Multifunctional weak measurement system that can measure the refractive index and optical rotation of a solution

2019 ◽  
Vol 114 (18) ◽  
pp. 181901 ◽  
Author(s):  
Yang Xu ◽  
Lixuan Shi ◽  
Tian Guan ◽  
Suyi Zhong ◽  
Xuesi Zhou ◽  
...  
Keyword(s):  
Refractive Index ◽  
Measurement System ◽  
Optical Rotation ◽  
Weak Measurement

scholarly journals Rapid Separation of Enantiomeric Impurities in Chiral Molecules by a Self-Referential Weak Measurement System

Sensors ◽  
2018 ◽  
Vol 18 (11) ◽  
pp. 3788 ◽  
Author(s):  
Yang Xu ◽  
Lixuan Shi ◽  
Tian Guan ◽  
Suyi Zhong ◽  
Xuesi Zhou ◽  
...  
Keyword(s):  
Measurement System ◽  
Optical Rotation ◽  
Polarization State ◽  
Optical Resolution ◽  
Weak Measurement ◽  
Quarter Wave Plate ◽  
Chiral Molecules ◽  
Rapid Separation ◽  
Detection Scheme ◽  
Central Wavelength

We propose a self-referential fast detection scheme for a frequency domain weak measurement system for the detection of enantiomeric impurities in chiral molecules. In a transmissive weak measurement system, the optical rotation (OR) is used to modify the pre-selected polarization state and the post-selection polarization state. We obtained the sum and difference of the optical rotations produced by the sample and the standard by rotating the quarter wave plate in the system. Then, we estimate the ratio of chiral molecules to enantiomeric impurities using the ratio of the central wavelength shifts caused by the addition and subtraction states described above. In this paper, our system has an optical resolution of 1.88 × 10−5°. At the same time, we completed the detection of the ratio of the two substances in the mixture of L-proline and D-proline in different proportions, which proved that our system can quickly detect the content of enantiomeric impurities in chiral molecules.

scholarly journals NILAI TAMBAH MINYAK AKAR WANGI DENGAN PEMEKATAN KADAR VETIVEROL MENGGUNAKAN EKSTRAKSI CO2 FLUIDA SUPERKRITIK

2014 ◽  
Vol 16 (2) ◽  
pp. 76-81 ◽  
Author(s):  
Anny Sulaswatty ◽  
Egi Agustian
Keyword(s):  
Carbon Dioxide ◽  
Refractive Index ◽  
Specific Gravity ◽  
Supercritical Fluid Extraction ◽  
Supercritical Fluid ◽  
Flow Rate ◽  
Optical Rotation ◽  
Process Conditions ◽  
Fluid Extraction ◽  
Great Opportunity

