EFFECT OF POST-CURING REGIME ON DENSITY, COMPRESSIVE STRENGTH AND CROSSLINKING OF POLYMER CONCRETE

2015 ◽  
Vol 77 (12) ◽  
Author(s):  
Nur Hafizah A. Khalid ◽  
Mohd Warid Hussin ◽  
Mohammad Ismail ◽  
Mohamed A. Ismail ◽  
Azman Mohamed ◽  
...  

Polymer concrete is produced from polymer binder, aggregates, and filler. Its curing follows the polymerization process once polymer additive is added, and can be accelerated through post-curing. In this study, the Orthophthalic- and Isophthalic-based polymer concrete (Ortho-PC and Iso-PC) were cured and investigated at different curing temperature (30oC, 50oC and 70oC) and period (1, 3, 6, 16, 24 hours) to complete the compressive strength development. Effect of curing temperature and period on apparent density, compressive strength, and morphology properties were investigated. The outcomes exhibited that all specimens had achieved full compressive strength within 6 hours of curing time at both 50oC and 70oC. When cured at 30oC, this went up to more than 16 hours of curing period to achieve the same compressive strength. The form of crosslinking at different curing conditions was captured in Scanning Electron Microscope, SEM images. Results also showed that curing temperature and period insignificant affected the apparent density. This study can be used as references to manufacturer, fabricator, and engineers when dealing with polymer concrete which goes for post-curing method as curing process.

2015 ◽  
Vol 2015 ◽  
pp. 1-12 ◽  
Author(s):  
Keun-Hyeok Yang ◽  
Jae-Sung Mun ◽  
Myung-Sug Cho

This study examined the relative strength-maturity relationship of high-strength concrete (HSC) specifically developed for nuclear facility structures while considering the economic efficiency and durability of the concrete. Two types of mixture proportions with water-to-binder ratios of 0.4 and 0.28 were tested under different temperature histories including (1) isothermal curing conditions of 5°C, 20°C, and 40°C and (2) terraced temperature histories of 20°C for an initial age of individual 1, 3, or 7 days and a constant temperature of 5°C for the subsequent ages. On the basis of the test results, the traditional maturity function of an equivalent age was modified to consider the offset maturity and the insignificance of subsequent curing temperature after an age of 3 days on later strength of concrete. To determine the key parameters in the maturity function, the setting behavior, apparent activation energy, and rate constant of the prepared mixtures were also measured. This study reveals that the compressive strength development of HSC cured at the reference temperature for an early age of 3 days is insignificantly affected by the subsequent curing temperature histories. The proposed maturity approach with the modified equivalent age accurately predicts the strength development of HSC.


2019 ◽  
Vol 31 ◽  
pp. 38-45
Author(s):  
Hiep Le Chi ◽  
Petr Louda ◽  
Totka Bakalova ◽  
Vladimír Kovačič

In this study, geopolymer samples were prepared by mixing metakaolin (MA) with activator solution made of potassium alkali silicate solution, potassium hydroxide flakes, and additional water. The aim of the experiment is to evaluate the mechanical strength of hardened samples based on four test variables including the SiO2/K2O molar ratios, K2O concentration, H2O/MA water coefficient, and curing temperature. The results reveal that K2O concentration and H2O/MA water coefficient impact strongly on the compressive strength, whereas varying of SiO2/K2O molar ratios in the range from 1.0 – 1.4 does not significantly change the compressive strength of geopolymer samples. On the other hand, high-temperature curing leads to higher mechanical strength of the samples in the early-age compared to curing at room temperature, due to the faster establishment of hard structure in the early-age of geo-polymerization process. However, curing at a temperature range of 80°C – 100°C contributes the non-linear strength development of the samples over the time.


