Low-Temperature Rapid Synthesis of Rod-Like ZrB2 Powders by Molten-Salt and Microwave Co-Assisted Carbothermal Reduction

2016 ◽  
Vol 99 (9) ◽  
pp. 2895-2898 ◽  
Author(s):  
Jianghao Liu ◽  
Zhong Huang ◽  
Chaoge Huo ◽  
Faliang Li ◽  
Haijun Zhang ◽  
...  
Materials ◽  
2019 ◽  
Vol 12 (16) ◽  
pp. 2555 ◽  
Author(s):  
Jie Liu ◽  
Jianghao Liu ◽  
Yuan Zeng ◽  
Haijun Zhang ◽  
Zhi Li

A molten-salt and microwave co-facilitated boro/carbothermal reduction methodology was developed for low temperature high-efficiency synthesis of TiB2 powders. By using relatively inexpensive titanium oxide (TiO2), boron carbide (B4C) and amorphous carbon (C) as raw materials, single-phase TiB2 powders were prepared after 60 min at as low as 1150 °C or after only 20 min at 1200 °C. Such synthesis conditions were remarkably milder than those required by the conventional reduction routes using the identical reducing agent. As-synthesized TiB2 powders exhibited single-crystalline nature and well-grown hexagonal-platelet-like morphology. The achievement of low temperature high-efficiency preparation of high-quality TiB2 microplatelets in the present work was mainly attributable to the synergistic effects of molten-salt medium and microwave heating.


2021 ◽  
Vol 129 (8) ◽  
pp. 528-534
Author(s):  
Jiangfeng HE ◽  
Yuan ZENG ◽  
Zhong HUANG ◽  
Jianghao LIU ◽  
Yunbo CAO ◽  
...  

2008 ◽  
Vol 23 (8) ◽  
pp. 791-795 ◽  
Author(s):  
Ying Lin ◽  
Haibo Yang ◽  
Jianfeng Zhu ◽  
Fen Wang ◽  
Hongjie Luo

Author(s):  
Bishnu Prasad Prasad Thapaliya ◽  
Huimin Luo ◽  
Mengya Li ◽  
Wan-Yu Tsai ◽  
Harry M Meyer Iii ◽  
...  

2019 ◽  
Vol 275 ◽  
pp. 290-296 ◽  
Author(s):  
Radha G. Bhuin ◽  
Patrick Schreiber ◽  
Bettina S.J. Heller ◽  
Marlene Scheuermeyer ◽  
Peter Wasserscheid ◽  
...  

2020 ◽  
Vol 61 (8) ◽  
pp. 1651-1656
Author(s):  
Kazuhiro Kumamoto ◽  
Akihiro Kishimoto ◽  
Tetsuya Uda
Keyword(s):  

2015 ◽  
Vol 162 (14) ◽  
pp. A2729-A2736 ◽  
Author(s):  
Brian L. Spatocco ◽  
Takanari Ouchi ◽  
Guillaume Lambotte ◽  
Paul J. Burke ◽  
Donald R. Sadoway

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