Development of electroless nickel-iron plating process for microelectronic applications

Author(s):  
Yu Luo ◽  
Sung K. Kang ◽  
Oblesh Jinka ◽  
Maurice Mason ◽  
Steven A. Cordes ◽  
...  
2015 ◽  
Vol 1113 ◽  
pp. 545-549
Author(s):  
Athirah Ahmad ◽  
Koay Mei Hyie ◽  
N.R. Nik Roselina ◽  
Firdaus Munir ◽  
Choong Soo Li ◽  
...  

Electrodeposition is a method to electrochemically deposit alloy on various types of metal. This method has ability to produce protective coating and thin films on the metal. In this research, one of the electrodeposition methods, Cyclic Voltammetry (CV) with 10 and 20 cycles was applied to deposit Cobalt-Nickel-Iron (Co-Ni-Fe) on Electroless Nickel Immersion Gold (ENIG) Flexible Printed Circuits (FPCs). The main purpose of this paper is to investigate the electrical properties, morphology and crystallographic structure of the electrodeposited coating. Curve Trace test was conducted to identify the contact resistance of the coating. In this case, the allowable contact resistance should be less or the same as ENIG FPCs which is 1.6 Ω. Morphology of the coated circuit was observed by using FESEM while crystallographic phase of the coating was identified by XRD. Morphology study on Co-Ni-Fe coated FPCs exhibited Cauliflower like shape with average grain size of 1.49 μm and 1.88 μm for 10 and 20 cycles, respectively. CoFe, FeNi and CoO.NiO phases was noticed in the electrodeposited coating. The obtained result showed that the electrodeposited Co-Ni-Fe produced with 10 cycles has the same contact resistance as ENIG which is 1.6 Ω. 20 cycles of CV produced 1.4 Ω of contact resistance, slightly smaller than the other FPCs. This research revealed that electrodeposited Co-Ni-Fe is suitable to be applied as a protective coating while still maintaining the electrical properties of FPCs.


Author(s):  
C. W. Price ◽  
E. F. Lindsey

Thickness measurements of thin films are performed by both energy-dispersive x-ray spectroscopy (EDS) and x-ray fluorescence (XRF). XRF can measure thicker films than EDS, and XRF measurements also have somewhat greater precision than EDS measurements. However, small components with curved or irregular shapes that are used for various applications in the the Inertial Confinement Fusion program at LLNL present geometrical problems that are not conducive to XRF analyses but may have only a minimal effect on EDS analyses. This work describes the development of an EDS technique to measure the thickness of electroless nickel deposits on gold substrates. Although elaborate correction techniques have been developed for thin-film measurements by x-ray analysis, the thickness of electroless nickel films can be dependent on the plating bath used. Therefore, standard calibration curves were established by correlating EDS data with thickness measurements that were obtained by contact profilometry.


Author(s):  
O. Yu. Kichigina

At production of stainless steel expensive alloying elements, containing nickel, are used. To decrease the steel cost, substitution of nickel during steel alloying process by its oxides is an actual task. Results of analysis of thermodynamic and experimental studies of nickel reducing from its oxide presented, as well as methods of nickel oxide obtaining at manganese bearing complex raw materials enrichment and practice of its application during steel alloying. Technology of comprehensive processing of complex manganese-containing raw materials considered, including leaching and selective extraction out of the solution valuable components: manganese, nickel, iron, cobalt and copper. Based on theoretical and experiment studies, a possibility of substitution of metal nickel by concentrates, obtained as a result of hydrometallurgical enrichment, was confirmed. Optimal technological parameters, ensuring high degree of nickel recovery out of the initial raw materials were determined. It was established, that for direct steel alloying it is reasonable to add into the charge pellets, consisting of nickel concentrate and coke fines, that enables to reach the through nickel recovery at a level of 90%. The proposed method of alloying steel by nickel gives a possibility to decrease considerably steel cost at the expense of application of nickel concentrate, obtained out of tails of hydrometallurgical enrichment of manganese-bearing raw materials, which is much cheaper comparing with the metal nickel.


Alloy Digest ◽  
1975 ◽  
Vol 24 (6) ◽  

Abstract ALLOY 48 is a vacuum-melted, 48% nickel-iron alloy designed for high permeability, and low core losses. It is ideal in applications requiring efficient magnetic core materials, such as audio and instrument transformers, instrument relays, and many other communication equipment devices. It is excellent for rotor and stator laminations, and is also a very effective magnetic shielding material. This datasheet provides information on composition, physical properties, hardness, elasticity, and tensile properties. It also includes information on corrosion resistance as well as forming, heat treating, machining, and joining. Filing Code: Fe-52. Producer or source: Magnetics Specialty Metals Division. See also Alloy Digest Fe-96, April 1992.


Alloy Digest ◽  
1969 ◽  
Vol 18 (10) ◽  

Abstract Niromet 46 is a 46% nickel-iron alloy having low and controlled coefficient of expansion. It is recommended for metal-to-glass seals and terminal bands in vitreous enameled resistors. This datasheet provides information on composition, physical properties, hardness, and tensile properties. It also includes information on corrosion resistance as well as forming, heat treating, machining, and joining. Filing Code: Fe-39. Producer or source: Wilbur B. Driver Company.


Alloy Digest ◽  
1968 ◽  
Vol 17 (1) ◽  

Abstract N1-SPAN-C alloy 902 is an age-hardenable, nickel-iron-chromium alloy. Its outstanding characteristic is a controllable thermoelastic coefficient. Proper combination of cold work and thermal treatment can produce an essentially constant modulus of elasticity from -50 F to +150 F. The alloy is especially suitable for many types of precision equipment where elastic members are subject to temperature fluctuations. This datasheet provides information on composition, physical properties, hardness, elasticity, and tensile properties as well as fracture toughness and fatigue. It also includes information on corrosion resistance as well as forming, heat treating, machining, joining, and surface treatment. Filing Code: Fe-32. Producer or source: Huntington Alloy Products Division, An INCO Company.


Alloy Digest ◽  
1964 ◽  
Vol 13 (3) ◽  

Abstract INVAR is a 36% nickel-iron alloy having the lowest coefficient of expansion, recommended for applications requiring no dimensional changes with temperature variations. This datasheet provides information on composition, physical properties, hardness, elasticity, and tensile properties. It also includes information on low and high temperature performance, and corrosion resistance as well as forming, heat treating, machining, joining, and surface treatment. Filing Code: Fe-24. Producer or source: Carpenter.


Alloy Digest ◽  
1992 ◽  
Vol 41 (5) ◽  

Abstract INCO ALLOY 330 is a nickel/iron/chromium austenitic alloy, not hardenable by heat treatment. It is a solid solution strengthened high-temperature alloy. This datasheet provides information on composition, physical properties, elasticity, and tensile properties as well as creep. It also includes information on high temperature performance and corrosion resistance as well as forming, heat treating, machining, and joining. Filing Code: Ni-403. Producer or source: Inco Alloys International Inc..


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