Elastic and Plastic Microscopic Undulation on the Surface of Polycrystalline Pure Titanium Under Tension

2017 ◽  
Vol 139 (6) ◽  
Author(s):  
Naoya Tada ◽  
Takeshi Uemori ◽  
Toshiya Nakata

Commercial pure titanium has been widely used in the aerospace, chemical, and biomedical industries because of its light weight, high corrosion resistance, high strength, high heat resistance, and good biocompatibility. Pure titanium takes the form of a hexagonal closed-pack structure with anisotropic elasticity and plasticity, with most of its components being polycrystalline aggregates having different crystal orientations. Small mechanical loading under elastic conditions therefore always induces inhomogeneous microscopic deformation, and the resulting inhomogeneity brings about various defects such as inhomogeneous plastic deformation, microcracking, and necking. It is therefore important to investigate the microscopic inhomogeneous deformation under elastic and plastic conditions. In this study, a plate specimen of commercial pure titanium was subjected to a tensile test on the stage of a digital holographic microscope (DHM), and the microscopic deformation of grains in the specimen under elastic and plastic conditions were observed and measured. During the test, the grains’ height distribution was measured in a fixed area on the specimen’s surface at each tensile loading step, and the correlation between height distributions at different loads was examined. We found from the measurements that each grain shows a different height change even under elastic conditions with a small load. This inhomogeneous height change was enhanced as the load was increased to plastic conditions. A strong correlation between the height changes under elastic and plastic conditions was also found. This result suggests that the microscopic deformation experienced under plastic conditions is predictable from that observed under elastic conditions.

Author(s):  
Naoya Tada ◽  
Yuki Doi

Commercial pure titanium has been widely used in aerospace, chemical, and biomedical industries for its lightweight, high corrosion resistance, high strength, high heat resistance and good biocompatible properties. Pure titanium takes hexagonal closed-pack structure with anisotropic elasticity and plasticity, and most of the components are polycrystalline aggregate with different crystal orientations. Therefore, inhomogeneous microscopic deformation always occurs by mechanical loading from the elastic condition and the inhomogeneity brings about various damages such as inhomogeneous plastic deformation, microcracking, necking, and so on. It is therefore important to investigate microscopic inhomogeneous deformation under elastic and plastic conditions. However only a few researches deal with the microscopic inhomogeneity because it is not easy to measure a small deformation of crystal grains under elastic condition or very small load. Recently, digital holographic microscope has been developed and a high-speed measurement of surface height of materials became possible with an accuracy of less than a micron meter in a relatively wide area. In this study, a tensile test of a plate specimen of commercial pure titanium was carried out on the stage of digital holographic microscope, and the microscopic deformation of grains was observed and measured under elastic and plastic conditions. During the test, the distribution of height of grains was measured in a fixed area on the specimen surface at each tensile loading step and the height distributions at different loads were correlated. It was found from the measurement results that each grain shows different deformation even under elastic condition with a small load, and the inhomogeneous deformation expanded with increasing the load to plastic condition. Also, a strong correlation was found in the height distributions under elastic and plastic conditions. This fact suggests that the microscopic deformation under plastic condition is predictable from that under elastic condition.


Author(s):  
Naoya Tada ◽  
Kentaro Kishimoto ◽  
Takeshi Uemori ◽  
Junji Sakamoto

Abstract Commercial pure titanium has been widely used in aerospace, chemical, and biomedical industries for its lightweight, high corrosion resistance, high strength, high heat resistance and good biocompatible properties. The market of pure titanium thin sheets is expected to increase in medical, dental, civil engineering, and acoustical engineering fields. On the other hand, pure titanium takes hexagonal closed-pack structure with anisotropic elasticity and plasticity. Inhomogeneous microscopic deformation always occurs by mechanical loading from the elastic condition. The inhomogeneity brings about various damages such as localized plastic deformation, microcracking, necking, and so on. Since the inhomogeneity is significant in thin sheets, it is important to investigate its deformation behavior. In this study, a tensile test was carried out using a thin sheet specimen of polycrystalline pure titanium, and the microscopic deformation of grains was measured by the digital holographic microscope. During the test, the height distribution of grains was measured in a fixed area on the front and back surfaces of the specimen at each tensile load step and the results at different load steps were compared. It was found from the measurement results that inhomogeneous deformation began at the small load due to anisotropic elasticity of crystal grains and expanded with the load by their anisotropic plasticity. Grain heights at grain center and those along grain boundaries were related with each other, and the grain heights on the front surface were inversely correlated with those on the back surface.


