Gold-induced faceting on a Si(001) vicinal surface: Spot-profile-analyzing LEED and reflection-electron-microscopy study

1999 ◽  
Vol 59 (3) ◽  
pp. 2363-2375 ◽  
Author(s):  
H. Minoda ◽  
K. Yagi ◽  
F.-J. Meyer zu Heringdorf ◽  
A. Meier ◽  
D. Kähler ◽  
...  
Author(s):  
M. Gajdardziska-Josifovska ◽  
M. R. McCartney ◽  
J. M. Cowley

The (100) surface of magnesium oxide is of considerable interest because of its frequent use as substrate for epitaxial growth of metal films, high Tc superconductors and model catalyst systems. A large number of surface characterization techniques have been used to determine the atomic structure of the cleaved (100) surface. Clean surfaces have been produced either by cleaving MgO crystals in-situ under ultra-high vacuum (UHV) conditions, or more frequently, by cleaving in air and subsequent annealing in UHV. A wide variety of annealing temperatures and times have been used by different researchers, the upper limit on the temperature being set at ≈900°C to avoid segregation of Ca to the surface. Calcium is the main impurity in even the purest MgO crystals and a few studies have dealt with the structure of the Ca-rich (100) surface of MgO. All of the existing studies have used diffraction and spectroscopy techniques without imaging of the surface. It is the purpose of this work to study the topography of the UHV-annealed (100) surface by reflection electron microscopy (REM).


1993 ◽  
Vol 228 (1-2) ◽  
pp. 12-17 ◽  
Author(s):  
Katsumichi Yagi ◽  
Hiroki Minoda ◽  
Masashi Shima

Author(s):  
Julie A. Martini ◽  
Robert H. Doremus

Tracy and Doremus have demonstrated chemical bonding between bone and hydroxylapatite with transmission electron microscopy. Now researchers ponder how to improve upon this bond in turn improving the life expectancy and biocompatibility of implantable orthopedic devices.This report focuses on a study of the- chemical influences on the interfacial integrity and strength. Pure hydroxylapatite (HAP), magnesium doped HAP, strontium doped HAP, bioglass and medical grade titanium cylinders were implanted into the tibial cortices of New Zealand white rabbits. After 12 weeks, the implants were retrieved for a scanning electron microscopy study coupled with energy dispersive spectroscopy.Following sacrifice and careful retrieval, the samples were dehydrated through a graduated series starting with 50% ethanol and continuing through 60, 70, 80, 90, 95, and 100% ethanol over a period of two days. The samples were embedded in LR White. Again a graduated series was used with solutions of 50, 75 and 100% LR White diluted in ethanol.


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