Quantitative measurement of residual biaxial stress by Raman spectroscopy in diamond grown on a Ti alloy by chemical vapor deposition

1993 ◽  
Vol 48 (4) ◽  
pp. 2601-2607 ◽  
Author(s):  
Joel W. Ager ◽  
Michael D. Drory
1992 ◽  
Vol 271 ◽  
Author(s):  
R. Morancho ◽  
A. Reynes ◽  
M'b. Amjoud ◽  
R. Carles

ABSTRACTTwo organosilicon molecules tetraethysilane (TESi) and tetravinylsilane (TVSi) were used to prepare thin films of silicon carbide by chemical vapor deposition (C. V. D.). In each of the molecule, the ratio C/Si = 8, the only difference between TESi and TVSi is the structure of the radicals ethyl (.CH2-CH3) and vinyl (.CH=CH2). This feature induces different thermal behavior and leads to the formation of different materials depending on the nature of the carrier gas He or H2· The decomposition gases are correlated with the material deposited which is investigated by I.R. and Raman spectroscopy. The structure of the starting molecule influences the mechanisms of decomposition and consequently the structure of the material obtained.


2020 ◽  
Vol 71 (5) ◽  
pp. 24-29
Author(s):  
Bianca Tincu ◽  
Mariaora Avram ◽  
Vasilica Tucureanu ◽  
Carmen Mihailaescu ◽  
Oana Tutunaru ◽  
...  

Recently, graphene as a material for sensors has attracted attention due to unique properties, such as: excellent electrical and thermal conductivity, chemical stability, high surface area and Young�s modulus ̴ 1GPa, very promising for electrochemical applications. Electrochemical sensors based on graphene have been used in many applications, such as: biomolecules, gases or metal ions detection. Here, we report the effect of morphology and orientation of graphene as electrode material with electrochemical method. We investigated the capacitive performance in the case of horizontal and vertical graphene sheets, synthetized by thermal chemical vapor deposition (CVD), respectively plasma enhanced chemical vapor deposition (PECVD). Graphene electrode is used in electrochemical cells with three electrodes as a working electrode. Raman spectroscopy was carried on the graphene films for quality and structure characterization. The working electrode was characterized by scanning electron microscopy (SEM), Raman spectroscopy and electrochemical method.


2013 ◽  
Vol 40 (7) ◽  
pp. 0707002
Author(s):  
薛海鹏 Xue Haipeng ◽  
卢文壮 Lu Wenzhuang ◽  
孙达飞 Sun Dafei ◽  
王浩 Wang Hao ◽  
王正鑫 Wang Zhengxin ◽  
...  

2016 ◽  
Vol 852 ◽  
pp. 1029-1033 ◽  
Author(s):  
Ning Wang ◽  
Jing Wang ◽  
Fu Wei Zheng ◽  
Yu Min Wu ◽  
Bao Rong Hou

This paper compares the microstructure and electrochemical properties of the diamond-like carbon films obtained by two different deposition methods - microwave electron cyclotron resonance plasma enhanced chemical vapor deposition (MWECR-PECVD) techniques and electro-deposition – chosen for their low cost and capacity to produce films. The microstructure of the DLC films are investigated by Raman spectroscopy, FTIR spectroscopy, and electrochemical behavior is investigated by potentiodynamic and electrochemical impedance spectroscopy (EIS). Raman spectroscopy indicates that all the films deposited by different techniques show amorphous structure and typical characteristic of DLC film. FTIR spectrum results indicate that these DLC films are a-C:H films. As a result of EIS, the DLC films made by different methods showed obviously different electrochemical characters. The obtained results show that the DLC films deposited using the PECVD methods provided the better results, presenting a high corrosion resistance , high adherence to substrate, and a denser and more uniform surface.


2015 ◽  
Vol 252 (11) ◽  
pp. 2385-2389 ◽  
Author(s):  
Maria O'Brien ◽  
Niall McEvoy ◽  
Damien Hanlon ◽  
Kangho Lee ◽  
Riley Gatensby ◽  
...  

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