One‐ and two‐dimensional exchangeJ‐resolved CP‐MAS NMR spectrum of adamantane

K. Takegoshi; C. A. McDowell

doi:10.1063/1.450813

One‐ and two‐dimensional exchangeJ‐resolved CP‐MAS NMR spectrum of adamantane

The Journal of Chemical Physics ◽

10.1063/1.450813 ◽

1986 ◽

Vol 84 (4) ◽

pp. 2084-2090 ◽

Cited By ~ 14

Author(s):

K. Takegoshi ◽

C. A. McDowell

Keyword(s):

Mas Nmr ◽

Two Dimensional ◽

Nmr Spectrum ◽

Cp Mas Nmr

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ChemInform Abstract: One- and Two-Dimensional Exchange J-Resolved CP-MAS NMR Spectrum of Adamantane.

Chemischer Informationsdienst ◽

10.1002/chin.198627053 ◽

1986 ◽

Vol 17 (27) ◽

Author(s):

K. TAKEGOSHI ◽

C. A. MCDOWELL

Keyword(s):

Mas Nmr ◽

Two Dimensional ◽

Nmr Spectrum ◽

Cp Mas Nmr

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One- and Two-Dimensional 15N Exchange CP/MAS NMR Studies of the Structure and Electronic Properties of the Intermolecular N—H⋯N Hydrogen Bond in Imidazole Crystal

Solid State Nuclear Magnetic Resonance ◽

10.1006/snmr.2001.0039 ◽

2001 ◽

Vol 20 (3-4) ◽

pp. 145-155 ◽

Cited By ~ 6

Author(s):

T. Ueda ◽

H. Masui ◽

N. Nakamura

Keyword(s):

Hydrogen Bond ◽

Electronic Properties ◽

Mas Nmr ◽

Two Dimensional ◽

Nmr Studies ◽

Cp Mas Nmr

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Variable-temperature one- and two-dimensional 13C CP/MAS NMR studies of the dynamics of monohaptocyclopentadienyl rings of hafnium and titanium tetracyclopentadienyl in the solid state

Journal of Organometallic Chemistry ◽

10.1016/s0022-328x(98)01020-1 ◽

1999 ◽

Vol 577 (1) ◽

pp. 19-23 ◽

Cited By ~ 5

Author(s):

Eric J. Munson ◽

Michelle C. Douskey ◽

Susan M. De Paul ◽

Marcia Ziegeweid ◽

Leonidas Phillips ◽

...

Keyword(s):

Solid State ◽

Variable Temperature ◽

Mas Nmr ◽

Two Dimensional ◽

Nmr Studies ◽

Cp Mas Nmr ◽

13C Cp Mas Nmr

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Molecular Dynamics of Solid (Me3Si)3C−C⋮C−C(SiMe3)3As Seen by One- and Two-Dimensional CP/MAS NMR†

Organometallics ◽

10.1021/om9705463 ◽

1997 ◽

Vol 16 (24) ◽

pp. 5218-5222 ◽

Cited By ~ 6

Author(s):

Xavier Helluy ◽

Jörg Kümmerlen ◽

Angelika Sebald

Keyword(s):

Molecular Dynamics ◽

Mas Nmr ◽

Two Dimensional ◽

Cp Mas Nmr

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η5-Cyclopentadienyl derivatives of tin(II) studied by two-dimensional multinuclear magnetic resonance in solution and by13C and119Sn CP/MAS NMR in the solid state

Magnetic Resonance in Chemistry ◽

10.1002/mrc.1260301010 ◽

1992 ◽

Vol 30 (10) ◽

pp. 964-968 ◽

Cited By ~ 22

Author(s):

Bernd Wrackmeyer ◽

Ēriks Kupče ◽

Gerald Kehr ◽

Angelika Sebald

Keyword(s):

Solid State ◽

Magnetic Resonance ◽

Mas Nmr ◽

Two Dimensional ◽

Cp Mas Nmr ◽

Derivatives Of ◽

Multinuclear Magnetic Resonance

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Comparison of structure and thermal chemistry of stoichiometric and catalytic alkoxy-substituted molybdenum heteropolyanions: carbon-13 CP-MAS NMR spectrum of a chemisorbed reaction intermediate

