Assessment and Verification of a Novel Method for Near Surface Measurement of Mechanical Properties

2007 ◽  
Vol 129 (2) ◽  
pp. 314-320 ◽  
Author(s):  
S. Ozcan ◽  
K. Farhang ◽  
P. Filip
Keyword(s):  
Modulus Of Elasticity ◽  
Fused Silica ◽  
Surface Measurement ◽  
Radius Of Curvature ◽  
Near Surface ◽  
Area Function ◽  
Atomic Force ◽  
Scanning Electron Microscope Measurement ◽  
Nanoindentation Measurement ◽  
Two Parameter

A novel two-parameter area function for determination of near surface properties of Young’s modulus of elasticity and hardness has shown promise for compensating for the imperfection of the tip-end in an instrumented indentation measurement. This paper provides a comprehensive study involving a Berkovitch tip. The tip is utilized in an MTS nanoindentation measurement machine and is used to establish load indentation information for fused silica samples. The geometry of the tip is then characterized independently using a highly accurate atomic force microscope. Using the indentation data along with the two-parameter area function methodology, the tip-end radius of curvature is found to provide the most consistent value of modulus of elasticity. Independently, the data from the scanning electron microscope measurement of the same tip is used to obtain the least-squares estimation of the tip curvature. The two approaches yield favorable agreement in the estimation of tip-end radius of curvature. Therefore, the validity of the two-parameter area function method is proved. The method is shown to provide a robust, reliable, and accurate measurement of modulus of elasticity and hardness in the nanoscale proximity of a surface.

Nano-Scale Indentation Measurement of Material Properties Using an Area Function of the Tip Geometry

2008 ◽  
Author(s):  
S. Ozcan ◽  
K. Farhang ◽  
P. Filip
Keyword(s):  
Modulus Of Elasticity ◽  
Fused Silica ◽  
Radius Of Curvature ◽  
Near Surface ◽  
Area Function ◽  
Atomic Force ◽  
Nanoindentation Measurement ◽  
Two Parameter ◽  
Indentation Measurement

A novel two-parameter area function for determination of near surface properties of Young’s modulus of elasticity and hardness has shown promise for compensating for the imperfection of the tip-end in an instrumented indentation measurement. This paper provides a comprehensive study involving a Berkovitch tip. The tip is utilized in an MTS nanoindentation measurement machine and used to establish load indentation information for fused silica samples. The geometry of the tip is then characterized independently using a highly accurate Atomic Force Microscope. Using the indentation data along with the two-parameter area function methodology, the tip-end radius of curvature is found to provide the most consistent value of modulus of elasticity. Independently, the data from the SEM measurement of the same tip is used to obtain the least squares estimation of the tip curvature. The two approaches yield favorable agreement in the estimation of tip-end radius of curvature. Therefore, the validity of the two-parameter area function method is proved. The method is shown to provide a robust, reliable and accurate measurement of modulus of elasticity and hardness in the nanoscale proximity of a surface.

Near Surface Measurement of Mechanical Properties Using Instrumented Indentation Measurements

2005 ◽  
Author(s):  
K. Farhang ◽  
L. E. Seitzman ◽  
B. Feng
Keyword(s):  
Young’S Modulus ◽  
Young's Modulus ◽  
Surface Measurement ◽  
Accurate Estimation ◽  
Radius Of Curvature ◽  
Instrumented Indentation ◽  
Near Surface ◽  
Parameter Function ◽  
Two Parameter ◽  
Indentation Measurement

A two-parameter function for estimation of projected area in instrumented indentation measurement is obtained to account for indenter tip imperfection. Imperfection near indenter tip-end is modeled using a spherical function and combined with a linear function describing the edge boundary of the indenter. Through an analytical fusion technique the spherical and linear functions are combined into a single function with two unknown geometric parameters of tip radius of curvature and edge slope. Data from indentation measurement of force and displacement, using a Berkovich tip and single crystal alumina and silica samples, are implemented in the proposed area function yielding estimated values of Young’s modulus. Results were compared with that obtained from Oliver and Pharr technique for deep as well as shallow indentation regimes. The estimates for Young’s modulus were found to agree quite favorably. More importantly, in contrast to the Oliver-Pharr technique, the use of the two-parameter function resulted in a significantly more accurate estimation of Young’s modulus for shallow indentation depth of 0 to 100 nm. The error in estimation of Young’s modulus was found to be within 10 percent for indentation depths 25 nm to 50 nm and within 20 percent for indentation depths 0 to 25 nm.

A Two-Parameter Function for Nanoscale Indentation Measurement of Near Surface Properties

2007 ◽  
Vol 130 (1) ◽  
Author(s):  
K. Farhang ◽  
L. E. Seitzman ◽  
B. Feng
Keyword(s):  
Young’S Modulus ◽  
Young's Modulus ◽  
Linear Functions ◽  
Accurate Estimation ◽  
Radius Of Curvature ◽  
Near Surface ◽  
Tip Radius ◽  
Parameter Function ◽  
Two Parameter ◽  
Indentation Measurement

A two-parameter function for estimation of projected area in instrumented indentation measurement is obtained to account for indenter tip imperfection. Imperfection near indenter tip is modeled using a spherical function and combined with a linear function describing the edge boundary of the indenter. Through an analytical fusion technique, the spherical and linear functions are combined into a single function with two unknown geometric parameters of tip radius of curvature and edge slope. Data from indentation measurement of force and displacement, using a Berkovich tip and single crystal alumina and silica samples, are implemented in the proposed area function yielding estimated values of Young’s modulus. Results were compared with that obtained from Oliver and Pharr technique for deep as well as shallow indentation regimes. The estimates for Young’s modulus were found to agree quite favorably. More importantly, in contrast to the Oliver–Pharr technique, the use of the two-parameter function resulted in a significantly more accurate estimation of Young’s modulus for shallow indentation depth of 0–50nm. The error in estimation of Young’s modulus was found to be within 10% for indentation depths of 25–50nm and within 20% for indentation depths of 0–25nm.

