Strain Hardening Exponent were determined for different specimen aspect ratios and extrapolated for the case with zero diameter to length ratio. Material properties were also determined at room temperature and compared against results available in the literature. Results demonstrate that PCL behaves in a brittle manner at cryogenic temperatures with more than ten times increase in Young’s modulus from its value at room temperature. The results were used to predict punching forces for the design of microscale hole punching dies and for validation of a microscale hole punching model that was created with a commercially available finite element software package, DEFORM 3D. The three parameters Yield Strength, Strength Coefficient, and Strain Hardening Exponent used in Ludwik’s equation to model flow stress of PCL in DEFORM 3D were determined to be 94.8 MPa, 210 MPa, and 0.54, respectively.


2008 ◽  
Vol 130 (4) ◽  
Author(s):  
Vishnu Verma ◽  
A. K. Ghosh ◽  
G. Behera ◽  
Kamal Sharma ◽  
R. K. Singh

The miniature disk bending test is used to evaluate the mechanical behavior of irradiated materials and their properties (e.g., yield stress and strain hardening exponent) to determine mainly ductility loss in steel due to irradiation from the load-deflection behavior of the disk specimen. In the miniature disk bending machine the specimen is firmly held between the two horizontal jaws of punch, and an indentor with a spherical ball travels vertically. Analytical solutions for large amplitude plastic deformation become rather unwieldy. Hence, a finite element analysis has been carried out. The finite element model considers contact between the indentor and test specimen, friction between various pairs of surfaces, and elastic plastic behavior. This paper presents the load versus deflection results of a parametric study where the values of various parameters defining the material properties have been varied by ±10% around the base values. Some well-known analytical solutions to this problem have also been considered. It is seen that the deflection obtained by analytical elastic bending theory is significantly lower than that obtained by the elastoplastic finite element solution at relatively small values of load. The finite element solution has been compared with one experimental result and values are in reasonably good agreement. With these results it will be possible to determine the material properties from the experimentally obtained values of load and deflection.


2021 ◽  
Vol 15 (1) ◽  
pp. 7662-7670
Author(s):  
N. Ali ◽  
M.S. Mustapa ◽  
T. Sujitno ◽  
T.E. Putra ◽  
Husaini .

This research aims to study the behavior of monotonic and cyclic plastic deformation on commercially pure titanium which has undergone surface treatment using the nitrogen ion implantation method. The doses of 2.0×1017 ions/cm2 and the energy of 100 keV were used to implant the nitrogen ions into the CpTi. Monotonic properties tests were performed in a laboratory air and at room temperature using ASTM E8 standard specimens. Fatigue and corrosion fatigue tests were conducted in a laboratory  air and in artificial saline solutions, at room temperature using ASTM 1801-97 specimens. Tensile tests were carried out with constant displacement rate and fatigue tests were carried under fully-reversed with stress-controlled conditions with stress amplitudes 230, 240, 250, 260, 270 and 280 MPa. The results showed the material properties of monotonic behavior for CpTi and Nii-Ti; tensile strength (σu) of 497 and 539 MPa and for 0.2% offset yield strength (σy) of 385 and 440 MPa, respectively and of cyclic behavior; cyclic strength coefficient (k’) of 568.41 and 818.64 and cyclic strain hardening exponent (n’) of 0.176 and 0.215, respectively. This study has succeeded in producing useful new material properties that will contribute to the field of material science and engineering.


2017 ◽  
Vol 898 ◽  
pp. 741-748 ◽  
Author(s):  
Meng Li ◽  
Hong Zhang ◽  
Meng Ying Xia ◽  
Kai Wu ◽  
Jing Tian Wu ◽  
...  

Due to the harsh environment for submarine pipelines, corrosion damage of the pipeline steels is inevitable. After the corrosion damage, pipelines are prone to failure and may cause serious consequences. The analysis of the effects of different steel properties on the collapse pressure of pipelines with corrosion defects is of importance for the option of appropriate pipeline and avoiding accidents. Based on the finite element method, the finite element model of the pipeline with defects under external pressure was built. Firstly, the accuracy of the numerical model was validated by comparing with previous experimental results. The effects of yield strength and strain hardening exponent on collapse pressure of pipelines with different sizes of defect were discussed in detail. Results showed that the yield strength and strain hardening exponent have different influences on collapse pressure: the collapse pressure increases with the increasing yield strength, and the collapse pressure decreases with the increasing strain hardening exponent.


Author(s):  
D G Walsh ◽  
A A Torrance ◽  
J Tiberg

Although thermally induced tensile residual stresses have been known to occur in ground components, it has not been possible to predict the critical temperature at which these stresses begin to manifest themselves in the workpiece. In this paper, a model of the formation of thermally induced tensile residual stresses is proposed and a simple method of calculating the critical temperature above which tensile residual stresses occur is developed. The analysis makes use of dimensional methods to characterize the critical temperature. In addition, a formula characterizing the yield strength as a function of temperature was developed. The model was then validated using finite element techniques and some experimental data. The analysis reveals that it is possible to determine the critical temperature above which tensile residual stresses will be manifested based on readily available material properties. A case study illustrates the application of the technique.


