Anode-Supported IT-SOFC anode Prepared by Tape Casting Technique

Author(s):  
Jiangrong Kong ◽  
Kening Sun ◽  
Derui Zhou ◽  
Jinshuo Qiao ◽  
Jigang Li
Author(s):  
Haoran Wang ◽  
Ze Lei ◽  
Han Zhang ◽  
Yongkang Li ◽  
Junmeng Jing ◽  
...  

Abstract A water-based tape casting slurry is reported to prepare the ceria and scandia co-doped zirconia (ScSZ) electrolyte films. The slurry is characterized and optimized through Zeta potential and rheological property measurements. Smooth and flat ScSZ electrolyte films are obtained by improving the sintering process. The microstructure, electrical performance, and mechanical property of ScSZ with adding different contents of Al2O3 are also investigated. The results show that a proper amount of Al2O3 has a beneficial effect on the densification of ScSZ. Significant decrease at the grain boundary resistance of ScSZ is observed by Al2O3 addition. The bending strength of the sample with 0.5 wt.% Al2O3 (ScSZ-0.5A) is about 400 MPa, which is 20% higher than pure ScSZ. The ScSZ-0.5A electrolyte film fabricated by water-based tape casting method shows appropriate electrical conductivity and high mechanical strength, which is promising for the practical application in solid oxide fuel cells (SOFCs).


2006 ◽  
Vol 175 (1-3) ◽  
pp. 358-363 ◽  
Author(s):  
Zbigniew S. Rak ◽  
Janusz Walter

MRS Bulletin ◽  
1989 ◽  
Vol 14 (1) ◽  
pp. 63-66 ◽  
Author(s):  
W.J. Nellis ◽  
L.D. Woolf

High Tc oxide superconductors can be prepared by a variety of novel metallurgical or ceramic processing techniques. For example, forming metallic precursors of YBa2Cu3 or REBa2Cu3, where RE is a rare earth element, followed by oxidation has yielded the corresponding ceramic oxide in pellet, wire, and thin film forms. Ceramic fabrication techniques (which often involve incorporating fine particles of the ceramic in a suitable vehicle) such as doctor-blade tape casting and screen printing have been utilized to synthesize both tapes and thin films. Due to intense worldwide effort to develop these ceramics into useable forms, many unique fabrication techniques have been employed, such as the melt-textured growth method of Jin et al. and dynamic compaction. In addition, it is likely that numerous laboratories, particularly industrial, are developing proprietary methods to fabricate wire and other forms but have not published these results due to the intensely competitive nature of this area. In this article, we review some of the methods reported so far for preparing high Tc ceramic superconductors, and we discuss one example of a proprietary method being developed at one of the author's (LDW) laboratories.Tapes of YBa2cu3O7-x fabricated using the doctor-blade tape casting technique were first displayed by AT&T Bell Laboratories scientists at the 1987 March meeting of the American Physical Society. This method involves mixing ceramic powder, a binder to provide green (unfired ceramic) strength, a plasticizer to provide flexibility, a dispersant to prevent particle agglomeration and a solvent. After mixing all these components together, the solution is poured into a “doctor blade” device which allows a controlled thickness of material to be deposited on a plastic film carrier that passes underneath the doctor blade.


2007 ◽  
Vol 23 (5) ◽  
pp. 549-555 ◽  
Author(s):  
Yasuhiro Tanimoto ◽  
Tohru Hayakawa ◽  
Kimiya Nemoto

2012 ◽  
Vol 2012 ◽  
pp. 1-4 ◽  
Author(s):  
B. Sahoo ◽  
P. K. Panda

A piezo multilayered stack of height 10 mm is fabricated using 80 μm thick PZT tapes prepared by tape-casting technique. About 120 layers of thin tapes are dried, screen-printed with Pt-electrode paste, stacked, laminated, and then isopressed to obtain a green multilayered stack. Cofiring of the stack is carried out at C for 1 h with very slow heating rate ( per 1 h). The sintered stack is poled at 2 kV per mm in hot (C) silicone oil bath for 45 minutes, and free displacement and block force were characterized. The actuator generates free displacement of 10 μm (0.1% strain) and block force of 1427 N at 175 V. In a similar way, a ring-shaped multilayered PZT stack was fabricated; the displacement was measured to be 8 μm. The ring-type actuator is mainly used for fluid flow control in space vehicles.


2007 ◽  
Vol 336-338 ◽  
pp. 109-110
Author(s):  
Chen Ai ◽  
Hao Xue ◽  
He Ping Zhou

In this work, tape-casting technique was employed to prepare Ba0.7Sr0.3TiO3 films for lens antenna system. Effects of slurry properties on the tape casting procedure were investigated and the thickness, tensile strength and the surface roughness of the tapes were studied. The structure, morphology and the dielectric properties of the films were analyzed.


2009 ◽  
Vol 3 (1-2) ◽  
pp. 65-71 ◽  
Author(s):  
Adelina Ianculescu ◽  
Sophie Guillemet-Fritsch ◽  
Bernard Durand

BaTiO3 powders were prepared by co-precipitation via oxalate route. The size, morphology and particle size distribution of the oxalate powders have been optimized by the control of different synthesis parameters during the precipitation reaction (nature of salts, concentration of different solutions, aging time). The single phase BaTiO3 oxide particles were obtained after a thermal decomposition of the as-synthesized powders at 850?C for 4 hours under air atmosphere. Oxide powders with a suitable specific surface area were selected in order to obtain thick films by the tape casting technique. The microstructure and dielectric properties of the thick films varied obviously depending on the deposition-calcination-sintering cycle used. A double deposition-calcination cycle followed by sintering, as well as a two step deposition-calcination-sintering procedure was used in order to improve the compactness and therefore, the dielectric behaviour. A higher dielectric constant value (~ 750) and lower dielectric losses (~ 2 %) were achieved at room temperature and at 1 kHz frequency for the dense, double-deposited film obtained after two deposition-calcination-sintering cycles. For this film, a superior value of the dielectric constant (~ 1100), almost frequency independent in the frequency range of 100 Hz - 10 kHz was gained also at the ferroelectric-paraelectric phase transition temperature of 130?C. .


2019 ◽  
Vol 34 (5) ◽  
pp. 509 ◽  
Author(s):  
Wei WANG ◽  
Li-Li YUAN ◽  
Qian-Yuan QIU ◽  
Ming-Yang ZHOU ◽  
Mei-Lin LIU ◽  
...  

2012 ◽  
Vol 37 (9) ◽  
pp. 8056-8061 ◽  
Author(s):  
Manuel Weirich ◽  
Jonas Gurauskis ◽  
Vanesa Gil ◽  
Kjell Wiik ◽  
Mari-Ann Einarsrud

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