Molecular Dynamics Simulation of AFM-Based Nanomachining Processes

2011 ◽  
Author(s):  
Rapeepan Promyoo ◽  
Hazim El-Mounayri ◽  
Kody Varahramyan ◽  
Ashlie Martini
Keyword(s):  
Molecular Dynamics ◽  
Friction Coefficient ◽  
Md Simulation ◽  
Computational Models ◽  
Dynamics Simulation ◽  
Radius Of Curvature ◽  
Force Microscopy ◽  
Indentation Force ◽  
Atomic Force ◽  
Development And Validation

Recently, atomic force microscopy (AFM) has been widely used for nanomachining and fabrication of micro/ nanodevices. This paper describes the development and validation of computational models for AFM-based nanomachining (nanoindentation and nanoscratching). The Molecular Dynamics (MD) technique is used to model and simulate mechanical indentation and scratching at the nanoscale in the case of gold and silicon. The simulation allows for the prediction of indentation forces and the friction force at the interface between an indenter and a substrate. The effects of tip curvature and speed on indentation force and friction coefficient are investigated. The material deformation and indentation geometry are extracted based on the final locations of atoms, which are displaced by the rigid tool. In addition to modeling, an AFM was used to conduct actual indentation at the nanoscale, and provide measurements to validate the predictions from the MD simulation. The AFM provides resolution on nanometer (lateral) and angstrom (vertical) scales. A three-sided pyramid indenter (with a radius of curvature ∼ 50 nm) is raster scanned on top of the surface and in contact with it. It can be observed from the MD simulation results that the indentation force increases as the depth of indentation increases, but decreases as the scratching speed increases. On the other hand, the friction coefficient is found to be independent of scratching speed.

Residual Stress in Bone: A Parametric Study

2008 ◽  
Author(s):  
A. Hizal ◽  
B. Sadasivam ◽  
D. Arola
Keyword(s):  
Residual Stress ◽  
Particle Size ◽  
Residual Stresses ◽  
Material Removal ◽  
Surface Deformation ◽  
Radius Of Curvature ◽  
Near Surface ◽  
Size And Shape ◽  
Air Jet ◽  
Particle Size And Shape

A preliminary study was conducted to evaluate the parametric dependence of the residual stress distributions in bone that result from an abrasive air-jet surface treatment. Specifically, the influence of particle size and shape used in the treatment on the residual stress, propensity of embedding particles and material removal were studied. Rectangular beams of cortical bone were prepared from bovine femurs and treated with aluminum oxide and glass particles with different treatment angles. Residual stresses within the bone were quantified in terms of the radius of curvature of the bone specimens measured before and after the treatments, as well as a function of time to quantify decay in the stress. The sub-surface distribution was also examined using the layer removal technique. Results showed that the particle size and shape could be used to control the amount of material removal and the magnitude of residual stress within the treated surfaces. An increase in size of the glass particles resulted in an increase in the residual stress and a decrease in material removed during the treatment. The magnitude of residual stress ranged from 22 MPa to nearly 44 MPa through modulation of the particle qualities (size and shape). A microscopic examination of the treated surfaces suggests that the residual stresses resulted primarily from near-surface deformation.

scholarly journals Sensitivity studies for a space-based methane lidar mission

2011 ◽  
Vol 4 (10) ◽  
pp. 2195-2211 ◽  
Author(s):  
C. Kiemle ◽  
M. Quatrevalet ◽  
G. Ehret ◽  
A. Amediek ◽  
A. Fix ◽  
...  
Keyword(s):  
Carbon Dioxide ◽  
Laser Power ◽  
European Space Agency ◽  
Surface Measurement ◽  
Performance Parameters ◽  
Measurement Sensitivity ◽  
Near Surface ◽  
Average Laser Power ◽  
Sensitivity Studies ◽  
Average Laser

Abstract. Methane is the third most important greenhouse gas in the atmosphere after water vapour and carbon dioxide. A major handicap to quantify the emissions at the Earth's surface in order to better understand biosphere-atmosphere exchange processes and potential climate feedbacks is the lack of accurate and global observations of methane. Space-based integrated path differential absorption (IPDA) lidar has potential to fill this gap, and a Methane Remote Lidar Mission (MERLIN) on a small satellite in polar orbit was proposed by DLR and CNES in the frame of a German-French climate monitoring initiative. System simulations are used to identify key performance parameters and to find an advantageous instrument configuration, given the environmental, technological, and budget constraints. The sensitivity studies use representative averages of the atmospheric and surface state to estimate the measurement precision, i.e. the random uncertainty due to instrument noise. Key performance parameters for MERLIN are average laser power, telescope size, orbit height, surface reflectance, and detector noise. A modest-size lidar instrument with 0.45 W average laser power and 0.55 m telescope diameter on a 506 km orbit could provide 50-km averaged methane column measurement along the sub-satellite track with a precision of about 1% over vegetation. The use of a methane absorption trough at 1.65 μm improves the near-surface measurement sensitivity and vastly relaxes the wavelength stability requirement that was identified as one of the major technological risks in the pre-phase A studies for A-SCOPE, a space-based IPDA lidar for carbon dioxide at the European Space Agency. Minimal humidity and temperature sensitivity at this wavelength position will enable accurate measurements in tropical wetlands, key regions with largely uncertain methane emissions. In contrast to actual passive remote sensors, measurements in Polar Regions will be possible and biases due to aerosol layers and thin ice clouds will be minimised.

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