2000 ◽  
Author(s):  
G. T. Kridli ◽  
L. Bao ◽  
P. K. Mallick

Abstract The tube hydroforming process has been used in industry for several years to produce components such as exhaust manifolds. Recent advances in forming machines and machine control systems have allowed for the introduction and the implementation of the process to produce several automotive components, which were originally produced by the stamping process. Components such as side rails, engine cradles, space frames, and several others can be economically produced by tube hydroforming. The process involves forming a straight or a pre-bent tube into a die cavity using internal hydraulic pressure, which may be coupled with controlled axial feeding of the tube. One of the remaining challenges facing product and process engineers in designing hydroformed parts is the lack of an extensive knowledge base of the process. This includes a full understanding of the process mechanics and the effects of the material properties on the quality of the hydroformed product. This paper reports on the results of two dimensional plane strain finite element models of the tube hydroforming process, which were conducted using the commercial finite element code ABAQUS/Standard. The objective of the study is to examine the effects of material properties, die geometry, and frictional characteristics on the selection of the hydroforming process parameters. The paper discusses the effects of the strain-hardening exponent, friction coefficient at the die-workpiece interface, initial tube wall thickness, and die corner radii on the thickness distribution of the hydroformed tube.


2015 ◽  
Vol 665 ◽  
pp. 97-100 ◽  
Author(s):  
Marko Katinic ◽  
Drazan Kozak ◽  
Ivan Samardzic ◽  
Antun Stoic ◽  
Zeljko Ivandic ◽  
...  

The interaction behavior of twin collinear through-wall cracks in tension loaded plate under elastic-plastic condition is investigated by the finite element method (FEM). The fracture parameter J integral for interacting cracks is calculated and compared to the J integral for a single crack the same size. In this way, the interaction factor of cracks under elastic-plastic condition is defined. This interaction factor is compared to the results of analytical solution of the interaction factor under linear elastic condition. The results show that interaction factor of cracks under elastic-plastic condition is higher than interaction factor of same cracks under linear elastic condition. Also the interaction effect of cracks under elastic-plastic condition is influenced not only by the crack configurations but also by the material properties, especially the strain hardening exponent n.


2012 ◽  
Vol 135 (1) ◽  
Author(s):  
M. R. Hardisty ◽  
R. Zauel ◽  
S. M. Stover ◽  
D. P. Fyhrie

As the average age of the population has increased, the incidence of age-related bone fracture has also increased. While some of the increase of fracture incidence with age is related to loss of bone mass, a significant part of the risk is unexplained and may be caused by changes in intrinsic material properties of the hard tissue. This investigation focused on understanding how changes to the intrinsic damage properties affect bone fragility. We hypothesized that the intrinsic (μm) damage properties of bone tissue strongly and nonlinearly affect mechanical behavior at the apparent (whole tissue, cm) level. The importance of intrinsic properties on the apparent level behavior of trabecular bone tissue was investigated using voxel based finite element analysis. Trabecular bone cores from human T12 vertebrae were scanned using microcomputed tomography (μCT) and the images used to build nonlinear finite element models. Isotropic and initially homogenous material properties were used for all elements. The elastic modulus (Ei) of individual elements was reduced with a secant damage rule relating only principal tensile tissue strain to modulus damage. Apparent level resistance to fracture as a function of changes in the intrinsic damage properties was measured using the mechanical energy to failure per unit volume (apparent toughness modulus, Wa) and the apparent yield strength (σay, calculated using the 0.2% offset). Intrinsic damage properties had a profound nonlinear effect on the apparent tissue level mechanical response. Intrinsic level failure occurs prior to apparent yield strength (σay). Apparent yield strength (σay) and toughness vary strongly (1200% and 400%, respectively) with relatively small changes in the intrinsic damage behavior. The range of apparent maximum stresses predicted by the models was consistent with those measured experimentally for these trabecular bone cores from the experimental axial compressive loading (experimental: σmax = 3.0–4.3 MPa; modeling: σmax = 2–16 MPa). This finding differs significantly from previous studies based on nondamaging intrinsic material models. Further observations were that this intrinsic damage model reproduced important experimental apparent level behaviors including softening after peak load, microdamage accumulation before apparent yield (0.2% offset), unload softening, and sensitivity of the apparent level mechanical properties to variability of the intrinsic properties.


Author(s):  
Wenping Song ◽  
Longqiu Li ◽  
Andrey Ovcharenko ◽  
Ding Jia ◽  
Guangyu Zhang ◽  
...  

Yield inception of a coated substrate indented by a rigid sphere is analyzed using finite element analysis. The critical interference is studied as a function of film thickness and material properties of both the film and the substrate. The results show that critical interference, corresponding to yield inception of the coated substrate, is a strong function of the film thickness, the Young’s modulus, and the yield strength of both the film and the substrate.


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