2018 ◽  
Vol 8 (10) ◽  
pp. 1907 ◽  
Author(s):  
Naoya Tada ◽  
Takeshi Uemori

A cyclic tensile test was carried out using a plate specimen of commercial pure titanium on a digital holographic microscope stage. Microscopic deformation of the grains was observed, and their height distribution was measured on the specimen surface. Each grain showed nanoscopic movement up and down, as well as reverse movement corresponding to specimen loading and unloading. We suggest that the different grain-specific changes in height were caused by microscopic inhomogeneities in the material, such as differences in the crystal orientation and geometries of both the surface and subsurface grains. Changes in grain height increased with tensile load, and a strong relationship was found between the height changes that occurred under elastic and plastic conditions. This suggests that microscopic plastic deformation is predictable from microscopic elastic deformation. In order to investigate the plastic deformation of grains in more detail, slip-line angles were measured after the tensile test. We found slip lines with similar angles in neighboring grains, suggesting that the plastic deformation of grains was not independent, but rather was related to that of surrounding grains and influenced by the deformation of subsurface grains.


Alloy Digest ◽  
1965 ◽  
Vol 14 (9) ◽  

Abstract MALLORY 53B is an economical copper alloy combining high strength with high heat and electrical conductivity and excellent corrosion resistance. It is heat treatable. This datasheet provides information on composition, physical properties, hardness, elasticity, tensile properties, and compressive strength. It also includes information on corrosion resistance as well as forming, heat treating, and machining. Filing Code: Cu-155. Producer or source: P. R. Mallory & Company Inc..


Alloy Digest ◽  
1955 ◽  
Vol 4 (7) ◽  

Abstract ARMCO 25-12 is an austenitic chromium-nickel stainless steel with high heat resisting qualities, high strength and creep values up to 2000 F. It is equivalent to AISI Type 309 stainless steel; and in the lower carbon grade is equivalent to AISI Type 309S. This datasheet provides information on composition, physical properties, hardness, elasticity, and tensile properties as well as fracture toughness, creep, and fatigue. It also includes information on high temperature performance and corrosion resistance as well as forming, heat treating, machining, and joining. Filing Code: SS-32. Producer or source: Armco Inc., Eastern Steel Division.


Alloy Digest ◽  
2003 ◽  
Vol 52 (4) ◽  

Abstract Hot-working die steel DH31-S has high strength, toughness, and high heat check resistance. This datasheet provides information on physical properties, elasticity, tensile properties, and shear strength. It also includes information on high temperature performance as well as heat treating. Filing Code: TS-600. Producer or source: International Mold Steel Inc., Daido Steel Company Ltd.


2018 ◽  
Vol 69 (6) ◽  
pp. 1416-1418
Author(s):  
Alexandru Szabo ◽  
Ilare Bordeasu ◽  
Ion Dragos Utu ◽  
Ion Mitelea

Hydroxyapatite (HA) is a very common material used for biomedical applications. Usually, in order to improve its poor mechanical properties is combined or coated with other high-strength materials.The present paper reports the manufacturing and the biocompatibility behaviour of two different biocomposite coatings consisting of alumina (Al2O3) and hydroxyapatite (HA) using the high velocity oxygen fuel (HVOF) spraying method which were deposited onto the surface of a commercially pure titanium substrate. The biological properties of the Al2O3-HA materials were evaluated by in vitro studies. The morphology of the coatings before and after their immersing in the simulated body fluid (SBF) solution was characterized by scanning electron microscopy (SEM). The results showed an important germination of the biologic hydroxyapatite crystallite on the surface of both coatings.


Author(s):  
Matthew James ◽  
Teresa Melfi ◽  
Rajeev Katiyar

Current requirements for high strength pipelines are placing extreme demands on welding consumables. These applications include strain based pipelines using X80 as well as traditionally designed pipelines using X100 and even X120 base materials. Traditional procedures used in the pipemills for both the seam weld and the jointer weld utilize a SAW process with very high dilution and high heat inputs. Existing consumables are not able to meet the minimum strength requirements under these conditions. A project was undertaken to develop an alloy system that could meet these requirements while still allowing the use of traditional welding processes. Testing results with this new consumable are presented and future work is described. This alloy system may also prove useful in other high dilution applications where high strength is required.


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