Transmission electron diffraction study of a uniaxially-ordered high-mobility polymeric semiconductor

Microscopy ◽  
2019 ◽  
Vol 68 (2) ◽  
pp. 167-173 ◽  
Author(s):  
Masayuki Sasaki ◽  
Yu Yamashita ◽  
Hiroyuki Matsui ◽  
Yoshifumi Oshima ◽  
Jun Takeya
Author(s):  
H. Rager ◽  
M. Schosnig ◽  
A.K. Schaper ◽  
A. Kutoglu ◽  
W. Treutmann

This paper deals with transmission electron microscope experiments of Ca,Sr-åkermanite solid solutions at temperatures between 100 K and 375 K. The aim of the investigations was to study the compositional and temperature dependence of phase transitions from the normal to the incommensurately modulated structure of(Ca


Carbon ◽  
2008 ◽  
Vol 46 (12) ◽  
pp. 1535-1543 ◽  
Author(s):  
Torgunn Garberg ◽  
Stine Nalum Naess ◽  
Geir Helgesen ◽  
Kenneth D. Knudsen ◽  
Gunnar Kopstad ◽  
...  

Author(s):  
R.A. Ploc ◽  
G.H. Keech

An unambiguous analysis of transmission electron diffraction effects requires two samplings of the reciprocal lattice (RL). However, extracting definitive information from the patterns is difficult even for a general orthorhombic case. The usual procedure has been to deduce the approximate variables controlling the formation of the patterns from qualitative observations. Our present purpose is to illustrate two applications of a computer programme written for the analysis of transmission, selected area diffraction (SAD) patterns; the studies of RL spot shapes and epitaxy.When a specimen contains fine structure the RL spots become complex shapes with extensions in one or more directions. If the number and directions of these extensions can be estimated from an SAD pattern the exact spot shape can be determined by a series of refinements of the computer input data.


Author(s):  
R. H. Geiss

The theory and practical limitations of micro area scanning transmission electron diffraction (MASTED) will be presented. It has been demonstrated that MASTED patterns of metallic thin films from areas as small as 30 Åin diameter may be obtained with the standard STEM unit available for the Philips 301 TEM. The key to the successful application of MASTED to very small area diffraction is the proper use of the electron optics of the STEM unit. First the objective lens current must be adjusted such that the image of the C2 aperture is quasi-stationary under the action of the rocking beam (obtained with 40-80-160 SEM settings of the P301). Second, the sample must be elevated to coincide with the C2 aperture image and its image also be quasi-stationary. This sample height adjustment must be entirely mechanical after the objective lens current has been fixed in the first step.


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