2019 ◽  
Vol 11 (7) ◽  
pp. 2094 ◽  
Author(s):  
Osama Ahmed Mohamed

The production of cement requires significant energy and is responsible for more than 5% of global CO2 emissions; therefore it is imperative to reduce the production and use of ordinary portland cement (OPC). This paper examines the compressive strength development of low water-to-binder (w/b) ratio self-consolidating concrete (SCC) in which 90% of the cement is replaced with industrial by-products including ground granulated blast furnace slag (GGBS), fly ash, and silica fume. The emphasis in this paper is on replacing a large volume of cement with GGBS, which represented 10% to 77.5% of the cement replaced. Fresh properties at w/b ratio of 0.27 were examined by estimating the visual stability index (VSI) and t50 time. The compressive strength was determined after 3, 7, 28, and 56 days of curing. The control mix made with 100% OPC developed compressive strength ranging from 55 MPa after three days of curing to 76.75 MPa after 56 days of curing. On average, sustainable SCC containing 10% OPC developed strength ranging from 31 MPa after three days of curing to 56.4 MPa after 56 days of curing. However, the relative percentages of fly ash, silica fume, and GGBS in the 90% binder affect the strength developed as well. In addition, this paper reports the effect of the curing method on the 28 day compressive strength of environmentally friendly SCC in which 90% of the cement is replaced by GGBS, silica fume, and fly ash. The highest compressive strength was achieved in samples that were cured for three days under water, then left to air-dry for 25 days, compared to samples cured using chemical compounds or samples continuously cured under water for 28 days. The study confirms that SCC with 10% OPC and 90% supplementary cementitious composites (GGBS, silica fume, fly ash) can achieve compressive strength sufficient for many practical applications by incorporating high amounts of GGBS. In addition, air-curing of samples in a relatively high temperature (after three days of water curing) produce a higher 28 day compressive strength compared to water curing for 28 days, or membrane curing.


2020 ◽  
Vol 2020 ◽  
pp. 1-10
Author(s):  
Yongli Xu ◽  
Guang Yang ◽  
Hongyuan Zhao

For cement-based materials, the curing temperature determines the strength gain rate and the value of compressive strength. In this paper, the 5% cement-stabilized macadam mixture is used. Three indoor controlled temperature curing and one outdoor natural curing scenarios are designed and implemented to study the strength development scenario law of compressive strength, and they are standard temperature curing (20°C), constant low temperature curing (10°C), day interaction temperature curing (varying from 6°C to 16°C), and one outdoor natural temperature curing (in which the air temperature ranges from 4°C to 20°C). Finally, based on the maturity method, the maturity-strength estimation model is obtained by using and analyzing the data collected from the indoor tests. The model is proved with high accuracy based on the validated results obtained from the data of outdoor tests. This research provides technical support for the construction of cement-stabilized macadam in regions with low temperature, which is beneficial in the construction process and quality control.


2021 ◽  
Vol 11 (11) ◽  
pp. 4754
Author(s):  
Assia Aboubakar Mahamat ◽  
Moussa Mahamat Boukar ◽  
Nurudeen Mahmud Ibrahim ◽  
Tido Tiwa Stanislas ◽  
Numfor Linda Bih ◽  
...  

Earth-based materials have shown promise in the development of ecofriendly and sustainable construction materials. However, their unconventional usage in the construction field makes the estimation of their properties difficult and inaccurate. Often, the determination of their properties is conducted based on a conventional materials procedure. Hence, there is inaccuracy in understanding the properties of the unconventional materials. To obtain more accurate properties, a support vector machine (SVM), artificial neural network (ANN) and linear regression (LR) were used to predict the compressive strength of the alkali-activated termite soil. In this study, factors such as activator concentration, Si/Al, initial curing temperature, water absorption, weight and curing regime were used as input parameters due to their significant effect in the compressive strength. The experimental results depict that SVM outperforms ANN and LR in terms of R2 score and root mean square error (RMSE).


2019 ◽  
Vol 2019 ◽  
pp. 1-9
Author(s):  
Bin Han ◽  
Shengyou Zhang ◽  
Wei Sun

This study investigated the influencing rules of curing temperature (5, 10, 16, and 20°C), cement ratio (8%, 10%, 12%, and 14%), and mass concentration (70%, 73%, 74%, and 75%) on the strength of backfill. In addition, a scanning electron microscope (SEM) is employed to analyze the microtopography of the backfill. Experimental results indicate that the uniaxial compressive strength (UCS) of the backfill decreases as the curing temperature diminishes; temperature substantially influences the earlier strength of backfill (it is much significant below 10°C). In addition, as the cement ratio rises, the critical point for the impact of temperature on strength gradually moves toward a low-temperature zone; in pace with the slurry mass concentration increase, the compressive strength of the backfill also rises and its rate of increase enlarges after going beyond the critical concentration. In case the curing temperature is lower than 10°C, the extent of hydration is also low inside the backfill. Through experiments, the critical concentration of slurry in the Jinying gold mine is determined as 73%, and the critical interval of the cement ratio ranged between 10% and 12%. Corresponding measures can be taken to increase the strength of backfill in the Jinying Gold Mine by 129.9%. As a result, backfill collapse is effectively controlled.