Journal of the American Chemical Society ◽

10.1021/ja00247a030 ◽

1987 ◽

Vol 109 (13) ◽

pp. 4018-4023 ◽

Cited By ~ 20

Author(s):

W. E. Farneth ◽

R. H. Staley ◽

P. J. Domaille ◽

R. D. Farlee

Keyword(s):

Mas Nmr ◽

Nmr Spectrum ◽

Reaction Intermediate ◽

Thermal Chemistry ◽

Cp Mas Nmr

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Effect of water in the carbon-13 CP/MAS NMR spectrum of white spruce wood

Macromolecules ◽

10.1021/ma00173a020 ◽

1987 ◽

Vol 20 (7) ◽

pp. 1554-1556 ◽

Cited By ~ 21

Author(s):

J. M. Willis ◽

F. G. Herring

Keyword(s):

White Spruce ◽

Mas Nmr ◽

Nmr Spectrum ◽

Effect Of Water ◽

Spruce Wood ◽

Cp Mas Nmr

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Mesoporous hybrid materials containing functional organic groups inside both the framework and the channel poresElectronic supplementary information (ESI) available: 29Si CP MAS NMR spectrum of a representative hybrid material. See http://www.rsc.org/suppdata/cc/b2/b202179j/

Chemical Communications ◽

10.1039/b202179j ◽

2002 ◽

pp. 1382-1383 ◽

Cited By ~ 78

Author(s):

Robert J. P. Corriu ◽

Ahmad Mehdi ◽

Catherine Reyé ◽

Chloé Thieuleux

Keyword(s):

Hybrid Materials ◽

Hybrid Material ◽

Mas Nmr ◽

Supplementary Information ◽

Nmr Spectrum ◽

Cp Mas Nmr

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Crystal structure and solid-state31P CP-MAS NMR spectrum of the bis(trifluoroacetato) (triphenylphosphine)mercury(II) dimer [Hg(CF3CO2)2PPh3]2

Journal of Crystallographic and Spectroscopic Research ◽

10.1007/bf01160967 ◽

1990 ◽

Vol 20 (2) ◽

pp. 149-155 ◽

Cited By ~ 2

Author(s):

Tim Allman ◽

Francine B�langer-Gari�py ◽

Andr� L. Beauchamp

Keyword(s):

Crystal Structure ◽

Mas Nmr ◽

Nmr Spectrum ◽

Cp Mas Nmr

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NMR studies of 1-phenylazo-3-substituted-2-naphthols in solution and in the solid state

Collection of Czechoslovak Chemical Communications ◽

10.1135/cccc19900193 ◽

1990 ◽

Vol 55 (1) ◽

pp. 193-201 ◽

Cited By ~ 12

Author(s):

Antonín Lyčka ◽

Miroslav Nečas ◽

Josef Jirman ◽

Jaroslav Straka ◽

Bohdan Schneider

Keyword(s):

Hydrogen Bond ◽

Solid State ◽

Nmr Spectra ◽

Equilibrium Mixture ◽

Mas Nmr ◽

Nmr Studies ◽

Nmr Spectrum ◽

Cp Mas Nmr ◽

Hydrazone Form

The 1H and 15Nα-enriched 1-phenylazo-3-X-2-naphthols, where X = COOH (I), X = COOCH3 (II), and X = CONHC6H5 (III), have been measured in various solvents. The values of 1J(15Nα, H) and σ(15N) indicate that in CDCl3, C6D6, CCl4, and CD3NO2 solutions the compounds I and III exist practically completely in their hydrazone forms. The hydrazone form is stabilized by the hydrogen bond of COOH or CONH protons to the C(2)=O group. The compound II represents an equilibrium mixture of azo and hydrazone forms, since it cannot form a similar hydrogen bond. Moreover, the 15N NMR spectra of compounds I-III have been measured in solid state by the CP/MAS technique. The results indicate the existence of two conformers differing by the conformation of COOCH3 group in compound II, which is supported by the 13C CP/MAS NMR spectrum of compound II.

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