Potensi Indonesia akan minyak akar wangi yang berorientasi ekspor dalam industri kosmetik, parfum, sabun, keperluan terapi, antiseptik, massage oil, farmasi dan pestisida memberikan peluang yang besar untuk memenuhi kebutuhan dunia. Guna nilai tambah minyak akar wangi dengan meningkatkan kadar vetiverol sebagai komponen utama, diaplikasikan teknologi ekstraksi fluida karbondioksida superkritik yang merupakan perpaduan ekstraksi, fraksinasi dan deodorisasi dengan didukung keunggulan karbondioksida sebagai pelarut yang inert, ramah lingkungan, mudah dipisahkan, dan berdaya larut tinggi.  Minyak akar wangi Garut (Java vetiver oil) sebagai bahan baku, mempunyai karakteristik  kadar vetiverol  39.03 %; Bobot jenis 0.9977; indeks bias 1.5247;  putaran optik +38.1; kelarutan dalam alkohol 95%  yaitu 1:1 jernih; bilangan asam 28.1; bilangan ester 24.6; bilangan ester setelah asetilasi 115.5; serta tidak mengandung minyak lemak dan  minyak keruing. Pemilihan kondisi proses guna menghasilkan kandungan vetiverol optimal dilakukan dengan memvariasikan laju alir gas CO2, tekanan dan suhu sebagai parameter penting dalam keberhasilan proses ekstraksi minyak akar wangi dengan fluida CO2 superkritik. Pemilihan laju alir konstan dan lebih stabil  diperoleh pada 5.5 liter/menit, sedangkan untuk variasi tekanan ekstraktor (1500, 1750, 2000 psi) dan suhu ekstraktor (40-50oC);  tekanan dan suhu separator  500 psi dan 25oC serta waktu proses selama lima jam dengan pengambilan ekstrak setiap jam. Tekanan dan suhu proses yang optimal diperoleh pada 1750 psi dan suhu 40oC  dengan  rafinat minyak akar wangi berkadar vetiverol  51.82 %,  bilangan ester 7.2 dan bilangan ester setelah asetilasi  172.4. Tingginya tekanan dan rendahnya suhu berpengaruh terhadap perolehan ekstrak; penurunan rafinat; peningkatan nilai  bobot jenis ekstrak dan rafinat; indeks bias ekstrak dan rafinat; putaran optik ekstrak dan rafinat; peningkatan viskositas ekstrak dan rafinat; peningkatan bilangan ester ekstrak, bilangan ester setelah asetilasi ekstrak, serta kandungan vetiverol.Kata Kunci: Minyak Akar Wangi, Vetiverol, Ekstraksi Fluida Superkritik Potential Indonesian vetiver oil export oriented industry of cosmetics, perfumes, soaps, therapeutic purposes, antiseptic, massage oil, pharmaceutical and pesticide presents a great opportunity to meet the needs of the world. In order to add value vetiver oil by increasing the levels vetiverol as the main component, was applied to carbon dioxide supercritical fluid extraction technology which is a combination of extraction, fractionation and deodorization with excellence supported carbon dioxide as an inert solvent, eco-friendly, easily separated, and the high solubility. Garut vetiver oil (Java vetiver oil) as raw material, has the characteristics vetiverol levels 39.03%, specific gravity of 0.9977; refractive index of 1.5247; optical rotation +38.1; solubility in alcohol 95% is a clear 1:1; acid number 28.1; ester number 24.6; ester number after acetylation 115.5; as well as fats and oils contain no oil keruing. The selection process conditions in order to produce optimal vetiverol content performed by varying the flow rate of CO2 gas, pressure and temperature as an important parameter in the success of vetiver oil extraction with supercritical CO2 fluid. The selection of a constant flow rate and more stable obtained at 5.5 liters / min, whereas for pressure variation extractor (1500-2000 psi) and extractor temperature (40-50oC); separator pressure and temperature of 500 psi and 25 °C as well as the processing time for five hours by taking extracts every hour. Pressure and temperature optimum process obtained at 1750 psi and a temperature of 40oC with rafinat vetiverol vetiver oil yield of 51.82%, ester number 7.2, and ester number after acetylation 172.4. The high pressure and low temperature affect the acquisition of the extract; rafinat decline; increase in the value of specific gravity and rafinat extracts; refractive index and rafinat extract; optical rotation and rafinat extract; increase in the viscosity of the extract and rafinat; increase in numbers ester extract, ester number after acetylation extracts, as well as the content vetiverol. Key word: Vetiver Oil, Vetiverol, Supercritical Fluid Extraction.

Optimization of a quantum weak measurement system with digital filtering technology

2018 ◽  
Vol 57 (27) ◽  
pp. 7956 ◽  
Author(s):  
Yang Xu ◽  
Lixuan Shi ◽  
Tian Guan ◽  
Dongmei Li ◽  
Yuxuan Yang ◽  
...  
Keyword(s):  
Measurement System ◽  
Digital Filtering ◽  
Weak Measurement

scholarly journals Drift Reduction of a 4-DOF Measurement System Caused by Unstable Air Refractive Index

Sensors ◽  
2020 ◽  
Vol 20 (21) ◽  
pp. 6329
Author(s):  
Ruijun Li ◽  
Yongjun Wang ◽  
Pan Tao ◽  
Rongjun Cheng ◽  
Zhenying Cheng ◽  
...  
Keyword(s):  
Refractive Index ◽  
Laser Beam ◽  
Measurement System ◽  
Degrees Of Freedom ◽  
Cost Effective ◽  
Control Mode ◽  
Detection Accuracy ◽  
Long Distance ◽  
Cost Effective Method ◽  
Novel Method

Laser beam drift greatly influences the accuracy of a four degrees of freedom (4-DOF) measurement system during the detection of machine tool errors, especially for long-distance measurement. A novel method was proposed using bellows to serve as a laser beam shield and air pumps to stabilize the refractive index of air. The inner diameter of the bellows and the control mode of the pumps were optimized through theoretical analysis and simulation. An experimental setup was established to verify the feasibility of the method under the temperature interference condition. The results indicated that the position stability of the laser beam spot can be improved by more than 79% under the action of pumping and inflating. The proposed scheme provides a cost-effective method to reduce the laser beam drift, which can be applied to improve the detection accuracy of a 4-DOF measurement system.

Optical method for measuring optical rotation angle and refractive index of chiral solution

2007 ◽  
Vol 46 (33) ◽  
pp. 8134 ◽  
Author(s):  
Jiun-You Lin ◽  
Kun-Huang Chen ◽  
Jing-Heng Chen
Keyword(s):  
Refractive Index ◽  
Optical Method ◽  
Rotation Angle ◽  
Optical Rotation

scholarly journals Optimization of a quantum weak measurement system with its working areas

2018 ◽  
Vol 26 (16) ◽  
pp. 21119 ◽  
Author(s):  
Yang Xu ◽  
Lixuan Shi ◽  
Tian Guan ◽  
Cuixia Guo ◽  
Dongmei Li ◽  
...  
Keyword(s):  
Measurement System ◽  
Weak Measurement
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