High Resolution Chromatographic Separation of Steroids With Open Tubular Glass Columns

1970 ◽  
Vol 8 (6) ◽  
pp. 346-350 ◽  
Author(s):  
M. Novotny ◽  
A. Zlatkis
2015 ◽  
Vol 51 (61) ◽  
pp. 12254-12257 ◽  
Author(s):  
Cheng-Xiong Yang ◽  
Chang Liu ◽  
Yi-Meng Cao ◽  
Xiu-Ping Yan

Facile room-temperature solution-phase synthesis of a spherical covalent organic framework with large surface area and good stability for high-resolution chromatographic separation.


Talanta ◽  
2018 ◽  
Vol 186 ◽  
pp. 445-451 ◽  
Author(s):  
Juan Zheng ◽  
Cuiming Lu ◽  
Junlong Huang ◽  
Luyi Chen ◽  
Chuyi Ni ◽  
...  

1980 ◽  
Vol 63 (4) ◽  
pp. 750-755
Author(s):  
James N Huckins ◽  
David L Stalling ◽  
Jimmie D Petty

Abstract Columns of activated carbon dispersed on shredded polyurethane foam were used to separate non-o,o´-chlorine (Cl) substituted polychlorinated biphenyls (PCBs) from mg quantities of Aroclors 1016, 1242, 1248, 1254, and 1260. Aroclor 1248 contained the highest concentration (3400 μg/g) of highly toxic 3,4,3´,4´tetrachlorobiphenyl (TCB). Lesser amounts of 3,4,3’,4’-TCB were also found in Aroclors 1242 and 1254. However, we were unable to detect 3,4,3’,4’-TCB in Aroclors 1016 and 1260. Varying amounts of the non-o,o´-Cl substituted 3,4,4´-trichlorobiphenyl and 3,4,3´,4´,5´-pentachlorobiphenyl were found in most of the Aroclor mixtures. No residues of 3,4,5,3´,4´,5´-hexachlorobiphenyl were detected in the Aroclor mixtures examined. Using carbon-foam chromatography and high resolution capillary gas chromatography, 0.11 μg 3,4,3´,4´-TCB/g was detected in 3 subsamples of a composite of 5 carp from the Ohio River.


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