Minerals ◽  
2019 ◽  
Vol 9 (3) ◽  
pp. 172
Author(s):  
Mamert Mbonimpa ◽  
Parrein Kwizera ◽  
Tikou Belem

When cemented paste backfill (CPB) is used to fill underground stopes opened in permafrost, depending on the distance from the permafrost wall, the curing temperature within the CPB matrix decreases progressively over time until equilibrium with the permafrost is reached (after several years). In this study, the influence of declining curing temperature (above freezing temperature) on the evolution of the unconfined compressive strength (UCS) of CPB over 28 days’ curing is investigated. CPB mixtures were prepared with a high early (HE) cement and a blend of 80% slag and 20% General Use cement (S-GU) at 5% and 3% contents and cured at room temperature in a humidity chamber and under decreasing temperatures in a temperature-controlled chamber. Results indicate that UCS is higher for CPB cured at room temperature than under declining temperatures. UCS increases progressively from the stope wall toward the inside of the CPB mass. Under declines in curing temperature, HE cement provides better short-term compressive strength than does S-GU binder. In addition, the gradual decline in temperature does not appear to affect the fact that the higher the binder proportion, the greater the strength development. Therefore, UCS is higher for samples prepared with 5% than 3% HE cement. Findings are discussed in terms of practical applications.


2012 ◽  
Vol 626 ◽  
pp. 931-936 ◽  
Author(s):  
Liew Yun Ming ◽  
Kamarudin Hussin ◽  
Mohd Mustafa Al Bakri Abdullah ◽  
Mohammed Binhussain ◽  
Luqman Musa ◽  
...  

The properties of metakaolin geopolymer paste are affected by the alkali concentration, the initial raw materials, solidification process, and amount of mixing water as well as the curing conditions. This study aimed to investigate the effect of curing temperature (room temperature, 40°C, 60°C, 80°C and 100°C) and curing time (6h, 12h, 24h, 48h and 72h) on the geopolymer pastes produced from geopolymer powder. The results showed that curing at room temperature was unfeasible. Heat was required for the geopolymerization process, where strength increased as the curing temperature was increased. Moderate elevated curing temperature favored the strength development of geopolymer pastes in comparison with those treated with extreme elevated curing temperature. When geopolymer paste was subjected to extreme elevated curing temperature, shorter curing time should be used to avoid deterioration in strength gain. Similarly, longer curing time was recommended for moderate elevated curing temperature. The microstructure of geopolymer paste cured at moderate curing temperature showed obvious densification of structure. In contrast, the structure formed was weak and less compact at very high elevated curing temperature.


2017 ◽  
Vol 744 ◽  
pp. 45-54
Author(s):  
Yong Min Yang ◽  
Zhao Heng Li ◽  
Tong Sheng Zhang ◽  
Qi Jun Yu

Previous studies showed that curing regime has a significant influence on mechanical properties of light-burned magnesium oxide (MgO) concrete. However, research has been limited mostly to constant-temperature studies, whereas dams manufactured from concrete exist in variable-temperature environments. In order to achieve material performance parameters that agree more closely with engineering practice, the development of mechanical properties of light-burned MgO concrete curing at constant temperature and simulated dam body temperature was studied. The compressive strength, elastic modulus and ultimate tensile strain of light-burned MgO concrete increased with the increase of curing temperature, MgO content and curing age. These constant-temperature properties were similar to those under simulated dam body temperature curing conditions. A comparison of experimental results of simulated dam body temperature curing and constant temperature curing showed that a thermostatic curing system was suitable for calculating the laws of mechanics development for dam concrete.


2017 ◽  
Vol 2017 ◽  
pp. 1-12
Author(s):  
Nan Ji Jin ◽  
Kyu-Seok Yeon ◽  
Seung-Ho Min ◽  
Jaeheum Yeon

The compressive strength of vinyl ester polymer concrete is predicted using the maturity method. The compressive strength rapidly increased until the curing age of 24 hrs and thereafter slowly increased until the curing age of 72 hrs. As the MMA content increased, the compressive strength decreased. Furthermore, as the curing temperature decreased, compressive strength decreased. For vinyl ester polymer concrete, datum temperature, ranging from −22.5 to −24.6°C, decreased as the MMA content increased. The maturity index equation for cement concrete cannot be applied to polymer concrete and the maturity of vinyl ester polymer concrete can only be estimated through control of the time interval Δt. Thus, this study introduced a suitable scaled-down factor (n) for the determination of polymer concrete’s maturity, and a factor of 0.3 was the most suitable. Also, the DR-HILL compressive strength prediction model was determined as applicable to vinyl ester polymer concrete among the dose-response models. For the parameters of the prediction model, applying the parameters by combining all data obtained from the three different amounts of MMA content was deemed acceptable. The study results could be useful for the quality control of vinyl ester polymer concrete and nondestructive prediction of early age strength.


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